Quality Assurance Project Plan Multi-City Study Sampling Task (NJ00666) BACK TO MAIN Revision No. : 1 Effective Date: M ay 14, 1999 Page i o f iv Quality Assurance Project Plan for Empirical Human Exposure Assessment Multi-City Study Sampling Task To May 14,1999 Prepared by Battelle 397 Washington Street Duxbury, MA 02332 (781) 934-0571 APPROVALS Sampling Task Leader Rosanna Buhl Battelle Sampling Task QA Officer __f l / ; JtjJy/,ATJl& Marcia Nishioka * Battelle Project Manager Susan bbgy Battelle Program QA Officer Date Date q n /n Date s litto Date Date Quality Assurance Project Plan Multi-City Study Sampling Task (N100666) Joseph Fiksel Marcia Nishioka Suan Abbgy Donald Gunster Rosanna Buhl Wayne Trulli Scott Macomber Chris Gagnon Kelly Irizarry Robert Mandeville Richard Restucci Kim Andrews Distribution List BACK TO MAIN Revision No.: 1 Effective Date: May 14, 1999 Page ii o f v BACK TO MAIN Quality Assurance Project Plan Multi-City Study Sampling Task (N100666) Revision No.: 1 Effective Date: May 14, 1999 Page iii o f v CONTENTS 1.

BACK TO MAIN MELTING POINT TEST SUBSTANCE Identity: Decafluoro(pentafluoroethyl)cyclohexanesulfonate, DEA salt; may be referred to as CS-2070.

BACK TO MAIN STABILITY IN WATER (HYDROLYSIS) TEST SUBSTANCE__________________ Identity: N-methylperfluorooctane sulfonamidoethanol; may also be referred to as 2(N-Methylperfluoroctanesulfonamido)-ethyl alcohol, N-MeFOSE Alcohol, FC-790, or FM-3925. (1-Octanesulfonamide, N-methyl1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-heptadecafluoro-N-(2-hydroxyethyl)-, CAS # 24448-09-7).

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BACK TO MAIN Im p in g er Studies o f V o la tility o f FC -95 and FC -143 Intoduction and Purpose: Thermospray mass spectrometry was used to quantitate a number of samples for FC-143 and FC-95.

BACK TO MAIN 3M Environmental Laboratory Report No.

A R 023-00 7^ LaboratoiyReport Analysis of Fluorochemicals in Wild Bird Livers Laboratoiy Report No.

i / )R O X -O I3 3 C O R N IN G Hazleton MUTAGENICITY TEST ON / T-6357 \^ \A IN AN IN VIVO MOUSE MICRONUCLEUS ASSAY FINAL REPORT AUTHOR Hemalatha Murli, Ph.D.

m -OSTOO - /3 7/f Attachments to Letter to C.

3M General Offices 3M Center St.

AR0U'OM3 C O R N IN G Hazleton MUTAGENICITY TEST WITH // ^ '< A \ T-6342 i \* IN THE SALMONELLA - ESCHERICHIA COI//MAMMALIAN-MICRSOME REVERSE MUTATION ASSAY ir-- - ^ FINAL REPORT AUTHOR Timothy E.

/IRlK-O%& 3M MEDICAL DEPARTMENT TOXICOLOGY SERVICES To: Geoijean Adams 290-4-01 cc: John ButenhofF 220-2E-02 From: Marv Case 220-2E-02 Subject: FC 95 and 143 Teratology Date: 26 May 1998 John passed on to me your request for someone to review and write an analysis on the eye lens defect that was reported in the original FC 95 rat teratology study.

A R m - 0 H6f| Attachments to Letter to C.

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3M General Offices \W ^ 3M February 5, 1999 5\1 Center SH& - 02.ee. 373Si.