Report E01-1245 PFOS: A Reproduction Study with the Nothern Bobwhite Study Title A nalytical Phase Report for PFOS: A Reproduction Study with T he Northern Bobwhite Data Requirement FIFRA Subdivision E, Section 71-4 OECD Guideline 206 Author Lisa A.

3M FLUOROCHEMICAL SUBMISSIONS February, 2002 - May, 2004 INDEX OF 3M'S 2002-2004 AR-226 DOCKET SUBMISSIONS BY DATE Back to Menu July 2003 Click on Study Title to View Report July 9, 2003 Page 1, 2 July 9, 2003 Submission Cover Letter Final Report, NIOSH Health Hazard Evaluation for Perfluorooctanoic Acid and Perfluorooctane Sulfonate, NIOSH HETA 20010235, July 31, 2001.

3M Specialty Materials 3M Center St.

SRPT T - 7 ^ ( / MIN 314/022208 PERFLUOROOCTANESULFONYL FLUOORRIDE (POSF) BACTERIAL REVERSE MUTATION TEST Sponsor 3M Center 3M Corporate Toxicology Building 220-2E-02 St Paul MN 55133-3220 USA T IP " Research Laboratory Huntingdon Life Sciences Ltd.

905 Sheehy Drive, fiUg.

BACK TO MAIN 3M FLUOROCHEMICAL SUBMISSION TOXICOLOGY, EPIDEMIOLOGY AND MEDICAL SURVEILLANCE May 2000 - October 2005 Click on Study Title to View Report PFOA Perfluorooctanoate Page 1, 2 1.

ACUTE TOXICITY TO FISH TEST SUBSTANCE Identity: Perfluorooctanoic acid; may also be referred to as PFOA, FC26, or FX-1001.

7 Mark H Russel!

A&3J6- I f S t PFOS: A DIETARY LC50 STUDY WITH THE MALLARD WILDLIFE INTERNATIONAL LTD.

Report E01-1256 PFOS: A Reproduction Study with the Mallard Study Title Analytical Phase R eport for PFOS: A Repro ductio n Stu d y w ith the Mallard Data Requirement FIFRA Subdivision E, Section 71-4 OECD Guideline 206 Author Lisa A.

26 November 2004 AR226-1889 To: Mary F.

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AR226-2024 XHTKHQFFICK HEM01 Bate: .

AR226-2122 file:///C|/WINDOWS/TEMP/C-8-FC-143 SP 9-2-81 in n i 3-8-VZ.fttm 't Test Results Sam ple Date R ange C oncentration R ange Action te v e l Industrial Hygiene 9/2/81 3/8/92 100% Sam ple Dt S am ple# ' D uration Type Employee Name Pere BTO: 08 TEFLON@ tO C : 704 AIS - FINE POWDER C-B WEIGH HOOD 4/29/87 34976 331 S Chemical Cone Unit P ercen t C-8/FC-143 0.148 MPB 26.4% BTO : tO C : 08 TEFLON@ 706 FINE POWDER DRYER #3 3/18/91 43734 390 S 3/18/91 43735 390 S 3/18/91 43736 3/18/91 43737 390 S 390 S 3/22/91 43738 390 S 3/22/91 43739 3/22/91 43740 390 S 390 S 3/22/91 43741 3/22/91 43742 3/22/91 43743 3/22/91 43744 390 S 390 S 390 s 390 s BTO : 08 TEFLON@ C-8/FC-143 >6.0 MPB 1071.4% C-8/FC-143 >6.0 MPB 1071.4% C-8/FC-143 0.152 MPB 27.1% C-8/FC-143 >6.0 MPB 1071.4% C-8/FC-143 >6.0 MPB 1071.4% C-8/FC-143 1,693 MPB 302.3% C-8/FC-143 >6.0 MPB 1071.4% C-8/FC-143 0.097 MPB 17.3% C-8/FC-143 0.187 MPB 33.4% C-8/FC-143 0.79 MPB 141.1% C-8/FC-143 0.134 MPB 23.9% A1P006220 8/9/2001 5:02 PM E ID 139462 TestRssults LOG: 720 INJECTION PUMP AREA 4/29/87 39691 330 S 3/8/92 44892 430 S file:WC1WIND0WS/TEMP/O8-FC-143 SP 9-2-81 thru 3-8-92.htm C-8/FC-143 0.279 MPB 49.8% C-8/FC-143 0.34 MPB 60.7% BTO : LOG ; 08 TEFLON 728 WAX ROOM -B -1 6 2 -1ST FLOOR 1/28/90 42843 480 S C-8/FC-143 >4.0 MPB 714.3% " BTO : 18 TEFLON COPOLYMERS LOG : 297 SPECIAL FEP SAMPLES 9/2/81 61628 S 9/2/81 61629 S 0/2/81 61630 9/3/81 61631 9/3/81 61632 9/3/81 61633 S s s s Thursday, August 09,2001 1:57:10 PM C-8/FC-143 0.11 MPB 19.6% C-8/FC-143 0.04 MPB 7.1% C-6/FC-143 0.22 MPB 39.3% C-8/FC-143 0.92 MPB 164.3% C-8/FC-143 0.37 MPB 66.1% C-8/FC-143 0.33 MPB 58,9% Page 1 of 2 2 of 4 Sam ple Dt Sam ple # Duration Type Employee Name 12/15/81 61634 S 12/15/81 61635 12/15/81 61636 S s * 12/15/81 61637 S Pars chem ical C-B/FC-143 C-8/FO-143 C-8/FC-143 C-8/FC-143 Cone Unit P ercent 0.03 MPB 0.03 MPB 0.04 MPB 0.04 MPB 5.4% 5.4% 7.1% 7.1% >4 ooOKnN> tHo-1 8/9/2001 5:02 PM EID 139463 TestResults / 12/15/81 61638 12/15/81 61639 12/15/81 61640 12/15/81 61641 12/15/81 61642 12/15/81 61643 12/15/81 61644 12/15/81 61645 12/16/81 61646 12/16/81 61647 12/16/81 61648 12/16/81 61649 12/16/81 61650 12/16/81 61651 12/16/81 61652 12/16/81 61653 12/16/81 61654 12/16/81 61655 12/16/81 61656 12/16/61 61657 S s s s s s s s s s s s s 's s s s s s s BTO: 18 TEFLON COPOLYMERS LOC: 299 #1 OVEN EXHAUST 9/28/81 61612 s 3 of4 file:///C|/W INDOW S/TEM P/C-8-FC-143 SP 9-2-81 thru3-8-92.htm C-8/FC-143 0.03 MPB 5,4% C-8/FC-143 0.03 MPB 5.4% C-B/FC-143 0.07 MPB 12.5% C-8/FC-143 0.03 MPB 5.4% C-B/FC-143 0.22 MPB 39.3% C-8/FC-143 0.04 MPB 7.1% C-8/FC-143 0.04 MPB 7.1% C-B/FC-143 0.04 MPB 7.1% C-8/FC-143 0,33 MPB 58.9% C-8/FC-143 0.07 MPB 12.5% C-8/FC-143 C-B/FC-143 0.15 MPB 0.07 MPB 26.8% 12.5% C-B/FC-143 0.04 MPB 7.1% C-8/FC-143 0.04 MPB 7.1% C-8/FC-143 0.48 MPB 85.7% C-B/FC-143 0.04 MPB 7.1% C-8/FC-143 0.07 MPB 12.5% C-6/FC-143 0.15 MPB 26.8% C-8/FC-143 0.63 MPB 112.5% ** C-8/FC-143 0.29 MPB 51.8% AJP0Q6222 C-8/FC-143 4.9 MPB 875.0% ** 8/9/2001 5:02 PM EID 139464 ^TestRcswlts VssMf 9/29/81 61613 S .

Tesffi.esuks ,, ; * % AR226-2129 file:///C|AVINDOWS/TEMP/RD C -81-3-79 thiu 4-30-811 pageitm 10f 2 T est R esu lts Sample Dale Range Concentration Range Action Level Industrial Hygiene 1/3/79 100% 4/30/81 Sample Dt Semple # Duration Type Employee Name Per* BTO : LOC : 17 RESEARCH 019 WEIGH AND ADD 0 8 TO POLYKETTLE 1/3779 47531 Z 1/4/79 47S32 Z Chemical Cone Unit Percent 0 8 <0.05 PPM 0.0% 0 8 <0.05 PPM 0.0% BTO : LOC : 17 RESEARCH 065 PPD SEM IW O RKS 4/6/81 57356 Z 0 8 <0.0001 PPM 0.0% BTO: LOC : 17 RESEARCH 100 P/S - EPM W AREHOUSE - FORK TRUCK OPERATION 4/30/81 60221 Z 0 8 0.0001 PPM 0.0% BTO: LOC : 17 RESEARCH 103 P/S FP POLLYKETTLE OPERATOR (17LG) 1/19/79 48192 Z 1/26/79 48193 Z 11/11/80 31069 P none 11/12/80 31070 P none 11/15/80 31071 P none 11/17/80 31072 P none 11/18/80 31073 P none 0 8 0.05 PPM 0.0% C-8 <0.01 PPM 0.0% C-8 <0.0001 PPM 0.0% 0 8 0.0005 PPM 0.0% 0 8 0.0005 PPM 0.0% 0 8 <0.0001 PPM 0.0% 0 8 <0.0001 PPM 8/28/2001 5:07PM E ID 129294 AJP0G6927 */ Test&?