/)R m - 0 1 % 3 Special Lens Oral Teratology Study of T-2999CoC in Two Strains of Rats Experiment No.: Conducted At: Dosing Period: Study Director: 0681TR0362 Safety Evaluation Laboratory Riker Laboratories Inc.

M u t a g e n i c i t y T e s t i n g of 2-[N-ethyl-N-perfruoloalkyl(C=l~ 8) sulfonylami.no] ethylacrylate in B a c t e r i a l R e v e r s e M u t a t i o n A s s a y s (study number 2862) T " 32-2.5 pie P' | B M L , INC.

fR 226~36i{ HYDROLYSIS (ALKALINE) TEST SUBSTANCE________________________________ Identity: N-ethylperfluorooctane sulfonamidoethanol; may also be referred to as N-EtFOSE Alcohol or FM-3422. (1-Octanesulfonamide, N-ethyl1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-heptadecafluoro-N-(2-hydroxyethyl)-, CAS #1691-99-2) Remarks: Material is an off-white, waxy solid of uncharacterized purity.

ff 3M Specialty Materials May 23, 2000 3M Center St.

AR& -0 H % BIOCONCENTRATION TEST SUBSTANCE Identity: Perfluorooctanoic acid, ammonium salt; may also be referred to as PFOA ammonium salt, Ammonium perfluorooctanoate, PFO, FC116, FC-126, FC-169, orFC-143.

Afi Jt%-053S MICROTOX TOXICITY TEST TEST SUBSTANCE Identity: Perfluorooctylsulfonate, didecyldimethylammonium salt; may also be referred to as Fluoroalkyl ammonium derivative. [1Decaminium, N-decyl-N,N-dimethyl-, salt with 1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-heptadecafluoro-1 octanesulfonic acid (1:1), CAS # 251099-16-8] Remarks: The 3M production lot number was Lot 1.

^ 036-0537 TOXICITY TO AQUATIC PLANTS (E.G., ALGAE) TEST SUBSTANCE Identity: Perfluorooctylsulfonate, didecyldimethylammonium salt; may also be referred to as Fluoroalkyl ammonium derivative. [1Decaminium, N-decyl-N,N-dimethyl-, salt with 1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-heptadecafluoro-1octanesulfonic acid (1:1), CAS # 251099-16-8] Remarks: The 3M production lot number was Lot 1.

AU 2 6 - 63ST ?

% J U(3i T l* . 7 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY WASHINGTON, D.C. 20460 FYT-0301- /37* March 20, 2001 FYI-00-001378 FYI-00 378 / !

( R R 9 .3 - & -4 R i i & - \ & C Ce: S.

f1 r Analytical Report: LIMS E02-1053 Analytical Report: LIMS E02-1053 J.A&_ uro A nalytical Laboratory Report Title Comparative Analysis of Fluorochemicats in Human Serum Samples Obtained Commercially Data Requirem ent Not Applicable A u th o r Lisa Stevenson Study Com pletion Date 1 1 /1 3 /0 2 Perform ing Laboratory Extractions and Analyses 3M Environmental Laboratory Building 2-3E-09,935 Bush Avenue St.

ARJUlG - 1171 CONSENT ORDER ISSUED PURSUANT TO ARTICLES 5 and 12, CHAPTER 22 AND ARTICLE 1, CHAPTER 16 OF THE WEST VIRGINIA CODE.

I yA, Acl _ // If.

AR AG _ TSCA NCIC Notification Form for CBI Documents Docket Number: _______ftR J 2& _______________ Document Control Number: (fC?

A d .16 / A 5 7 Ce: R.