PERFLUOROOCTANESULFONATE, POTASSIUM SALT (PFOS): A 96-HOUR STATIC-RENEWAL ACUTE TOXICITY TEST WITH THE SHEEPSHEAD MINNOW (Cyprinodon variegatus) FINAL REPORT WILDLIFE INTERNATIONAL, LTD.

S A N IT IZ E D AR jU -co3 $ i REPORT EXPLORATORY 28-DAY ORAL TOXICITY STUDY WITH TELOMER ALCOHOL, TELOMER ACRYLATE PFHS AND PFOS (positive control) BY DAILY GAVAGE IN THE RAT FOLLOWED BY A 14/28-DAY RECOVERY PERIOD NOTOX Project 242933 NOTOX Substances 83484, 83493, 83502, 84456 and 84141 3M Test No.

62# 3M General Offices f> 7 - 0500 1313M Center St.

^ 226- 02/6 Attachments to Letter to C.

C O RN IN G Hazleton MUTAGENICITY TEST ON ; IN AN /A VIVO MOUSE MICRONUCLEUS ASSAY FINAL REPORT AUTHOR Hemalatha Murli, Ph.D.

IN VITRO MICROBIOLOGICAL MUTAGENICITY ASSAYS OF 3M COMPANY'S COMPOUND T-3610 Final Report September 1984 By: / O j u ^ i i L L Debra E.

ACUTE TOXICITY TO FISH TEST SUBSTANCE Identity: Perfluorodecanesulfonate, ammonium salt; may also be referred to as PFDS, FC-121-X, or3M Sample E2112and E2566-1. (1Decanesulfonic acid, 1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heneicosafluoro-, ammonium salt, CAS # 67906-42-7) Remarks: Test sample is a mixture of the test substance in water and 2propanol, 1-(1,1-dimethylethoxy).

A(U2rO51% PFOA and Associated Salts Ecotoxicity Elements Title Activated Sludge R espiration Inhibition T es t - F C -1 0 1 5 -X Acute Toxicity o f F C -1 01 5 to the Fathead Minnow, Pim ephales prom elas Growth and Reproduction Toxicity Test with F C -1 01 5 and the Freshw ater Alga, Selenastrum capricornutum Acute Toxicity o f F C -1 0 1 5 to the Daphnd, D aphnia m agna Laboratory or Author 3M Env.

3M ENVIRONMENTAL LABORATORY REPORT NO.

Precise Research.

INTERIM REPORT # 8 - Analysis of Sediment Samples STUDY TITLE Analysis of Perfluorobutanesulfonate (PFBS), Perfluorohexanesulfonate (PFHS), and Perfluorooctanesulfonate (PFOS) in Water, Soil, Sediment, Fish, Clams, Vegetation, Small Mammal Liver and Small Mammal Serum Using LC/MS/MS for the 3M Decatur Monitoring Program DATA REQUIREMENTS EPA TSCA Good Laboratory Practice Standards 40 CFR 792 STUDY DIRECTOR Jaisimha Kesari P.E., DEE Weston Solutions, Inc. 1400 Weston Way West Chester, PA 19380 ' Phone: 610-701-3761 INTERIM REPORT COMPLETION DATE 07/13/06 PERFORMING LABORATORY Exygen Research 3058 Research Drive State College, PA 16801 Phone: 814-272-1039 STUDY SPONSOR 3M Company 3M Building 0236-01-B-10 St.

SEVERN TRENT LABORATORIES ANALYTICAL REPORT JOB NUMBER: 245986 Prepared For: Weston Solutions, Inc. 1400 Weston Way Building 5-2 West Chester, PA 19380-1499 Project: Confidential Decatur - FC Investigation Attention: Jai Kesari Date: 05/05/2006 Signature Name: Richard C.

BIODEGRADATION A R22-0057 FT--3 TEST SUBSTANCE_______________________________________________ Identity: Periluorooctanesulfonate; may also be referred to as PFOS or FC-95. (1-Octanesulfonic acid, 1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8heptadecafluoro-, potassium salt, CAS # 2795-39-3) Rem arks field: The test substance is a white powder of uncharacterized purity.

A W # - a -if ACTIVATED SLUDGE RESPIRATION INHIBITION TEST TEST SUBSTANCE Identity: Perfluorooctanesulfonate, Lithium salt; may also be referred to as PFOS Li salt, FC-94, or FC-94-X. (1-Octanesulfonic acid, 1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-heptadecafluoro-, lithium salt, CAS #29457-72-5) Remarks: The test sample is a mixture of the test substance in water (approximately 24.5% test substance and 75.5% water).

AP STUDY SUMMARY FOR W ORK PERFORMED DURING 1977-1979 TEST SUBSTANCE_____________________________________ Identity: Perfluorooctanesulfonate; may also be referred to as PFOS or FC-95. (1-Octanesulfonicacid, 1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8heptadecafluoro-, potassium salt, CAS # 2795-39-3) Rem arks field: The test substance is a white powder of uncharacterized purity.