3M FLUOROCHEMICAL SUBMISSIONS February, 2002 - May, 2004 INDEX OF 3M'S 2002-2004 AR-226 DOCKET SUBMISSIONS BY DATE Back to Menu MARCH 2002 Click on Study Title to View Report March 13, 2002 March 13, 2002 Submission Cover Letter Final Report, Identification of Fluorochemicals in Human Sera.

PFOS: A DIETARY LC50 STUDY WITH THE MALLARD WILDLIFE INTERNATIONAL LTD.

BACK TO MAIN 3M FLUOROCHEMICAL SUBMISSION TOXICOLOGY, EPIDEMIOLOGY AND MEDICAL SURVEILLANCE December 2004 Click on Study Title to View Report December 2, 2004 "Ammonium Perfluorooctanoate: Age Effect on the PFOA Plasma Concentration in Post-Weaning Rats Following Oral Gavage," Paul M.

ACUTE TOXICITY TO FISH ARW W TEST SUBSTANCE Identity: Perfluorooctanesulfonyl fluoride; may also be referred to as POSF, or FX-8. (1-Octanesulfonyl fluoride, 1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-heptadecafluoro-, CAS #30735-7).

ff 3M Specialty Materials May 23, 2000 3M Center St.

P^ TX-^ % A C U TE TOXICITY TO FISH (FATHEAD MINNOW) TEST SUBSTANCE Identity: Perfluorooctanesulfonylamido(ethyl)acetate; may also be referred to as PFOSAA, FC-128 or as the major component of FC-127, FC-129, FC-109, or FC-109-X.

/waa-oMsq C O R N IN G Hazleton MUTAGENICITY TEST ON T-6342 MEASURING CHROMOSOMAL ABERRATIONS IN CHINESE HAMSTER OVARY (CHO) CELLS: WITH A CONFIRMATORY ASSAY WITH MULTIPLE HARVESTS FINAL REPORT AUTHOR Hemalatha Murli, Ph.D.

Attachments to Letter to C.

SUBMITTED BY: PREPARED BY: APPROVED BY: ARm-0503 E G & G, Bionomics Aquatic Toxicology Laboratory 790 Main Street Wareham, Massachusetts June, 1978 Brenda F.

A 2 2 2 -lclort Report Title Evaluation of the Northwest Bioanalytical Method Validation Reports for P F O S and Related Analytes in Human Serum or Plasm a in Meeting the Requirements of the _________ EDABioanalyticaLM ethod Validation Q A I Report No. 405-503 Data Requirement Full Validation of Bioanalytical Method Author Nancy Benson Philippe O urisson Quality Associates, Inc. 9017 Red Branch Road, Suite 102 Columbia, M D 21045 Sponsor 3M Environmental Laboratories 935 Bush Avenue Bldg 2-3E-09 St Paul, M N 55106 Report Date December 31, 2001 Report Number QAI 405-503 Number of Pages 26 337 TABLE OF CONTENTS I.

3 February 2004 AR226-1938 To: Mary F.

Katherine E.

3M 30p Kather ine E.

AR226-2017 AIR MONITORING FOR WORKER EXPOSURE TO C-B WASHINGTON WORKS TEN JOB ASSIGNMENTS WERE MONITORED (82 PERSONNEL SAMPLES) IN 1991.

TestResults flle:///C|/WINDOWS/TEMP/Polymers C-8 7-24-78 thru 1-3-98 23 pages.htm % I 1of43 AR226-2126 TestResulte sam ple Date Range C oncentration Range A ction Level Industrial Hygiene 7/24/78 100% 1/3/98 Sample D t Sam ple U D uration Type Employee Name Pars BTO : 18 TEFLON COPOLYMERS LOG: 001 FEP OVENS NORTH SIDE 12/18/79 47723 Z 1/15/80 47724 Z 1/22/80 47725 Z 8/8/80 47726 Z C hem ical Cone U nit Percent 0 8 0.0005 PPM 0.0% 0 8 0.0006 PPM 0.0% 0 8 0.0009 PPM 0.0% 0 8 0.0095 PPM 0.0% B TO : 18 TEFLON COPOLYMERS LOG : 002 FEP OVENS SOUTH SIDE 12/19/79 47601 z 1/25/80 47602 z 0 8 0.0001 PPM 0.0% 0 8 0.0031 PPM 0.0% AJP00694i BTO : 18 TEFLON COPOLYMERS LOC : 003 #1 OVEN COOLING TOWER 2/5/81 54696 z 2/11/81 54697 z 3/17/81 54698 z 5/23/81 54699 z 8/10/81 54700 z 8/11/81 54701 z . 0 8 0.0001 PPM 0.0% C-8 <0.0001 PPM 0.0% 0 8 0.0002 PPM 0.0% C-8 <0.0001 PPM 0.0% 0 8 0.0001 PPM 0.0% 0 8 <0.0001 PPM 0.0% 8/28/20014:49 PM E ID 140183 TestResults file:///C|/WINDOWSnTEMP/Polymers C-8 7-24-78 thru 1-3-98 23 pages.htm 8/12/81 64702 2 BTO: IO C : 18 TEFLON COPOLYMERS 004 #2 OVEN C 0 0 L IN 6 TOWER 2/5/81 61788 Z 2/11/81 61789 Z 3/17/81 61790 2 8/10/81 61791 2 8/11/81 61792 Z 8/12/81 61793 Z BTO: LOG: 18 TEFLON COPOLYMERS 183 FEP SHUTDOWN SAMPLES 5/12/81 61936 Z 5/12/81 81937 Z Tuesday, August 28,20013:24:20 PM C-8 <0.0001 PPM 0.0% C-8 0.0002 PPM 0.0% C-8 08001 PPM 0.0% C-8 0.0002 PPM 0,0% 0 8 0.0001 PPM 0.0% C-8 0.0001 PPM 0.0% C-8 <0.0001 PPM 0.0% C-8 <0.0001 PPM 0.0% C-8 <0.0001 PPM 0.0% Page 1 of 23 2 of43 AJP006942 Sample Dt Sam ple# D uration TYP Employee Name 5/12/81 61938 Z S/12/81 61939 2 5/12/81 61940 5/12/81 61341 5/12/81 61942 Z z z Pees Chem ical 08 08 08 08 . 08 Cone U nit Percent <0.0001 PPM <0.0001 PPM <0.0001 PPM <0.0001 PPM <0.0001 PPM 0.0% 0.0% 0.0% 0,0% 8/28/20014:49 PM E ID 140184 TesiResults file:///C|/WINDOWS/TEMP/Polymers C-8 7-24-78 thru 1-3-98 23 pages.htm 0.0% 5/13/81 61943 ) 5/13/81 61944 Z z C-8 <0.0001 PPM 0.0% C-8 <0.0001 PPM 0.0% 5/13/B1 61945 z C-8 <0.0001 PPM 0.0% 5/13/81 61946 z C-8 0.0001 PPM 0.0% 5/14/81 61947 z C-8 <0.0001 PPM 0.0% 5/14/81 61948 z C-8 <Q.0001 PPM 0.0% 5/14/81 61949 z 0 8 <0.0001 PPM 0.0% 5/14/81 61950 z O B <0.0001 PPM 0.0% 5/14/81 61951 z 0 8 <0.0001 PPM 0.0% 5/15/81 61952 2 0 8 <0.0001 PPM 0.0% 5/15/81 61953 Z 0 8 <0.0001 PPM 0.0% 5/15/81 61954 Z 0 8 <0.0001 PPM 0.0% 5/15/81 61955 Z 0 8 <0.0001 PPM 0.0% 5/15/81 61956 z 0 8 <0.0001 PPM 0.0% 5/18/81 61957 z 0 8 <0.0001 PPM 0 .0% 5/18/81 61958 z 0 8 <0.0001 PPM 0.0% 5/18/81 61959 z 0 8 <0.0001 PPM 0.0% 5/18/81 61960 z 0 8 <0.0001 PPM 0.0% 5/18/81 61961 z 0 8 <0.0001 PPM 0.0% 5/19/81 61962 Z ' 0 8 <0.0001 PPM 0.0% AJP006943 BTO: LOC: 18 184 TEFLON COPOLYMERS CLEAN-UP FOR SHUTDOWN 3 of 43 8/28/2001 4:49 PM E ID 140185 TestResults .j S/9/81 61900 S/9/B1 61901 5/9/B1 61902 5/10/81 61903 5/10/81 61904 5/10/81 61905 5/18/81 61906 file:///C|/WINDOWS/TEMP/Polymere C-8 7-24-78 thru 1-3-98 23 pages.hlm Z C-8 0.0002 PPM 0.0% Z C-8 0.0003 PPM 0.0% z C-8 0.0006 PPM 0.0% Z 0 8 0.0004 PPM 0.0% Z C-8 0.0004 PPM 0.0% Z 0 8 <0.0001 PPM 0.0% z C-8 <0.0001 PPM 0.0% BTO : 18 TEFLON COPOLYMERS LOG : 187 CONTRACTOR CLEANING AREAS 2/22/81 61816 z 3/12/81 61817 z Tuesday.