p. 1 M ~~+ CVA cc U c~ o a W ct r--~ ~ . o U o3 ). eG . . : ;' 1 ~~~

p. 1 a'~'1 ~ O O aG L ~ = . .

~FR a26 6/D United Nations Environment Programm e UNEP F'OGRAMME CES NA!

ADVANCE UNEDITED DRAF T P.

.

~ Katherine E .

Study Title INHERENT AEROBIC AQUATIC BIODEGRADABILITY OF FLUOROALIPHATIC POLYMERIC ESTER OFf ]" - Data Requirement 40 CFR 792 [ Authors Study Completion Date Date of signi ng Performing Laboratory 3M Environmental Technology and Safety SeNices I 3M Environmental Laboratory 935 Bush Avenue St.

FINAL REPORT Epidemiology, 220-6W-08 `Medical Department 3M Company St.

: Smite, Sous AR7126-C032 SrCorporatToagy TY Se sa BG 3M Mortality Study of Employees at 3M Plant in Decatur, Alabama A retrospective cohort mortality studyofemployees, who worked at least one year (beginning in March, 1961) at the 3M chemical and film plants in Decatur Alabama, was conducted by University of Minnesota epidemiologists to determine whether the mortality experienceofthese employees was significantly different from that which `would be expected.

fe-y AIR/WATER PARTITION COEFFICIENT ITEESSTSSUUBSTTAANNCCEE ~~~ =000000000 Identity: PFeCr-f9l5u.oro(o1c-tOacnteasnuelsfuolnfaotnei;c macaiyd,a1l,s1o,2b,e2,r3e,f3e.r4r,e4d,5t,o5a.6s.6P,7F,O7.S8,o8r,6- heptadecafiuoro-, potassium salt, CAS #2795-39-3) Remarks: The test substance is a white powder.

AR226-00 33 LEY ACUTE EASTERN OYSTER SHELL DEPOSITION TEST SUBSTANCE Identity: PFCe-r9f5l.uor(oo1c-tOancetsaulnfeosnautlef;moacnaiiydc,al1s,o1,2b.e2,r3e,f3e.r4r,e4d,5t,o5,a6s,6P,7F,O7,S8.o8r,8heptadecafluoro-, potassium salt, CAS # 2795-35-3) 3ReMmlaort knsu:mbTehre2t1e7st. sSuabsmtpalnecewaissastwohrietde upnodwedrera.mbSiaenmtplceonwdiatsiotnaskepnriofrrotom teelsetmiengn.taPluraintayldyesteesrmteicnhendiqtouebse. 90.49% by LC/MS, H-HMR, "*F-NMR and METHOD TMyeptheo:d:StaOtiPcPaTcuSte850.1025 GLP: Yes YSpeeacriceso:mpClreatsesdo:stSrteuadvyircgoimnpiclaeted 1999.

ATTACHMENT TO LETTER TO C.

bo226-0209 PTO7S0F9P1K. 3M MEDICAL DEPARTMENT, CORPORATE TOXICOLOGY Protocal for Study No.

REPORT EVALUATION OF THE ABILITY OF T5869 TO INDUCE CHROMOSOME ABERRATIONS IN CULTURED PERIPHERAL HUNAN LYWPHOCYTES (WITH INDEPENDENT REPEAT) HNOOTTOOXX SPurbosjteacntce11358914936 - page 10f 26 - RECEIVED HOV a-9ng1994 TOACOLOLY 005605 T5869 - NOTOX Project 11593 STATEMENT OF GLP COMPLIANCE -- cr ----------------------imme NOTOX B.Y.., *s-Hertogenbosch, The Netherlands Trheecesnttudeyditdieosncriofb:ed in this report was conducted fn compliance with the most The OECD Principles of Good Laboratory Practice Which are essentially in conforaity with: The United States Food and Drug Adafnistration.

i-3 EETR226 -- 1017 :~ i i - rn CENTRAL SCIENCE LABORATORY >> i i [reid i, LY L. a i, e Ly STUDY NUMBERHTS602 PERFLUOROOCTANESULFONATE, POTASSIUM SALT(PFOS): _ TiTTHHE EHONEHONYEYBBEEEE & MAFF - 000002 CSL Study Number HT5602 STUDY NUMBER: HTS602 PAENRFALCUUOTREOOORCTAALNTEOSXUILCFIOTNYASTTEU,DPYOWTIATSHSITUHMESHAOLNTE(YPFBOS0)2: REPORT AMENDMENT NO | EPPO GUIDELINE 170 OECD GUIDELINE 213 i AUTHOR: 3 Paul Wilkins STUDY INITIATION DATE: 11Sepember2000 STUDY REPORT DATE: 23 March 2001 SUBMITTED TO: Evir3oMnCmoerpnorLaatbioornatory ScPa9u3,5 MBuiUsmshnkAevseonu5e5106 : Pertrming Laboratory: 3 EmEinvriornomnemnenttlalBRo&gDsTGeeaomnp 7 Central Science Laboratory = YorkSYanOdu1Hut1t1o7n, UK Environmental LaboratoryorFPrroect NumbPeargeU2l7of235 000003 (CSL Study Number HT5602 CENTRAL SCIENCE LABORATORY `CONFIDENTIAL Study title Test fucilty Study number Numberofpages: REPORT AMENDMENT 1 tPoexrifcliutoyrosotcutdaynwesiutlhftohneatBeo,nePyotbaesesium Salt (PFOS): An acute oral Environmental R&D Team, CSL, Sand Hutton, York, UK HTS602 5| i Signature, ithe Date OS/otft @aimmiyy) SPEntWvuiidlrykoiDninmrseencttaolr R&D Team, CSL Authorisation of release of report amendment SEE sigmue___|[Athens Management Representative MHeHadBEenvwironmental Biology Group, CSL Date_:&-01 (dd/mmiyy) eee st 2 This amendment has been noted by Quality Assurance as correction othe report 4 A sigue Cl ass (Dulles Date|C8tel(ddimmyy) MQrAsACudVitWoarlker Central Science Laboratory Environmental Laboratory Prcject Nomber U2723 Page 2015 000004 CSL Study Number HTS602 "wRTheheiasrsehoantshfeboeTreeansmtceoInrideemmctehenadtd:tboeTPehenerrfmeliuswo-arsospoeclttaaynspeosPguerlrfafopunhoairtcoeao,lcPetoartnraeossusolnifupomanSgaetas,l7P(oPatFnaOdsS)s.ioumAtfShfalotrfmi(naPatlFiOrneSgp)ort 1 ceroreocrtheadd.occurred on page 7, which had obscured the lengthofexposure.