WATER SOLUBILITY TEST SUBSTANCE Identity:N-methylperfluorooctanseulfonamidoethanolm;ay alsobe referredtoas N-MEFOSE Alcohol,FC-790, or FM-3925. (1Octanesulfonamide,N-methyl-1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8heptadecafluoro-N-(2-hydroxyethyClA)S-,# 24448-09-7) 'Remarks: Materialisan off-whitew,axy solid.Sample was taken from 3M lotnumber 505.

InternatioRneaslearcahndDevelopmenCtorporation SPONSOR: C OL.1P 0 U'-.

InternatioRneaslearcahndDevelopmenCtorporation SPONSOR: TEST MATERIAL: SUBJECT: 3M Company Fluorad Flucrochemical FC-143 Acute Oral Toxicity (LD Study in Rats. 50 Wilson P Dean, B.A.

Conducted at: During: Conducted by: Report by: Reviewed by: Riker Laboratories, Inc.Subsidiary of 3H St.

AR2X-05X BIOSEARCH, INC. p.o. box 8598 Philadelphia, Pennsylvania 19101 t el ephone: (215) 848-4499 Submitted to: Materi al : Sample Received: Date o f Report: T e s t: Object of Test: Procedure: R e s u lts : Conclus io n: 3M Company 3M Center S t.

R K i-O II ACUTE TOXICITY TO FISH TEST SUBSTANCE Identity: Perfluorooctanesulfonate, Ammonium salt; may also be referred to as PFOS NH4+ salt or FC-93. (1-Octanesulfonic acid, 1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-heptadecafluoro-, ammonium salt, CAS #29081-56-9) Remarks: Test sample was taken from 3M production lot #1.

ARiW-0350 BIOCONCENTRATION TEST SUBSTANCE_________________________________________________ Identity: N-ethylperfluorooctane sulfonamidoethanol; may also be referred to as N-EtFOSE Alcohol or FM-3422. (1-Octanesulfonamide, N-ethylI.I^.S.S^AS.S.e.e.TJ.S.S.S-heptadecafluoro-N-^-hydroxyethyl)-, CAS #1691-99-2) Remarks: Material is an off-white, waxy solid of uncharacterized purity.

/|R M - ACUTE TOXICITY TO FISH TEST SUBSTANCE Identity: Perfluorooctanesulfonylamido(ethyl)acetate; may also be referred to as PFOSAA, FC-128 or as the major component of FC-127, FC-129, FC-109, orFC-109-X.

/dR226- ACUTE TOXICITY TO FISH TEST SUBSTANCE Identity: Perfluorooctanesulfonylamido(ethyl)acetate; may also be referred to as PFOSAA, FC-128 or as the major component of FC-127, FC-129, FC-109, orFC-109-X.

fiKSLS.6 - O Z 2 9 ACUTE TOXICITY TO AQUATIC INVERTABRATES (DAPHNIA MAGNA) TEST SUBSTANCE____________________________________________ Identity: A mixture containing periluorooctanesulfonate, which may also be referred to as PFOS, FC-95, or as a component of FC-600. (1-Octanesulfonicacid, 1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8heptadecafluoro-, potassium salt, CAS # 2795-39-3) Remarks: The 3M production lot number was not noted.

BIOACCUMULATION (ANALYTICAL ONLY) TEST SUBSTAN Identity: NN--eEtthyFlOpSeErfAilucoorhooolctoarneFMs-u3lf4o2n2a.mi(d1o-eOtchtanaonle;sumlafoynaamlisodeb,eNr-eeftehryrle-d to as C1,A1S,2#.21,639,13-,49,94.,25),5,6,6,7.7.8,8,8-heptadecafluoro-N-(2-hydroxyethyl)-, Remarks: Material is an off-white, waxy solidof uncharacterized purity.

AR 836 -- 0789 ACUTE TOXICITY TO FISH (FATHEAD MINNOW) JIEST ~~ SUBSTANCE Identity: A mixture containing perfluorooctanesulfonate, which may also be referred to as PFOS, FC-95, or as a component of FC-206 or L3243. (1-Octanesulfonic acid) (CAS # 2795-39-3).

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SOIL ADSORPTION (METHOD DEVELOPMENT /PILOT STUDIES) TEST SUBSTANCE Identity:N-ethylperfluorooctasnuelfonamidoethanolm;ay alsobe referredto as N-ETFOSE Alcoholor FM-3422. (1-Octanesulfonamide,N-ethyl1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-heptadecafluoro-N-(2-hydroxyethyly, CAS # 1691-99-2) Remarks: Materialisan off-whitew,axy solidofuncharactedzed purity.

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