Ea `ff - ~ { AR2_83460!

ARRAG _ S416 - 20 Pe 000212 ARBRE - DHE .

3M ENVIRONMENTALLABORATORY PROJECT05-0210: INTERIMREPORT#20 Interim Report #20: Analysis of Water Samples from Northern Alabama Potable Water Systems, February 2006 Study Title ANALYSISOF PERFLUOROBUTANESULFO(PNFABTSE), PERFLUOROHEXANESULFONATE (PFHS), AND PERFLUOROOCTANESULFONATE(PFOS) IN WATER, SOIL, SEDIMENT, FISH, CLAMS, VEGETATION, SMALL MAMMALIVERAND SMALL MAMMALSERUM USING LC/MS/MS FOR THE 3M DECATURMONITORINGPROGRAM Data Requirement EPA TSCA Good Laboratory Practice Standards 40 CFR 792 Author Susan T.

Je3 : B .

WATER DEPARTMENT : 167 MAIN STREET *SAYREVILLE, N.J. 08872 : `TEL. (732) 390-7060 * FAX(732)238-2147 November 16, 2007 SDteaptaerotfmeNnetwofJeErnsveiyronmental Protection Bureau of Safe Drinking Water P.0.

-~-----~-~~--~-

pt Perfluorinated Sulfonic Acids and Perfluorinated Carboxylic Acids by HPCL/MS n CPlrioejnetc:t: Sample Matrix: LaSabmpCloedeN:ame: Analytical Report BaCraomnp D&reBsusderdP&.CM/e9K5e7e7,0-I7n5co3r1p9orated (CDM) Water FKi1e0ld00B9l1an1k00#11 P2 SeDravtieceCoRlelqeucetsetd:: K2/10101009019143 DateReceived: 2/210 BUansiitss:: NnAp Perfluorinated Sulfonic Acids and Perfluorinated Carboxylic Acids by HPLCIMS APnraelpytMiectahloMde:thod: MPeFtOhAod Analyte Name PPerfleuoroo-ni-reinddeceacnaoincoacciaded Porfluarobuanesufonate PPeerrflluuoorrcobduecaannoeiScuAlfcoindate PerfluorodecanoicAcid PPeerrflluuaarroohdeopdeicaanniocieAcAicdid Perluorohexancsulfonate PePrelrufolrooronhoenxaannaciicc AAcciidd Perfluorooctanesulfonate PPeerrfflluuoorrooopcetnatnaonicciAccAicdid PerfluoroundecanaicAcid Rest@ NNDUU NDU [ENwU DU NNDUUT eR) 0N34DU 039) N0D0 1U NU MRL MDL DFialctwoorn ExtDraatceted AmDlayteed ExtrLaocttion AnaLloytsisNote 5300 005%5 T 1 i 2an0 uTmiR02O0sNe Tloossiaz T10o3a6 50 omy 1 Jamo 28nooeis isi isi 5500 000I95 11 22w4ln0o 2am9i0002604s6 1lo0s5i4e6z2 11950033662 50 08 1 4no amiss si loess: T5s0o 000858 11 2u4n0o0 a29m10o06s46 Il0ossiic2z 1190036s2 50 000 1 2410 29100686 losic2 looser SS000011 50006 11 1 u24o10 1290020604s6 1l0o5s2e 11930033662 2410 uss iosi2 looser 5S00 000066111 2244Nm00 21n002060d46 l100s5i4s6z2 115900336622 50 13 1 Jano moss losis 1o0s Surrogate Name %Rec CoLnimtirtosl AmDlatyeed Q Nowe PaPrefrlulolrioo-rno-a{1.1223344.51-31043)03b]utnanooi maacdd 8105 SS001100 I29O/1N00S6: PePrefrlfulouroor-on-.n(-1{.1221334C-21)3dCe4c]aoncotiacnaoiccidacid Perfluoro-n-[12-13C2] hexanoic acid 0100 1015500 228m110022005544 5 50150 29000646 PPeerrfflluucorroo--nn--{{11.22--1133CC22Jludnoddeeccaanncciic AAcciidd Solum pero 1,234.130H onesie a5 77 0000500 22110022005544 S150 M0208 Sodiumperhuoro--hexane{1802sulfonate 0 S150 200646 Comments -_-- -_ Fd im S 22u1013m35ss fomia Soames toms 12 Client: SPraomjpeclte:Matrix: Sample Name: Lab Code: Analytical Report BCaarmopn &DBruded&sPM.scCK9eSeTerT.0-I7nSc3or1p9orated (CDM) Water EKl1ly0s0o0n91"1R-a0w0"2 p.3 SeDravtieceCoRlelqeucetsetd:: K21010/1009111002 DateReceived: 2/210 Units: Basis: nglL NA Perfluorinated Sulfonic Acids and Perflsorinated Carboxylic Acids by HPLC/MS PAnraelpytMiectahloMde:thod: PFOA Method APnerae fllyvtoreo-e Nna-tmeetradecanoicacid.

oo | AR126-0007 = AbsorepvteironaofsiFngel-e252O-r4Macs D1onsreata 6 cotober 26, 1973 Conducted at: Durtig: Conducted bys Report by: Reviewed by: RSSiuekbesripdauiLlaa,rbyoMraoitfnonreaisneost,a Inc. 55101 une to uly, 1979 5. 3.

AR226-00%3 pros `A 96-HOUR STATIC ACUTE TOXICITY TEST `WITH THE FATHEAD MINNOW(Pimephales promelas) FINAL REPORT `WILDLIFE INTERNATIONAL LTD.

`CENTRE FOR XENOBIOTIC RESEARCH University of Dundee, Biomedical Research Centre, Level 5, Ninewells Hospital and Medical School, Dundee, DD1 9SY Study Report Determinationofcyanide insensitive Palmitoyl-CoA oxidation in samples from 3M Environmental Laboratory -- Covance Studies 6329-183 and 6329-212 Study Number XR0108 w pater: So fore lion .

July 30, 1998 OTs atid!

3M MEDICAPLroDtoEcPolAfRoTr MStEuNdTy,NoC.OTR-7P1O32R.2A;TSET-T3O9XICOLOGY PHARMSTA UDYC OFPO ERFK LUOI ROOCNTANE ESUT LFOI NAMC IDE INRATS TSchlpereaarogabunjeceecDtaainvwedloebfiyotrlhaoitgssisctaaufldtpyeearrisssitiosntageslnesceeoosrasflPtdehoerspfeol.tueoAnrntoailoayclstfiaosnorefoStauhlleafbossneoarrmupimtd,ieov(neP,ruF,rOuirSniaArn)yeaainnnmddafrfosoceasl PmfeoFrtOhpoSodtAesn.itsiPatrlheemveiutolautbisomslatitutedeimseesotoafbfPotFlhiOetSeNA-inetwahitylsllb(de1e,rp2i)ev;rafhtoiovrwemeoevfdebrP,yFLtOhCeSMAanSahlayavtniecdaclpoetnrechclahupiosqdoutdehheeurtsed in PptehFreOfsleSsutAourdotiooecrstwaenaesssultuofhnoialnbalitvesetse(ouePdFeaOtnSed)cs.teaaNlrlocphpofthoearnrtmioaatclhoemkreitpnaoebstosiilcbiltseteu,mdeiitenascblohuladivitenegsyeitnbteheenurdionneesocna lafeenvcdeelst.

@ HAZLETON oroncs ones ve cron s onIO 07 KINSMAN BLYD + .0.B0KT643 + MADISON, WISCONSIN $3767 - PH6O082N614E71 + LXT0358RAZTALWES 05 FINAL REPORT EETEEE\ ( sanazies \w,e 4 as ges" FRTIOONGXENIRECSOOL6.TOAGYPMESRIEKNIRINVNSIGCE&SMANUFACTURING COMPANY ST.

Attachments to Letter to C.

gr 25, 1399812:41PK POREDICAL 220 ZF 02c@oucuTess + E7zi77s %0. 0773 5253 ' REPORT EVALUATION OF THE MUTAGENIC ACTIVITY OF 1.6506 IN AN JVNITRO MAMMALIAN CELL GENE MUTATION TEST WITH L5178Y MOUSE LYMPHOMA CELLS (WITH INDEPENDENT REPEAT) NNOOTTOOXX SPurbosjteacntce22738475481 * page 1 of 31 - , ~ ._ 738 MZ emiroars ag i asa samen2een i : ry i --_--r-i80b i 001362 UN 25, 1398912: 41PM POHEDouICAL 220 JFE Q2ENMOUTERSTERS+ 67331773 Ho.0mE3 E3 T-6906 S-T_ATEMENT OF GLP CoupLIANCE NOTOX Project 223458 !