AR 2 6 _ 021 ACUTE TOXICITY TO FISH (BLUEGILL) TEST SUBSTANCE_______________________________________ Identity: A mixture containing perfluorooctanesulfonate, which may also be referred to as PFOS, FC-95, or as a component of FC-600. (1-Octanesulfonic acid, 1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8heptadecafluoro-, potassium salt, CAS # 2795-39-3) Remarks: The 3M production lot number was not noted.

AKZ2G - BIODEGRADATION (BOD/COD) TEST SUBSTANCE Identity: A mixture containing perfluorooctanesulfonate, which may also be referred to as PFOS, FC-95, or as a component of FC -201. (1Octanesulfonic acid, perfluoroalkyl sulfonate salts (5) + (5140P)) (CAS # 2795-39-3) Rem arks: The 3M production lot number was not noted.

Conducted at: During: Conducted by: Report by: Reviewed by: Riker Laboratories, Inc.Subsidiary of 3H St.

AR2X-05X BIOSEARCH, INC. p.o. box 8598 Philadelphia, Pennsylvania 19101 t el ephone: (215) 848-4499 Submitted to: Materi al : Sample Received: Date o f Report: T e s t: Object of Test: Procedure: R e s u lts : Conclus io n: 3M Company 3M Center S t.

R K i-O II ACUTE TOXICITY TO FISH TEST SUBSTANCE Identity: Perfluorooctanesulfonate, Ammonium salt; may also be referred to as PFOS NH4+ salt or FC-93. (1-Octanesulfonic acid, 1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-heptadecafluoro-, ammonium salt, CAS #29081-56-9) Remarks: Test sample was taken from 3M production lot #1.

ARiW-0350 BIOCONCENTRATION TEST SUBSTANCE_________________________________________________ Identity: N-ethylperfluorooctane sulfonamidoethanol; may also be referred to as N-EtFOSE Alcohol or FM-3422. (1-Octanesulfonamide, N-ethylI.I^.S.S^AS.S.e.e.TJ.S.S.S-heptadecafluoro-N-^-hydroxyethyl)-, CAS #1691-99-2) Remarks: Material is an off-white, waxy solid of uncharacterized purity.

/|R M - ACUTE TOXICITY TO FISH TEST SUBSTANCE Identity: Perfluorooctanesulfonylamido(ethyl)acetate; may also be referred to as PFOSAA, FC-128 or as the major component of FC-127, FC-129, FC-109, orFC-109-X.

/dR226- ACUTE TOXICITY TO FISH TEST SUBSTANCE Identity: Perfluorooctanesulfonylamido(ethyl)acetate; may also be referred to as PFOSAA, FC-128 or as the major component of FC-127, FC-129, FC-109, orFC-109-X.

fiKSLS.6 - O Z 2 9 ACUTE TOXICITY TO AQUATIC INVERTABRATES (DAPHNIA MAGNA) TEST SUBSTANCE____________________________________________ Identity: A mixture containing periluorooctanesulfonate, which may also be referred to as PFOS, FC-95, or as a component of FC-600. (1-Octanesulfonicacid, 1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8heptadecafluoro-, potassium salt, CAS # 2795-39-3) Remarks: The 3M production lot number was not noted.

Corporate Occupational Medicine 3M Center, Building 220-3W-05 St.

BACK TO MAIN i Attached are comments on the 3M Technical Report "Soil Thin Layer Chromatography - FC95, FC143, FM3422.

BACK TO MAIN Centre Analytical Laboratories, Inc. 3048 Research Drive State College, PA 16801 www.centrelab.com ^P hone: (814) 231-8032 Fax: (814) 231-1253 or (814) 231-1580 Analytical Report Fluorochemical Characterization of Sediment and Sludge Samples Cleveland, TN (W1973) Centre Analytical Laboratory Report No. 023-014Q (Revision 1) Revision Date 3/27/01 Testing Laboratory Centre Analytical Laboratory, Inc. 3048 Research Drive State College, PA 16801 3M Environmental Laboratory Contact Kent R.

A R m -0138 International Research and Development Corporation r^ l SPONSOR: COMPOUND: SUBJECT: 3M Company Fluorad Fluorochemical Surfactant FC-95 90-Day Subacute Rhesus Monkey Toxicity Study.

M M 6 - 0175 BIODEGRADATION (BOD/COD) TEST SUBSTANCE________________________________________________ Identity: A mixture containing perfluorooctanesulfonate, which may also be referred to as PFOS, FC-95, or as a component of FC-783. (1Octanesulfonic acid) (CAS # 2795-39-3).

AR22-OSOM ACUTE TOXICITY TO FISH TEST SUBSTANCE Identity: Perfluorooctanoic acid, ammonium salt; may also be referred to as PFOA ammonium salt, Ammonium perfluorooctanoate, PFO, FC116, FC-126, FC-169, orFC-143.