Document q3Yxa5m58dD56Jq6RDL3dNVpR

26 _ 06& T BIODEGRADATION (BOD/COD) TEST SUBSTANCE _________________________________________ Identity: A mixture containing perfluorooctanesulfonate; may also be referred to as PFOS, FC-95, or as a component of FC-185F. (1Octanesulfonic acid) (CAS # 2795-39-3) Rem arks: The 3M production lot number was 1-2303. The test sample is FC-185F, cc 817-19. Current information indicates it is a mixture of 4% PFOS, 36% diethylene glycol butyl ether, 29.29% water, 14% ethylene glycol, 8% Sultone foamer, 8.35% sodium octyl sulfate, 0.3% sodium lauryl sulfate, and 0.06% tolyltriazole. The following summary applies to a mixture with incompletely characterized concentrations o f impurities. Data may not accurately reflect the biodegradability o f the fiuorochemical component o f the test sample. M E T H O D :________________________________________________________ Method: Not noted. Type: Aerobic GLP: No Year completed: 1982 Contact time: 20 days Inoculum: Not given. RESULTS Chemical Oxygen Demand (COD): 1,200,000 mg/kg 1,200,000 mg/kg (replicate) Biochemical Oxygen Demand (BOD): 5-Day: 10-Day: 20-Day: 250.000 mg/L 990.000 mg/L 1,200,000 mg/L C O N C L U S IO N S ___________________________________________________ No conclusions given. Submitter: 3M Company, Environmental Laboratory, P.O. Box 33331, St. Paul, Minnesota, 55133 000116 DATA QUALITY R eliability: Klimisch ranking = 4. Values are from a summary sheet only raw data not found. Study lacks description and records of the method followed. The inoculum was not properly characterized. There is no characterization of the test substance purity, analytical measurement of the test concentrations, and confirmation of the amount of fluorochemical components in the solution. REFERENCES____________________________________________________ This study was conducted by the 3M Environmental Laboratory, St. Paul, Minnesota, Lab Request number 7544,1982. OTHER______________________________ . ______________________ Last changed: 6/26/00 000117 05/30/2000 ENVIRONMENTAL LABORATORY ARCHIVED FINAL REPORT 1 LAB REQUEST NO. 7544 REQUESTOR NAME: EAR DEPARTMENT: 0535 PROJECT NO: 9972210100 DATE RECEIVED: 12/17/1981 DESC: FC-185F (CC817-19) LOT 1-2303 CONTRACT LAB(S): EXP COMP DATE: 01/18/1982 DATE COMPLETED: 02/24/1982 PROJECT LEAD: SA BEACH PHONE NO: 651-778-7452 3M FAX NO: 651-778-6176 SAMPLE DATE CODE DESCRIPTION RESULT MDL on (95% C.I.) 1 1-2303 FC-185F 96-HR-LC50 BOD-05 BOD-10 BOD-20 COD SLUDGE-TOX FISH ACUTE TEST - 96 HOUR BOD-05 BOD-10 BOD-20 COD SLUDGE TOXICITY COMPLETE 250000 MG/L 990000 MG/L 1200000 MG/L 1200000 MG/KG SEE ATTACHED REPORT 2 DUP #1 ............ COD COD 1200000 MG/KG OOOllS