Material Tested: Material Submitted by AR226-2748 Copies to: E.

-I AR226-2762 Zm I* du Font da Honours and Coopany Haslcoll Laboratory for Toxicology and Industrial Medicine E lk to s Road, Hswsrk, Delaware 19711 HASKELL LABORATORY REPORT MO. 205-81 Material Tested ' Octanole add, pentadecafluoro-, ammonium salt* ' Haskell Ho." 12,037 Study Initiatsd/CosplsEed 2718/80' - 5>23>80--- Material Submitted bv W BSBBFl-------- Polymer Products Department Washington Works sobacpteIIHHALATIOH TOXICITY OF PgWTADECArLDOROOCTAHOIC ACID.

AR226-3039 Study Title Approximate Lethal Dose (ALD) of H-2I460 in Rats Laboratory Project ID Haskell Laboratory Report No. 176-96 Author Tracy A.

AR226-3337 Migration QtAgEQ frQjn^IFE It was decided to develop a new method of extraction of APFO from PTFE samples (extraction during 8 h at reflux with 9 5 % ethanol at pH - 10 on finely ground material) as well as a new method of detection of APFO using capillary gas chromatography.

Z 6T 000 et b r i ' W W CONFIDENTIAL MEMO TO: F, E.

000133 o jo -fit ~ 9 M W M am '*, ) BIOANALYTICAL REPORT Title: Date: Authors: Quantitative Determination o f Ammonium Perfluorooctanoate (APFO), M easured as the Perfluorooctanoate Anion (PFOA), in Human Serum from Study DW04 Using Turbo Ion Spray LC/MS/MS 30 September 2003 David J.

MiZG ~ ^ 7 7 * TSCA NC1C Notification Form for CBI Documents Docket Number: ^ ~ k (o _______ Document Control Number: ^ o (g o o o o o o 3 Document Date: Document Type: i> oc^ r ^ _______________ &fcL at f> IT-} C ~i O -v* KQi'X> o ?

P-1 A -fL A . $ 6 2 7 INTERIM REPORT #23 Aaaivsis of Sediment Samples STUDY TITLE Analysis o f Perfluorooctanoic Acid (PFOA) in Water, Soil, Sediment, Fish, Clams, Vegetation, Small Mammal Liver and Small Mammal Serum Using LC/MS/MS for the 3M Decatur Monitoring Program DATA REQUIREMENTS EPA TSCA Good Laboratory Practice Standards 40 CFR 792 STUDY DIRECTOR Jaisimha Kesari P.E., DEE Weston Solutions, Inc. 1400 Weston Way West Chester, PA 19380 Phone: 610-701-3761 INTERIM REPORT COMPLETION DATE May 2,2006 PERFORMING LABORATORY Exygen Research 3058 Research Drive State College, PA 16801 Phone: 814-272-1039 STUDY SPONSOR 3M Company 3M Building 0236-01-B-10 St.

Andrea V.

FINAL STUDY TITLE Ammonium Perfluorooctanoate: Phase II.

April 1,2008 Water D epartment 167 M a w STREEt * SAYREVILLE, N .J. 08872 Tel. (732) 390-7060 Fax (732) 238-2147 State o f New Jersey Department of Environmental Protection Bureau of Safe Drinking Water P.O.

"McCrea, Deborah" <mccrea@taftlaw.com> 10/05/2010 11:39 AM AlZcr3<l4% P-1 To NCIC OPPT@EPA cc "Bilott, Robert A."

INTERIM REPORT #3 - Analysis of Fish and Clam Samples STUDY TITLE Analysis of Perfluorobutanesulfonate (PFBS), Perfluorohexanesulfonate (PFHS), and Perfluorooctanesulfonate (PFOS) in Water, Soil, Sediment, Fish, and Clams Using LC/MS/MS for the 3M Decatur Monitoring Program DATA REQUIREMENTS EPA TSCA Good Laboratory Practice Standards 40 CFR 792 STUDY DIRECTOR Jaisimha Kesari P.E., DEE Weston Solutions, Inc. 1400 Weston Way West Chester, PA 19380 Phone: 610-701-3761 INTERIM REPORT COMPLETION DATE June 17, 2008 TESTING FACILITY MPI Research, Inc. 3058 Research Drive State College, PA 16801 Phone: 814-272-1039 STUDY SPONSOR 3M Company 3M Building 0236-01-B-10 St.

SEVERN TRENT STL STL Chicago 2417 ond Street University Park, IL 60466 Tel: 70S 534 5200 Fax: 70S 534 5211 www.stl-inc.com SEVERN TRENT LABORATORIES ANALYTICAL REPORT JOB -NUMBER:- 244402'"' ' P r e p a r e d 'F o r : W e sto n Solutions.,...

& & S .6 - o e r if PFOS Pharmacokinetic - 000186 Corning Hazleton Inc.