Report E01-1256 PFOS: A Reproduction Study with the Mallard AR226-1743 Study Title Analytical Phase Report for PFOS: A Reproduction Study with the Mallard Data Requirement FI FRA Subdivision E, Section 71-4 OECD Guideline 206 Author Lisa A.

TITLE: SAMPLE TRACKING OF WILDLIFE SAMPLES ANALYZED FOR CONCENTRATIONS OF PERFLUORINATED COMPOUNDS BY: John L.

i /[R 2 1 6 -0 4 5 H 3M Environmental Laboratory Final Report- Analytical Study Single-Dose Dermal Absorption/Toxicity Study of T-6067, T-6068 and T-6069 in Rabbits In-Vivo Study Reference Number: HWI#6329-152 Study Number: A M D T-011095.1 Test Substance: L -13492 (T-6067, T-6068 and T-6069) Name and Address of Sponsor: 3M SCD Division 367 Grove Street St.

A R 2 2 6 -1 9 5 4 Bladder Cancer in Perfluorooctanesulfonyl Fluoride Manufacturing Workers Final Report to ---*<* . t 13C :"n RF.TE!

AR226-2111 Test R esu lts Industrial Hygiene Sample Date Range 1/1/83 12/31/83 Concentration Range A ction Level 100% - -V.............. - Sample Dt Sam ple# D uration Type Employee Name Pere Chemical - BTO: 07 LO G : 411 TECHNICAL BLDG. 1 6 3 -1LAB GENERAL AREA 1/3/83 34060 1/4/83 34051 413 Z 403 z 2/4/83 34052 2/4/83 34053 424 z 427 z 3/1/83 34054 3/1/83 34055 418 z 419 z 4/5/83 34056 4/5/83 34057 433 z 431 z 4/29/83 34058 4/29/83 34059 5/10/83 34060 5/10/83 34061 441 z 441 z 444 z 443 z C-8/FC-143 C-8/FC-143 C-8/FC-143 C-8/FC-143 C-8/FC-143 C-8/FC-143 C-8/FC-143 C-8/FC-143 C-8/FC-143 C-8/FC-143 C-8/FC-143 C-8/FC-143 BTO: 08 TEFLON LOC : 701 FINE POWDER DRYER-EAST SIDE #2 1/3/83 46216 360 z 1/4/83 46217 360 z 1/4/83 48218 355 z 1/17/83 46219 360 z . 1/17/83 46220 360 z 1/18/83 46221 400 z 2/8/83 46222 360 z 3/1/83 46223 310 z 3/4/83 46224 300 z 3/4/83 2 2 5 300 z 3/7/83 46226 360 z 3/8/83 46227 300 z 4/10/83 46228 360 z 4/20/83 46229 300 z . 4/20/83 46230 270 z 5/18/83 46231 360 z 5/18/83 46232 360 z Tuesday, January 16,2001 10:26:39 AM C-8/FC-143 C-8/FC-143 C-8/FC-143 C-8/FC-143 C-8/FC-143 C-8/FC-143 C-8/FC-143 C-8/FC-143 C-8/FC-143 C-8/FC-143 C-8/FC-143 C-8/FC-143 C-8/FC-143 C-8/FC-143 C-8/FC-143 CS/FC-143 C-8/FC-143 Cone U nit Percent <103 MPB 0.11 MPB <0.03 MPB <0.03 MPB 0 .0 3 MPB 0 .0 3 MPB 0.35 MPB 0.12 MPB 0.03 MPB 0 .0 3 MPB 0.03 MPB 0.03 MPB 5.4% 19.6% 54% 5.4% 5.4% 5.4% 625% 21.4% 5.4% 5.4% 6.4% 5.4% 0 .0 3 MPB 0.12 MPB 0.06 MPB 0 .0 3 MPB 0 .0 3 MPB 0.04 MPB 0.04 MPB 0 .0 3 MPB 0.62 MPB 0.86 MPB 0.19 MPB <0.03 MPB 0 .0 3 MPB 0.2 MPB 0.06 MPB 1.58 MPB 0.03 MPB 5.4% 21.4% 14.3% 5.4% 5.4% 7.1% 7.1% 5.4% 110.7% ** 153.6% 33.9% 5.4% 5.4% 35.7% 10.7% 282.1% ** 5.4% Page 1 o f 43 AJP003948 EID 113083 1 Ta Sample D t Sam ple# D uration Type Em ployee Name 5/18/83 46233 6/4/B3 2 3 4 6/4/B3 4623S 6/4/83 46236 6/7/83 46237 6/8/83 46238 6/8/83 2 3 9 7/3/83 46240 8/15/83 46241 6/15/83 46242 8/15/B3 46243 10S/83 46244 11/22/83 46245 11/23/83 46246 360 2 400 Z 395 z 390 z 255 z 370 z 365 z 325 z 390 z 360 z 375 z 420 z 340 z 440 z Pera Chem ical C-8/FC-143 C-8/FO-143 C-8/FC-143 C-8/FC-143 C-8/FC-143 C-8/FC-143 C-8/FC-143 C-8/FC-143 C-8/FC-143 C-8/FC-143 C-8/FC-143 C-8/FC-143 C-8/FC-143 C-8/FC-143 BTO ; 08 LO C; 702 TEFLON FINE POWDER DRYER CONTROL ROOM (ALSO SEE TTF031 2/1/83 36514 560 z C-8/FC-143 3/2/83 36515 3/2/83 36516 3/6/83 36517 3/7/83 36518 3/7/83 36519 3/7/83 36620 390 z 390 z 360 z 360 z 360 z 360 z C-8/FC-143 C-8/FC-143 C-8/FC-143 C-8/FC-143 C-8/FC-143 C-8/FC-143 3/9/83 36521 3/14/83 36622 3/14/83 36623 3/14/83 36524 4/10/83 36525 375 z 393 z 396 z 396 z 360 z C-8/FC-143 C-8/FC-143 C-8/FC-143 C-8/FC-143 C-8/FC-143 4/18/83 36526 4/18/83 36527 4/18/83 365% 4/25/83 36529 4/25/83 36530 360 z 0 z 360 z 357 z 352 z C -8/F 0143 C -8/F C 443 C-8/FC-143 C-8/FC-143 C-8/FC-143 4/25/83 36531 5/17/83 36532 5/17/83 36533 6/2/83 36534 360 z 420 z 420 z 325 z C-8/FC-143 C-6/FC-143 C-a/PC-143 C-8/FC-143 6/2/83 36535 325 z C-8/FC-143 Tuesday, January 16,2001 10:26:39 AM 3.7^ MPB 04KM PB 0 ,o i'M P B 0 .3 # MPB a irfM P B 0.41 MPB 0.3M PB I 0 .4 9 |m PB 0.16|M PB 2.06 MPB 0B#M PB O .II m PB 0.07|M PB 0.19 MPB Percent 669.6% ** 83.9% , 5.4% 69.6% 33.9% 73.2% saw 875% m m ," 28.6% -t jgJ.. 3675% 153.6% ** 30.4% -SKPlISi 12.5% 335% 0.17 MPB 0.45 MPB 0.36 MPB 0.83 MPB 0.09 MPB 0.05 MPB 0.07 MPB <0.03 MPB 1.64 MPB 1.78 MPB 154 MPB 0.37 MPB 0.08 MPB 0.04 MPB 0.04 MPB 0.1 MPB 0.1 MPB 0.1 MPB 0 .

AR226-2523 % THIRD QUARTER 2003 C-8 SURFACE WATER AND GROUNDWATER MONITORING REPORT FOR WASHINGTON WORKS FACILITY AND LOCAL, LETART AND DRY RUN LANDFILLS WASHINGTON, WV Date: October 2003 Project No. : D6WW7423.01 18983632.00028 18983633.00026 18983634.00026 HI CORPORATE REM EDIATIO N G R O U P An Alliance between DuPont and URS Diamond Barley Mill Plaza, Building 27 Wilmington, Delaware 19805 ASH026479 EXD779761 E ID 779761 Surface W ater And Groundwater Monitoring Report Table of Contents TABLE OF CONTENTS 1.0 Introduction..,,...,.......--....*............ 2.0 C-8 Analytical Reporting............. . 3.0 Washington Works Facility 4.0 Local Landfill............................. ... 5.0 Letart Landfill................... ....:...... 6.0 D r y Run landfill,. >*>********>**************'***************#********>** 7.0 References,.,...,.,............ ............... ........................ ....................... ............................. .8 fable 1.0 Table 1.1A Table 1.1B Table 2.0 Table 2.1A Table 2.1B Table 3.0 Table 3.1A Table 3.1B Table 4.0 Table 4.1A Table 4.

AR226-2571 To: Andrew S Hartten/AE/DuPont@DuPont cc: Subject: Protocol for sampling and testing Forwarded by Isidores J Zan ikos/A E /D u Pon t on 10/02/2001 02:55 P M $ George H Senkler_Jr ' 10/02/2001 01:32 PM To: Isidores J Zanikos/AE/DuPont@DuPont, Mary A Kaiser/AE/DuPont@DuPont cc: John R Bowman/A/DuPont@DuPont Subject: Protocol for sampling and testing Per our discussion of last week, l have taken the materials that Mary had provided and crafted a document that might provide the "road map" for the procedures we use to map, sample and test, I would very much approcuiate your comments as to the adequacy of these instructions.

" pT Er Michael A.

GLP10-01-02; Amended Interim Report 14 Analysis of PFBS, PFHS, and PFOS in Groundwater BFI Morris Farm Landfill - MArch 2011 GLP10-01-02: Interim Report 14 - Analysis of PFBS.

INTERIM REPORT #24 - Analysis of Water.

Attachments to Letter to C.

BACK TO MAIN Study Title Microbial Metabolism (Biodegradation) Studies of Perfluorooctane Sulfonate (PFOS) II.

AR 126-OOI1 3M Environmental Laboratory Final Report- Analytical Study Single-dose Intravenous Pharmacokinetic Study of T-6049 in Rabbits In-Vivo Study Reference Number: HWI#6329-129 Study Number: AMDT-112294.1 Test Substance: FC-95 (T-6049) Name and Address of Sponsor: 3M SCD Division 367 Grove Street St.

/1R126-OK8 ATTACHMENT TO LETTER TO C.

fif 2 .6 _ 1 / ^ 3 JULY 2002 SURFACE WATER MONITORING REPORT FOR WASHINGTON WORKS FACILITY AND LOCAL, LETART AND DRY RUN LANDFILLS WASHINGTON, WV Date: September 2002 Project No.: D6WW7423.01 18983635.20000 CORPORATE REMEDIATION GROUP An Alliance between DuPont and URS Diamond Barley Mill Plaza, Building 27 Wilmington, Delaware 19805 Surface water Monitoring Report Table of Contents TABLE OF CONTENTS 1.0 Introduction...................................................................................................................1 2.0 C-8 Analytical Reporting.............................................................................................2 3.0 Washington WorksFacility..........................................................................................3 4.0 Local Landfill............................................................................................................... 4 5.0 Letart Landfill.............................................................................................................. 5 6.0 Dry Run Landfill.......................................................................................................... 6 7.0 References.................................................................................................................... 7 Table 1.0 Table 2.0 Table 3.0 Table 4.0 Figure 1.0 Figure 1.1 Figure 1.2 Figure 2.0 Figure 2.1 Figure 2.2 Figure 3.0 Figure 3.1 Figure 3.2 Figure 4.0 Figure 4.1 Figure 4.2 TABLES C-8 in Surface Water - Washington Works Facility C-8 in Surface Water - Local Landfill C-8 in Surface Water - Letart Landfill C-8 in Surface Water - Dry Run Landfill FIGURES Site Location Map - Washington Works Facility Surface Water Sample Location Map - Washington Works Facility C-8 Concentration Map July 2002 - Washington Works Facility Surface Water Site Location Map - Local Landfill Surface Water Sample Location Map - Local Landfill C-8 Concentration Map July 2002 - Local Landfill Outfalls Site Location Map - Letart Landfill Surface Water Sample Location Map - Letart Landfill C-8 Concentration Map July 2002 - Letart Landfill Outfalls Site Location Map - Dry Run Surface Water Sample Location Map - Dry Run Landfill C-8 Concentration Map July 2002 - Dry Run Landfill Outfalls JULGMR.doc Sep. 17. 02 Wilmington, DE 000444 Surface water Monitoring Report Table of Contents Appendix A Appendix B Appendix C Appendix D Appendix E Appendix F Appendix G Appendix H APPENDICES Laboratory Analytical Data Reports - Washington Works Facility Chain-of-Custody Records - Washington Works Facility Laboratory Analytical Data Reports - Local Landfill Chain-of-Custody Records - Local Landfill Laboratory Analytical Data Reports - Letart Landfill Chain-of-Custody Records - Letart Landfill Laboratory Analytical Data Reports - Dry Run Landfill Chain-of-Custody Records - Dry Run Landfill JULGMR.doc Sep. 17. 02 Wilmington, DE 060445 ii Surface water Monitoring Report Introduction 1.0 INTRODUCTION A multi-media consent order (Order No.