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AR226-3121 CONFIDENTIAL DPT 433/984485/AC acute derm al to xicity to the rat Sponsor DuPont Speciality Chemicals Jackson Laboratory Chambers Works Deepwater NJ 08023 USA Research Laboratory Huntingdon Life Sciences Ltd PO Box 2 Huntingdon Cambridgeshire PE18 6ES ENGLAND Report issued 5 May 1999 Page 1 of 16 ..

M .M & 414 TRADE SECRET Study Title H-24768: Developmental Toxicity Study in Rats Laboratory Project ID: DuPont-6515 DuPont-6515 T e s t G u i d e l i n e s : U.S.

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p. 1 - byo'j Journal o f Toxicology: C linical Toxicology Jan 1996 v34 n l p 2 1 ( 4 ) Page 1_________________________________________________________________ Pulmonary toxicity following exposure to an aerosolized leather protector. by Keith K.

October 31, 2006 Charles M.

Andrea V.

A t ^ 3-6 "McCrea, Deborah" <mccrea@taftlaw.com> 06/12/2009 03:54 PM To NCIC OPPT@EPA cc "Bilott, Robert A."

P-1 "McCrea, Deborah" < m ccrea@ taftlaw .com > 12/14/2009 03:38 PM To NCIC O PPT@ EPA cc "Bilott, Robert A." < bilott@taftlaw.com> bcc Subject 12/14/2009 Letter To EPA Docket Center f i / L Z I G ' 3> 9 x l Taft/ Deborah McCrea / Legal Assistant Taft Stettinius & Hollister LLP 425 Walnut Street, Suite 1800 Cincinnati, Ohio 45202-3957 Tel: 513.381.2838 Fax: 513.381.0205 www.taftlaw.com / mccrea@taftlaw.com Internal Revenue Service Circular 230 Disclosure: As provided for in Treasury regulations, advice (if any) relating to federal taxes that is contained in this communication (including attachments) is not intended or written to be used, and cannot be used, for the purpose of (1) avoiding penalties under the Internal Revenue Code or (2) promoting, marketing or recommending to another party any transaction or matter addressed herein.

INTERIM REPORT #3 - Analysis of Fish and Clam Samples STUDY TITLE Analysis of Perfluorobutanesulfonate (PFBS), Perfluorohexanesulfonate (PFHS), and Perfluorooctanesulfonate (PFOS) in Water, Soil, Sediment, Fish, and Clams Using LC/MS/MS for the 3M Decatur Monitoring Program DATA REQUIREMENTS EPA TSCA Good Laboratory Practice Standards 40 CFR 792 STUDY DIRECTOR Jaisimha Kesari P.E., DEE Weston Solutions, Inc. 1400 Weston Way West Chester, PA 19380 Phone: 610-701-3761 INTERIM REPORT COMPLETION DATE June 17, 2008 TESTING FACILITY MPI Research, Inc. 3058 Research Drive State College, PA 16801 Phone: 814-272-1039 STUDY SPONSOR 3M Company 3M Building 0236-01-B-10 St.

STL Burlington Colchester, Vermont Sample Data Summary Package SDG: 117591 STLS E V E R N TRENT November 30, 2006 Mr.

fifL - o 6 9 *> ACUTE TOXICITY TO FISH (FATHEAD MINNOW) TEST SUBSTANCE_____________________ Identity: A mixture containing perfluorooctanesulfonate, which may also be referred to as PFOS, FC-95 or as a component of FC-201AF. (1Octanesulfonic acid) (CAS # 2795-39-3).

A R a a 6 -c r?

AR&9.6 _ OSOO m ACTIVATED SLUDGE RESPIRATION INHIBITION TEST TEST SUBSTANCE________________________________________________ Identity: A mixture containing perfluorooctanesulfonate, which may also be referred to as PFOS, FC-95, or as a component of FC-206A. (1Octanesulfonic acid) (CAS # 2795-39-3).

A R .& & 6 _ O S O H - A C U T E T O X IC IT Y TO F IS H (M U M M IC H O G ) T E S T S U B S T A N C E ____________________________________________________ Id en tity: A mixture containing perfluorooctanesulfonate; m ay also be referred to as P F O S , FC-95, or as a com ponent of FC-206C and 81-2/8. (1-O ctanesulfonicadd, 1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-heptadecafluoro-, potassium salt, C A S # 2795-39-3) R em arks: The 3M production lot number w as not noted.