Document 82nGLpaemY9qqwb2Om9vkVJVB
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BIODEGRADATION (BOD/CODfTOC)
TEST SUBSTANCE
Identity: Perfluorooctanesulfonylamido(ethyl)acetate; may also be referred to as PFOSAA, FC-128 or as the major component of FC-127 or FC-129. (Glycine, N-ethyl-N[(heptadecafluorooctyl)sulfonyl]-, potassium salt, CAS # 299151-7)
Rem arks: The test sample is FC-128. Current information indicates it is a mixture of 86% test substance and 14% C4-C7fluoroalkyl carboxylate compounds. 3M production lot number 751.
METHOD:
Method: Not noted. Type: Aerobic GLP: No Year completed: 1977 Contact time: NA Innoculum: Not noted
RESULTS
BOD20: COD: TOC:
<7600 mg/kg 140,000 mg/kg 162,000 mg/kg
Remarks: The 5-, 7-, 11-, and 14-day BOD values could not be calculated because of insufficient dissolved oxygen depletion.
CONCLUSIONS
No reliable conclusions can be derived from this study.
Subm itter: 3M Company, Environmental Laboratory, P.O. Box 33331, St. Paul, Minnesota, 55133
DATA QUALITY
Reliability: Klimisch ranking 4. Summary was created using only a listing of test values. The original study procedure and raw data were not found.
REFERENCES
000326
The COD and BOD studies were conducted by the 3M Company, Environmental Laboratory, St. Paul, MN, Lab Request number 3844, 7/8/77. The TOC study was conducted by ARRO Laboratories at the request of 3M, Lab Request number 3849, 1977 OTHER Last changed: 5/16/00
000327
F o rm IOeaO-5-PtyO cc: LA B RjEQUEST BOOK - 42-5W
Ref: ENVJR. ASSESS. INQ. #_ ^PRO DUCT:
PRODUCT ECOLOGICAL ASSESSMENT REQUEST FOR LABORATORY WORK
DIVISION
LAB REQUEST NO
3KJ3 'Action'00 Paper
REQUESTER
Name -L2gJk Request Date: ~?/ <r'/ J 7
Project N o.~ /
Code N o.:
____________
Sample D ate:__________________
Phone No. Prob. N o .. Date Needed:
Description: Purpose o f Tests:
S ~ > 3
f 'fit j'W CC
PHYSICAL & CHEMICAL PROPERTIES Heat of C om bustion Cal/G (B T U /L b .)
D ensity Ash O ther
*0 V r '
LABORATORY
Date Received Sample:. A n a ly s t:____________ Date Completed:. Hours S pent:___ Y ___________ B _
Please Call Requester I f Delays Are Encountered.
%^ - 7 ' (I t f / %. t -)>"/ ___ f c u ? u n o
1
WATER POLLUTION pH
COD bod5
BOD, U ltim ate ' TOC
) GC
O xygen Uptake Dehydrogenase A c tiv ity (TTC) O th e r
"TT*
BIOASSAY
S pecify Organism and M ethod:
/. * ^ i ' CfC('U>.
LEACHATE FROM LEACHING TEST
PH COD bod5 BOD, U ltim ate TOC GC Bioatsav O ther
CO.O
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Bioaccum ulation ^P ersistence
D egradation Products
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W h it* R eturn to R iq u c c ttr Cenery - Environm ental Engra O ffic e File
hole E n v iro n m e n ta l Engrg. L i b
G o ld e rtro d - R e tu rn to A e o u e tte r
- A lt RCSUlTS EXPRESSED
analysis re 103.a
ENVIRONMENTAL l A6
data SHEET
, 2 3 4
5
7 8 3 10 11
O O 13 M
M 15 CD 16
17
18 19 20 21 22 23 24 25 26
27
28 29 30 31
32
33
34
E ! L 8 ,4 0 s C 3 W AtJo 3341
FC 4 3 FC I S "
LO T 2 .5 3
lo t S6 3
e c 4 8 _______ L O T 3 I S
Fc l i e
Lor 75'/
rc M S
l o t 2- < * l
Fc 17/
to r 1
Pc Zo7
lo t
2,
PC Z 0 7 8
LOT z
PC a i l - ^ o LOT S '0 8
f c 2j 7
LOT 5 / 7
f c Z I8
lot 8 7
PC 3 2 .
COT 5 3 7
f t 3Z|
lcT 5 7 2
fC 3 71
l o t 5*2 r
pc 3S7
LOT lo o
FC 430
LOT 7 .4
FC 4 3 /
lo t
fi
pc 504
lo t
1
f t 50
LOT 1 .'
FC 8 0 5 FC 0 7
lot 5 4 0 lo t lo o
FC SS1
LOT U S '
FC S o il* /
F M 3422 LOT 7 / i ,
K c -T O 'fe o to re te )
\ ,/ F C - k l 4 - ^ f \ SAMPLES
Ft . Z 3 2 X > HYDROLYSIS
c A /^ 2./
\ s t u d ie s
Pp&oS" "
c_eo7
\
3 .3
.5
7.7
< 180 t
< 1 ,0 0 0 78,000
<1,000 n% ooo
110,090 /4 2,ooo
1000
l t i ,000 *38000
600.000 206.000
1 X0,000 11,000
1 X 0.000 IlijO O O
3 3 8 f 61,000
280,000 3 1 .0 0 0
SOO.000 H 1.000
V6A000 IV , 000
290,000 *
2.8QOOC 210,000 >510,coo *
ftS fo iliE iX E (100,000 330,000
910,ooo 4
< 0 .0
7 3 o .o o o iSO .ooo ljo o ,o o o 203,o00 < 1 0 4iAooo 9 1 ,0 0 0 130,000 *
180.000 *
XLOjOoe
S i)O O o
K -- 44 *** * - * < 7,800 -- 44 46 16 K <3,8 0 0
-- I t 4t 46 4< < 1 .6 0 0
* -- 14 46
16 OtyLOO
-- 48
64 44 8.000 36,ooo 53,000
- 72,000 /2Qooo 100,000 300,000 3V9.00C 320,000 -- 8 0 ,o o o 8 ftOOO 110.000 200. OOO 3SO.OOO 390,oo
/ 10,000 -- /VO,ooo / 80,000 /to , to o n o ,o o o /to ,o o o
- 9S',ooo 130, o o o 120,0 00 20)000 110,000 7.0,000
n o .o o o f t 0 ,0 0 0 n o jo o o /20,000 n o , o oo 00,000
nof ooo -
/ 3o,ooo /S O ,o o o 10 ,0 0 0 3 0 ,0 0 0 20,000
3*1,000 -
V,e>00 110,000 7 0 ,0 0 0 i to,ooo 8 8 ,0 0 0
1
i
r S
i
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r *
578.000
*' 46 48 ' #
46 46 44 # *-1/ 1,000 VoS',ooo l3 l, o o tm .o o o 995.000 190,000
4 4 * 2 ,ooo 350,600 780,000 7VO,oo 170,000 7VO,ooo
6 WOJOOO 2 5 , Ooo 2I0.OOO / 70,ooo
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