AR226-2853 Material ted Copies to: E I. du Font de Nemours and Company Haskell Labi .atory for Toxicology and Industrial Medicine HASKELL LABORATORY REPORT NO. 960-76 MR Haskell No.

AR226-3330 Copy No.

* .

ACTIVATED SLUDGE RESPIRATION INHIBITION TEST * -z' TEST SUBSTANCE Identity: Periluorooctanesulfonate, DEA salt; may also be referred to as PFOS DEA salt, FC-99, or 3M Sample No. 2. (1-Octanesulfonic acid, 1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-heptadecafluoro-, compd. with 2,2'-iminobis[ethanol] (1:1), CAS # 70225-14-8) Remarks: Test sample is a mixture of the test substance in water (approximately 25% test substance and 75% water).

BACK TO MAIN Centre Analytical Laboratories, Inc. 3048 Research Drive State College, PA 16801 www.centrelab.com ^P hone: (814) 231-8032 Fax: (814) 231-1253 or (814) 231-1580 Analytical Report Fluorochemical Characterization of Drinking Water Samples Cleveland, Tennessee (W1973) Centre Analytical Laboratory Report No. 023-007A (Revision 1) Revision Date 3/19/01 Testing Laboratory Centre Analytical Laboratory, Inc. 3048 Research Drive State College, PA 16801 3M Environmental Laboratory Contact Kent R.

flR f i - O IM I A International Research and Development Corporation SPONSOR: COMPOUND: SUBJECT: 3M Company Fluorad Fluorochemical FC-143 Ninety Day Subacute Rat Toxicity Study.

m form 0747 & y I'f.

Aim G-O O & S Centre Analytical Laboratories, Inc. 3048 Research Drive Phone: (814) 231-8032 State College, PA 16801 Fax: (814) 231-1253 or (814) 231-1580 Analytical Report Fluorochemical Characterization of Drinking Water Samples Decatur, Alabama (W1979) Centre Analytical Laboratory Report No. 023-007B Testing Laboratory Centre Analytical Laboratory, Inc. 3048 Research Drive State College, PA 16801 3M Environmental Laboratory Contact Kent R.

BACK TO MAIN Centre Analytical Laboratories, Inc. 3048 Research Drive State College, PA 16801 www.centrelab.com ^P h on e : (814)231 -8032 Fax: (814) 231 -1253or (814) 231 -1580 Analytical Report Fluorochemical Characterization of POTW Effluent Cleveland, Tennessee (W1973) Centre Analytical Laboratory Report No. 023-0141 (Revision 1) Revision Date 3/26/01 Testing Laboratory Centre Analytical Laboratory, Inc. 3048 Research Drive State College, PA 16801 3M Environmental Laboratory Contact Kent R.

Ak 2.6 - Q Z $ 0 ACUTE TOXICITY TO AQUATIC INVERTABRATES (DAPHNIA MAGNA) TEST SUBSTANCE____________________________________________ Identity: A mixture containing periluorooctanesulfonate, which may also be referred to as PFOS, FC-95, or as a component of FC-600. (1-Octanesulfonic acid, 1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8heptadecafluoro-, potassium salt, CAS # 2795-39-3) Remarks: The 3M production lot number was not noted.

j\R l% S-0J55 28 Day Percutaneous Absorption Study with FC-95 in Albino Rabbits Experiment No.: Conducted At: Dates Conducted: Conducted By: Reviewed By: de: M.

ARllt-03G6 Attached are comments on the 3M Technical Report "Analytical Methodology and Support.

M A 2 6 - 07/6 ACUTE TOXICITY TO FISH (BLUEGILL SUNFISH) TEST SUBSTANCE____________________________________________ Identity: A mixture containing perfluorooctanesulfonate, which may also be referred to as PFOS, FC-95, or as a component of FC-203. (1Octanesulfonic acid) (CAS # 2795-39-3).

fiKSLS.6 - O Z 2 9 ACUTE TOXICITY TO AQUATIC INVERTABRATES (DAPHNIA MAGNA) TEST SUBSTANCE____________________________________________ Identity: A mixture containing periluorooctanesulfonate, which may also be referred to as PFOS, FC-95, or as a component of FC-600. (1-Octanesulfonicacid, 1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8heptadecafluoro-, potassium salt, CAS # 2795-39-3) Remarks: The 3M production lot number was not noted.

ACUTE TOXICITY TO BLUEGILL SUNFISH TEST SUBSTANCE______________________________________________ Identity: Perfluorooctanesulfonate; may also be referred to as PFOS or FC-95. (1-Octanesulfonic acid, 1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8heptadecafluoro-, potassium salt, CAS # 2795-39-3) Remarks: The test substance is a white powder (3M Lot 583) of uncharacterized purity.