3M General Offices 3S6Mi5.UPCaeu3m3l.eM1i1N1055144-1000 _ 3 T 7 September 24, 2003 IJ By Hand Delivery Document Processing Center (7407) Office of Poilution, Prevention and Toxics U.S.

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p. i "McCrea, Deborah" < mccrea@taftlaw.com> 06/04/2010 02:14 PM To NCIC OPPT@EPA cc "Bilott, Robert A."

P-1 Acquisition Date Vial Position Sample Name Acquisition Method 1 2/17/2010 18:30 1 IB PFCkinetexLong.dam 2 2/17/2010 18:52 2 PFC O.IOppb PFCkinetexLong.dam 3 2/17/2010 19:00 3 PFC 0.5ppb PFCkinetexLong.dam 4 2/17/2010 19:08 4 PFC 1.Oppb PFCkinetexLong.dam 5 2/17/2010 19:15 5 PFC 5.Oppb PFCkinetexLong.dam 6 2/17/2010 19:23 6 PFC10ppb PFCkinetexLong.dam 7 2/17/2010 19:30 7 PFC 20ppb PFCkinetexLong.dam 8 2/17/2010 19:38 8 PFC 50ppb PFCkinetexLong.dam 9 2/17/2010 19:53 7 PFC 20ppb CCV PFCkinetexLong.dam 10 2/17/2010 20:01 9 PFC 20ppb ICV PFCkinetexLong.dam 11 2/17/2010 20:08 25 K1001011-001 PFCkinetexLong.dam 12 2/17/2010 20:16 26 K1001011-002 PFCkinetexLong.dam 13 2/17/2010 20:23 27 K1001011-003 PFCkinetexLong.dam 14 2/17/2010 20:31 28 K1001011-004 PFCkinetexLong.dam 15 2/17/2010 20:38 29 K1001011-005 PFCkinetexLong.dam 16 2/17/2010 20:46 30 K1001011-006 PFCkinetexLong.dam 17 2/17/2010 20:54 31 K1001011-007 PFCkinetexLong.dam 18 2/17/2010 21:01 32 K1001011-008 PFCkinetexLong.dam 19 2/17/2010 21:09 33 K1001011-009 PFCkinetexLong.dam 20 2/17/2010 21:16 34 K1001011-010 PFCkinetexLong.dam 21 2/17/2010 21:24 35 K1001011-011 PFCkinetexLong.dam 22 2/17/2010 21:31 36 K1001011-012 PFCkinetexLong.dam 23 2/17/2010 21:39 37 K1001011-013 PFCkinetexLong.dam 24 2/17/2010 21:46 38 K1001011-014 PFCkinetexLong.dam 25 2/17/2010 21:54 39 K1001011-015 PFCkinetexLong.dam 26 2/17/2010 22:02 40 K1001011-016 PFCkinetexLong.dam 27 2/17/2010 22:09 41 K1001011-017 PFCkinetexLong.dam 28 2/17/2010 22:17 42 K 1001011-018 PFCkinetexLong.dam 29 2/17/2010 22:24 43 K1001011-019 PFCkinetexLong.dam 30 2/17/2010 22:32 44 K1001011-020 PFCkinetexLong.dam 31 2/17/2010 22:39 45 KQ1000664-01 PFC kinetexLong .dam 32 2/17/2010 22:47 46 KQ1000664-02 PFCkinetexLong.dam 33 2/17/2010 22:54 47 KQ 1000664-03 PFCkinetexLong.dam 34 2/17/2010 23:02 48 KQ 1000664-04 PFCkinetexLong.dam 35 2/17/2010 23:10 49 KQ 1000664-05 PFCkinetexLong.dam 36 2/17/2010 23:17 50 KQ 1000664-06 PFCkinetexLong.dam 37 2/17/2010 23:25 23 KQ1000620-01 PFCkinetexLong.dam 38 2/17/2010 23:32 24 KQ1000620-02 PFCkinetexLong.dam 39 2/17/2010 23:40 22 KQ1000620-05 PFCkinetexLong.dam 40 2/17/2010 23:47 21 KQ 1000620-06 PFCkinetexLong.dam File Name 021710\CalLong.wiff 021710\CalLong.wiff 021710\CalLong.wiff 02171 OICalLong.wiff 021710\CalLong.wiff 02171 OICalLong.wiff 02171 OICalLong.wiff 02171 OICalLong.wiff 02171 OICalLong.wiff 02171 OICalLong.wiff 021710\SamplesLong.wiff 021710\SamplesLong.wiff 021710\SamplesLong. wiff 021710\SamplesLong,wiff 021710\SamplesLong.wiff 021710\SamplesLong.wiff 021710\SamplesLong.wiff 02171 OISamplesLong.wiff 021710\SamplesLong.wiff 02171 OVSamplesLong.wiff 021710\SamplesLong.wiff 021710\SamplesLong.wiff 021710\SamplesLong.wiff 02171 OISamplesLong.wiff 021710\SamplesLong.wiff 02171 OISamplesLong. wiff 021710\SamplesLong.wiff 021710\SamplesLong. wiff 02171 OISamplesLong.wiff 021710\SamplesLong. wiff 021710\SamplesLong.wiff 021710\SamplesLong.wiff 021710\SamplesLong.wiff 021710\SamplesLong.wiff 021710\SamplesLong.wiff 021710\SamplesLong.wiff 021710\SamplesLong. wiff 021710\SamplesLong,wiff 021710\SamplesLong.wiff 021710\SamplesLong.wiff IS Peak Area (counts) 450.62 2504200 2783700 2542500 2677400 2754900 2957800 2651100 2907400 2664400 3217400 3083200 3489500 3542200 3322000 3135900 2890600 3090100 3320900 3007600 2911800 3291800 3060500 3300300 3145300 2786900 3174100 2954300 2900400 2939100 2634600 2867600 2693100 2491600 2954000 2741700 2971200 2881600 2873500 2808200 Z 402 Prep Run#: 105653 Team: Petroleum HC/SMCDONALD Number o f Copies to make: 1 # Lab Code Client ID 1 K1000968-001 2 K 1000968-020 3 K1000968-019 4 K 1000968-018 5 K 1000968-017 6 K 1000968-016 7 K1000968-015 8 K 1000968-014 9 K1000968-013 10 K 1000968-012 11 K 1000968-011 12 K1000968-010 13 K 1000968-009 K1000968-008 K1000968-007 16 K1000968-006 17 K1000968-005 18 K 1000968-004 19 K 1000968-003 20 K 1000968-002 21 K Q 1000620-03 22 K Q 1000620-04 23 KQ 1000620-01 24 KQ 1000620-02 25 KQ1000620-05 26 KQ 1000620-06 Field Blank 2 Field Blank 3 F: Scott "Treated" F:Scott "Raw" West Well Plant "Treated" West Well Plant "Raw" W & Avery "Treated" W & Avery "Raw" West Pensacola "Treated" West Pensacola "Raw" Bronson "Treated" Bronson "Raw" Lillian "Treated" Lillian "Raw" Dunaway "Treated" Dunaway "Raw" McCory "Treated" McCory "Raw" University Parkway "Treated" University Parkway "Raw" K1000968-010 MS K 1000968-010 DMS K 1000968-011 MS K1000968-011 DMS LCS MB Preparation information encnsneet Prep WorkFlow: OrgExtAq(14) Prep Method: Method Status: Prepped Prep Date/Time: 2/8/10 07:28 AM B # Method /Test .01 PFO A PFO A .01 PFOA/PFOA .01 PFOA/PFOA .01 PFOA/PFOA .01 PFOA'PFOA .01 PFOA'PFOA .01 PFOA/PFOA .01 PFO A PFO A .01 PFOA'PFOA .01 PFO A PFO A .01 PFO A PFO A .01 PFO A PFO A .01 PFO A PFO A .01 PFO A PFO A .01 PFO A PFO A .01 PFO A PFO A .01 PFO A PFO A .01 PFO A PFO A .01 PFO A PFO A .01 PFO A PFO A .01 PFO A PFO A .01 PFO A PFO A .01 PFO A PFO A .01 PFO A PFO A X PFOAPFOA PFOAPFOA pH Matrix X Water 7 Water 7 Water 7 Water 7 Water W ater X X Water / Water 7 Water W ater 7 y Water 7 Water 7 Water X Water 7 Water X Water 7 Water 7 Water 7" Water 7 Water 7 Liquid 7 Liquid 7 Liquid Liquid X 7 Liquid 7 Liquid Amt.

INTERIM REPORT # 1-Analvsis of Public Water Samples STUDY TITLE Analysis of Perfluorobutanesulfonate (PFBS), Perfluorohexanesulfonate (PFHS), and Perfluorooctanesulfonate (PFOS) in Water, Soil, Sediment, Fish, Clams, Vegetation, Small Mammal Liver and Small Mammal Serum Using LC/MS/MS for the 3M Decatur Monitoring Program DATA REQUIREMENTS EPA TSCA Good Laboratory Practice Standards 40 CFR 792 STUDY DIRECTOR Jaisimha Kesari P.E., DEE Weston Solutions, Inc. 1400 Weston Way West Chester, PA 19380 Phone: 610-701-3761 INTERIM REPORT COMPLETION DATE March 8, 2005 PERFORMING LABORATORY Exygen Research 3058 Research Drive State College, PA 16801 Phone: 814-272-1039 STUDY SPONSOR 3M Company 3M Building 0236-01-B-10 St.

3M Company St.

3M Environmental Laboratory Report No.

3M Company St.

INTERIM REPORT #3 - Analysis of Fish and Clam Samples STUDY TITLE Analysis of Perfluorobutanesulfonate (PFBS), Perfluorohexanesulfonate (PFHS), and Perfluorooctanesulfonate (PFOS) in Water, Soil, Sediment, Fish, and Clams Using LC/MS/MS for the 3M Decatur Monitoring Program DATA REQUIREMENTS EPA TSCA Good Laboratory Practice Standards 40 CFR 792 STUDY DIRECTOR Jaisimha Kesari P.E., DEE Weston Solutions, Inc. 1400 Weston Way West Chester, PA 19380 Phone: 610-701-3761 INTERIM REPORT COMPLETION DATE June 17, 2008 TESTING FACILITY MPI Research, Inc. 3058 Research Drive State College, PA 16801 Phone: 814-272-1039 STUDY SPONSOR 3M Company 3M Building 0236-01-B-10 St.

31VI General Offices April 21, 2000 3M Center St.

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HAZLETON WASHINGTON 9SOO LE ESBU RG PIKE V I E N N A , VA. 2 2 1 8 8 - 1 6 9 9 154-209 ANALYSIS OF T-5878 IN A CELL PROLIFERATION ASSAY IN RAT LIVER CELLS FINAL REPORT AUTHOR Maria A.