RECYCLED O) o> AR226-2676 PROJECT ANNUAL C 8 SAMPLING 1991 ANNUAL C8 SAMPLING 1991 ANNUAL C8 SAMPLING 1991 ANNUAL C8 SAMPLING 1991 ANNUAL C8 SAMPLING 1994 ANNUAL C8 SAMPLING 1994 ANNUAL C8 SAMPLING 1994 ANNUAL C8 SAMPLING 1994 ANNUAL C8 SAMPLING 1994 ANNUAL C8 SAMPLING 1994 ANNUAL C8 SAMPLING 1994 ANNUAL C8 SAMPLING 1994 ANNUAL C8 SAMPLING 1994 ANNUAL C8 SAMPLING 1997 ANNUAL C8 SAMPLING 1997 ANNUAL C8 SAMPLING 1997 ANNUAL C8 SAMPLING 1997 ANNUAL C8 SAMPLING 1997 ANNUAL C8 SAMPLING 1997 ANNUAL C8 SAMPLING 1997 ANNUAL C8 SAMPLING 1997 ANNUAL C8 SAMPLING 1997 ANNUAL C8 SAMPLING 1998 ANNUAL C8 SAMPLING 1998 ANNUAL C8 SAMPLING 1998 ANNUAL C8 SAMPLING 1998 ANNUAL C8 SAMPLING 1998 ANNUAL C8 SAMPLING 1998 ANNUAL C8 SAMPLING 1998 ANNUAL C8 SAMPLING 1998 ANNUAL C8 SAMPLING 1999 ANNUAL C8 SAMPLING 1999 ANNUAL C8 SAMPLING 1999 ANNUAL C8 SAMPLING 1999 ANNUAL C8 SAMPLING 1999 ANNUAL C8 SAMPLING 1999 ANNUAL C8 SAMPLING 1999 ANNUAL C8 SAMPLING 1999 ANNUAL C8 SAMPLING 1999 ANNUAL C8 SAMPLING 1999 ANNUAL C8 SAMPLING 1999 ANNUAL C8 SAMPLING 2000 ANNUAL C8 SAMPLING 2000 ANNUAL C8 SAMPLING 2000 ANNUAL C8 SAMPLING 2000 SRCNAME LOWER POND LOWER POND UPPER POND UPPER POND LM W -2A L M W -2A L M W -5B LM W -5B LOWER POND LOWER POND STREAM MN RD STREAM MN RD UPPER POND LMW-1 LM W -2A L M W -5B LM W -7 L M W -8 LOWER POND R T 33 STREAM TRIP BLANKS UPPER POND LMW-1 LM W -2A L M W -6 LM W -7 LM W -8 LOWER POND TRIP BLANKS UPPER POND EQUIPM ENT BLANKS LEACHATE LMW-1 L M W -2A LM W -3A L M W -5B LM W -7 L M W -8 LOWER POND RT 33 STREAM UPPER POND 002(LEACHATE BASIN) FIELD BLANKS LEACHATE LMW-1 C8 results Envista 111104.xls THEME O ther liquid O ther liquid O ther liquid O ther liquid Groundwater Groundwater Groundwater Groundwater O ther liquid O ther liquid O ther liquid O ther liquid O ther liquid Groundwater Groundwater Groundwater Groundwater Groundwater O ther liquid O ther liquid Blank W ater O ther liquid Groundwater Groundwater Groundwater Groundwater Groundwater O ther liquid Blank W ater O ther liquid Blank W ater O ther liquid Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater O ther liquid Surface W ater O ther liquid O ther liquid Blank W ater O ther liquid Groundwater DATESMPL SMPLT 11/22/1991 FS 12/27/1991 FS 11/22/1991 FS 12/27/1991 FS 3/15/1994 FS 9/20/1994 FS 3/15/1994 FS 9/20/1994 FS 3/15/1994 FS 9/20/1994 FS 3/15/1994 FS 9/20/1994 FS 3/15/1994 FS 7/23/1997 FS 7/23/1997 FS 7/23/1997 FS 7/23/1997 FS 7/23/1997 FS 7/23/1997 FS 7/23/1997 FS 7/23/1997 TB 7/23/1997 FS 5/28/1998 FS 5/28/1998 FS 5/28/1998 FS 5/28/1998 FS 5/28/1998 FS 5/28/1998 FS 5/28/1998 TB 5/28/1998 FS 7/19/1999 EB 7/20/1999 FS 7/20/1999 FS 7/20/1999 FS 7/19/1999 FS 7/20/1999 FS 7/20/1999 FS 7/20/1999 FS 7/19/1999 FS 7/20/1999 FS 7/19/1999 FS 7/25/2000 FS 7/24/2000 FB 7/25/2000 FS 7/24/2000 FS LTL SAMPLE NUMBER LOWER POND LOWER POND UPPER POND UPPER POND L M W -2A L M W -2A LM W -5B LM W -5B LOWER POND LOWER POND STREAM MN RD STREAM MN RD UPPER POND W W K-LMW -1 W W K-LMW -2A W W K-LMW -5B W W K-LMW -7 W W K-LMW -8 W W K-LOW ERPOND W W K-RT 33 STREAM W W K-TRIP BLANK W W K-UPPERPOND W W K-LT-LM W 1 W W K-LT-LMW 2A W W K-LT-LMW 6 W W K-LT-LMW 7 W W K-LT-LMW 8 W W K-LOW ERPOND TRIP BLANK W W K-UPPERPOND W WK-K-EQBLK W W K-G-LT-LEACHATE W W K-G-LT-MW -1 W W K-G-LT-MW -2A W W K-G-LT-MW -3A W W K-G-LT-MW -5B W W K-G-LT-M W -7 W W K-G-LT-MW -8 W W K-W -LT-LOW ER-POND W W K-W -LT-RT-33-STREAM W W K-W -LT-UPPER-POND LTL -W -002 LTL-K-FBLK-1 LTL-L-LEACHATE LTL-G -LM W -1 Page 1 oeoei!

3 Final Report Study Title Anaerobic Biodegradability Testing of the Perfluoroalkyl Substances PFOS, PFBS, PFOA, PFBA, MeFBSE, EtFOSE, 6:2-FTS, 6:2 FTOH and 8:2 FTOH, and also 246-Trichlorophenol and Pentachlorophenol Data Requirement Exploratory/Method Development Author Cleston C.

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o Safety &n Health Research Laboratories SPONSOR Avenue E. vAanPNMiEewenhuyse, 4 B-11B60OXBru3ssels Belgium AR226-1803 AMMONIUM PERTFELSUTORITOEOMCTANOATE (APFO) EARLY-LIFE STAGE TSOXTIUCDIYTTYITTELEST IN RAINBOW TROUT UNDER FLOW-THROUGH CONDITIONS DATA REQUIREMENT OECD Guideline No. 210, 17th July 1992 STJUacDqYueDsIL'RHEarCidToOn R [EXPERIMENTAL COMPLETIONDATE 7 August 2003 DCAaTE lOFyISS2U0E k TEST FcArCILITY BP 563 -27005 Evreus - France LABORATORY 226S39TEUCDPY NUMBER Page 10f 112, 1SSNMCmRaeCcTohaprnche 4a40?

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BACK TO MAIN SUMMARY OF ANALYTICAL RESULTS: MULTI-CITY FOOD STUDY The Multi-City Study was originally designed by Battelle Memorial Institute (Columbus, OH), to obtain preliminary data about the presence of fluorochemicals in foods and in drinking water to understand the potential sources of human exposure.

BACK TO MAIN SUMMARY OF ANALYTICAL RESULTS: MULTI-CITY FOOD STUDY The Multi-City Study was originally designed by Battelle Memorial Institute (Columbus, OH), to obtain preliminary data about the presence of fluorochemicals in foods and in drinking water to understand the potential sources of human exposure.

ANNEX III References [1] Henry, B.

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3M Medical Department Study: T-6295.12 Analytical Report: FACTTOX-110 LRN-U2849 Table 7: Ambient-Temperature Stability of PFOS in Rat Serum After 24 Hours Run 11 QC (Theoretical Cone.)

Bestimmung von summarisch erfassbaren organisch gebundenen Halogenen in wssrigen Umweltproben mittels Hochtemperaturverbrennung und ionenchromatographischer Analyse (CIC) - Vergleich mit der LC-MS/MS-Einzelstoffanalytik unter Bercksichtigung von per- und polyfluorierten Alkylsubstanzen (PFAS) Determination of summarized organically bound halogens in environmental water samples using combustion ion chromatography (CIC) - Comparison to LC-MS/MS analysis of individual per- and polyfluorinated alkylcompounds (PFAS) Dissertation zur Erlangung des akademischen Grades doctor rerum naturalium (Dr. rer. nat.) im Fachbereich 08 - Biologie und Chemie der Justus-Liebig-Universitt Gieen durchgefhrt im Landesbetrieb Hessisches Landeslabor Abteilung IV - Landwirtschaft und Umwelt Fachgebiet IV.2 - Organische Kontaminanten und Umweltanalytik vorgelegt von Eleonora von Abercron (geb.

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