INTERIM REPORT #26 - Analysis of Groundwater Samples STUDY TITLE Analysis of Perfluorobutanesulfonate (PFBS), Perfluorohexanesulfonate (PFHS), and Perfluorooctanesulfonate (PFOS) in Water, Soil, Sediment, Fish, Clams, Vegetation, Small Mammal Liver and Small Mammal Serum Using LC/MS/MS for the 3M Decatur Monitoring Program DATA REQUIREMENTS EPA TSCA Good Laboratory Practice Standards 40 CFR 792 STUDY DIRECTOR Jaisimha Kesari P.E., DEE Weston Solutions, Inc. 1400 Weston Way West Chester, PA 19380 Phone: 610-701-3761 INTERIM REPORT COMPLETION DATE January 9, 2007 PERFORMING LABORATORY Exygen Research 3058 Research Drive State College, PA 16801 Phone: 814-272-1039 STUDY SPONSOR 3M Company 3M Building 0236-01-B-10 St.

M zz - 07S3 BIODEGRADATION (BOD/COD) TEST SUBSTANCE____________________________________________ Identity: Mixture containing perfluorooctanesulfonate, which may also be referred to as PFOS, FC-95, or as a component of FC-203CF-X or FC-203CF. (1-Octanesulfonic acid) (CAS # 2795-39-3).

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ARA.G _ 0 0 5 ACUTE TOXICITY TO FISH (FATHEAD MINNOW) TEST SUBSTANCE Identity: A mixture containing perfluorooctanesulfonate, may also be referred to as PFOS, FC-95, or as a component of FC-3072. (1Octanesulfonic acid) (CAS # 2795-39-3).

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3M ENVIRONMENTAL LABORATORY REPORT NO.

3M ENVIRONMENTAL LABORATORY REPORT NO.

3 Environmental Laboratory E05-0210 Interim Report#15 Interim Report #15: Analysis of Water Samples from Northern Alabama Potable Water Systems Study Title Analysis of Perfluorobutanesulfonate (PFBS), Perfluorohexanesulfonate (PFHS), and Perfluorooctanesulfonate (PFOS) in Water, Soil, Sediment, Fish, Clams, Vegetation, Small Mammal Liver and Small Mammal Serum Using LC/MS/MS for the 3M Decatur Monitoring Program Data Requirement EPA TSCA Good Laboratory Practice Standards 40 CFR 792 Author Michelle D.

EOS-0210 Interim Report #18 Northern Alabama Potable Witter Systems, December 2005 Interim Report #18: Analysis of Water Samples from Northern Alabama Potable Water Systems, December 2005 Study Title A nalysis of Perfluo robutanesulfonate (PFBS), Perfluorohexanesulfonate (PFHS), an d Perfluorooctanesulfonate (PFOS) in Wate r , So il, S edim ent, Fis h , Clam s, V eg etatio n , Sm all Mam m al Liver an d Sm all Mam m al S erum Using LC/MS/MS FOR THE 3M DECATUR MONITORING PROGRAM Data Requirement EPA TSCA Good Laboratory Practice Standards 40 CFR 792 Author M ichelle D.

A R 1 U -0 1 5 I Laboratory Report Interim Report of Preliminary Data for 26 Week Capsule Toxicology Study with PFOS in Cynomolgus Monkeys Laboratory Report No.

HAZLETON WASHINGTON 9 2 0 0 LE E S B U R G PIKE V I E N N A .

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ARa%-03l8 REPORT EVALUATION OF THE ABILITY OF T-5869 TO INDUCE CHROMOSOME ABERRATIONS IN CULTURED PERIPHERAL HUMAN LYMPHOCYTES (WITH INDEPENDENT REPEAT) NOTOX Project 115943 NOTOX Substance 38196 - page l of 26 - Rfc-C&VED NOV - 9 1994 T"C/a O t--'O Oi \ 005605 T -5869 STATEMENT OF GLP COMPLIANCE NOTOX Project 115943 NOTOX B.V., 's-Hertogenbosch, The Netherlands The study described in this report was conducted in compliance with the most recent edition of: The OECD Principles of Good Laboratory Practice which are essentially in conformity with: The United States Food and Drug Administration.

* T -H *)g o 28 Day Percutaneous Absorption Study with FC-98 in Albino Rabbits 'r e c ' AL.- f i W t \\ ~\0 X.I ' L LtX ' Experiment No Conducted At: Dates Conducted: Conducted By: 0979AB0630 Safety Evaluation Laboratory Riker Laboratories, Inc.

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