- h k M - 3AS.O DuPont-5990 TRADE SECRET Study Title H-24768: Subchronic Toxicity 90-Day Gavage Study in Rats with One-Generation Reproduction Evaluations Volume 2 of 5 Laboratory Project ID: DuPont-5990 Test Guidelines: U.S.

( Z A l S _ }JLHl Haskell Laboratory for Toxicology and Industrial Medicine April 5, 2002 J& M - TO: Study in Rats epeated-Dose Oral Toxicity Gavage Range Finder cc: G.

Maat - a n 439 >v TRADE SECRET Study Title H-25434: Static, Acute, 96-Hour Screening Test to Pimephales promelas Laboratory Project ID: DuPont-11408 3AS7 DuPont-11408 A u t h o r : Laurie D .

F 477 TRADE SECRET Study Title H-25878: ISO Biocompatibility Testing M IM DuPont-13216 Study M onitor: Carol Finlay, B.A.

000133 o jo -fit ~ 9 M W M am '*, ) BIOANALYTICAL REPORT Title: Date: Authors: Quantitative Determination o f Ammonium Perfluorooctanoate (APFO), M easured as the Perfluorooctanoate Anion (PFOA), in Human Serum from Study DW04 Using Turbo Ion Spray LC/MS/MS 30 September 2003 David J.

_A R a .% & it + S 000433 .A R M 6 - (fTMUIMEDIWl E. 1. d u P o n t d e N e m o u r s & C o m p a n y IHeOMMUTtD P.O.

Precise Research.

-ARSLI& _ / 3AO TSCA NCIC Notification Form for CBI Documents GDocket Number: _________ oLpt-_______ Document Control Number: o 3> c p c x p o o Document Date: (k~ Q ^ > ________________ Document Type: F __________________ C=3 css U) cC_Z 030 Z ~ o rn 1 "0 O <> -- i m T?

ftRAA, M M im t m m s x m M & t m c rii*--.

BOILING POINT TEST SUBSTANCE Id e n tity: Perfluorooctanesulfonate; may also be referred to as PFOS or FC-95. (1-O ctanesulfonicacid, 1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8heptadecafluoro-, potassium salt, CAS # 2795-39-3) Rem arks: Testing was not conducted.

Electronically Served 9/22/2017 10:33 PM Hennepin County, MN 27-CV-10-28862 Filed in Fourth Judicial District Court 11/17/2017 7:31 PM Hennepin County, MN STATE OF MINNESOTA DISTRICT COURT FOR THE COUNTY OF HENNEPIN FOURTH JUDICIAL DISTRICT CIVIL ACTION NO. 27-CV-10-28862 STATE OF MINNESOTA, et al. v. 3M COMPANY EXPERT REPORT OF PHILIPPE GRANDJEAN, MD, DMSc _________________________ PREPARED ON BEHALF OF PLAINTIFF STATE OF MINNESOTA 22 September, 2017 CONFIDENTIAL - SUBJECT TO A PROTECTIVE ORDER ENTERED IN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 27-CV-10-28862 Filed in Fourth Judicial District Court 11/17/2017 7:31 PM Hennepin County, MN TABLE OF CONTENTS I.

From: To: CC: Sent: Subject: Attachments: Hunstad, Mary P CIV NAVSEA HQ, SEA 05 Willey, Janice L CIV SEA04X, LQAO; Adelson, Jordan M CIV SEA04X, LQAO Corl III, William E CIV Chemist, LQAO, C1198; Fletcher, Steven G CIV NAVSEA HQ, SEA 05; Berkoski, Daniel T CIV NAVSEA, SEA 05 1/17/2017 2:46:38 PM Ausrailian Lab Proficiency Report NMI Proficiency report 2016 - PFOS & PFOA lab sampling-AQA16-06.pdf Jordan/Janice - Sending for info, you may already have it.

From: To: Sent: Subject: Attachments: Mach, Richard CIV OASN (EI&E), ODASN (Environment) Adelson, Jordan M CIV SEA04X, LQAO; Barclift, David J CIV NAVFAC LANT, EV; Berkoski, Daniel T CIV NAVSEA, SEA 05; Blodgett, Wayne CIV NAVFAC HQ, EV; Brant, Byron C CIV NAVFAC LANT, EV; Brown, Kim P CIV NAVFAC HQ, EV; Carlson, Margaret M CIV OASN (EI&E), OAGC (EI&E); Coghlan, Gunarti H CIV NAVFAC HQ, ENV; Corack, Jennifer M CIV NAVFAC Atlantic, EV; Derrick, Amy E CAPT CHINFO, DCI; Duchnak, Laura S CIV NAVFAC HQ, BRAC PMO; Dumenigo, Mario O CIV NAVFAC HQ, EV; Frederickson, Joshua M CIV OPNAV, N45; Gamache, Christopher D CIV l&L, GF; Greek, Patricia Z CIV CNIC, N452; Hayes, Dan E CIV NAVFAC HQ, EV; Heilman, David H CIV NAVFAC HQ, BRAC PMO; Holmes, Wanda L CIV OPNAV, N45; Hunstad, Mary P CIV NAVSEA HQ, SEA 05; Jaime Vega (jaime.vega2.mil@mail.mil); Laitila, Jeffrey P CIV NAVFAC MIDLANT, EV; Lansdale, Lawrence L CIV NAVFAC HQ, BRAC PMO; Nashold, Elizabeth A CIV NAVFAC MIDLANT, EV BLC; Nehm, Lindsay R CIV OPNAV, N45; Onyekanne, Chika LT CHINFO, 01-2; Porter, Christine H CIV CNIC HQ, N45; Preston, Gregory C CIV NAVFAC HQ, BRAC PMO; Puckett, Thomas G CIV CNIC HQ, OGC; Reisch, Timothy A CIV NAVFAC LANT, EV; Rosen, Marc S CDR OLA, LA-63; Rudroff, Jim CIV OASN (EI&E), ODASN Environment; Runyon, Rex A CIV PA; Sadorra, Robert A CIV NAVFAC HQ, EV; Schirmer, Robert G CIV NAVFAC MIDLANT, EV; Taplin, Aundrea E CIV OASN (EI&E), OAGC EI&E; Turner, Misha GS13 l&L, LFL; Walker, Yvonne P.

DEPARTMENT Oc TUE NAVY NAVAL SURFACE WARFARE CENTER CARDEROCK DIVISION NAVAL SHIP SYSTEMS ENGINEERING STATION 5001 S.

From: To: CC: Sent: Subject: Attachments: Mach, Richard CIV OASN (EI&E), ODASN (Environment) Hunstad, Mary P CIV NAVSEA HQ, SEA 05 John P.