FILE NAME: Flooring (FLR) DATE: 1994 Feb DOC#: FLR012 DOCUMENT DESCRIPTION: Journal Article - Airborne Asbestos Concentrations During Spray-Buffing of Resilient Floor Tile fc v b d Airborne Asbestos Concentrations During * Spray-Buffing of Resilient Floor Tile b b s; A lv a E d w a r d s ,* Jo h n R .

FILE NAME: Johnson & Johnson (JAJ) DATE: 1991 DOC#: JAJ 122 DOCUMENT DESCRIPTION: Journal Article - Amphibole Content of Cosmetic and Pharmaceutical Talcs - Environmental Health Perspectives Environmental Health Perspectives tbl. 94, pp. 225-230,1991 Amphibole Content of Cosmetic and Pharmaceutical Talcs by A.

FILE NAME Insurance Industry INS DATE 1992 May 19 DOC INS079 DOCUMENT DESCRIPTION Legal - Deposition of Harvey Lewis NO 0615 SHERMAN A.

267 The Classification o; Cheat Radiographs lor Coal Workers' Pneumoconiosis.

FILE NAME Brakes BRK DATE 1994 DOC BRK211 DOCUMENT DESCRIPTION OSHA Standard Work practices and engineering controls for automotive brake and clut /ww.osha.gov/pls/oshaweb/owadisp.show_document //www.osha.gov/pls/oshaweb/owadisp.show_document DOL = , OSHA Advanced Search SEARCH | OSHA to Index | En Espa^-ol| Us Contact | About OSHA 9 QuickTakas QuickTakas Biweekly Newsletter jn, Feeds [J Print Page 3 Text Size | Occupational Safety & Health Administration We Can Help Home Workers Regulations Enforcement Data & Statistics Training Publications OSHA What's New | Offices Grale Grale michanics michanics file OSHA standard standard 1994 1 of3 9/18/2010 2:57 PM Work practices and engineering controls for automotive brake and clut /ww.osha.gov/pls/oshaweb/owadisp.show_document //www.osha.gov/pls/oshaweb/owadisp.show_document p_tabl Regulations Standards - 29 CFR - Table of Contents 'Part Number Part Title Subpart Subpart Title Standard Number Title 1910 Occupational Safety and Health Standards Z Toxic and Hazardous Substances 1910.1001 App F Work practices and engineering controls for automotive brake and clutch inspection disassembly repair and assembly -- Mandatory | This mandatory appendix specifies engineering controls and work practices that must be brake and clutch inspection disassembly repair and assembly operations implemented by the employer during automotive Proper use of these engineering controls and work practices by trained employees will reduce employees asbestos exposure below the permissible exposure level during clutch and brake inspection disassembly repair and assembly operations The employer shall institute engineering controls and work practices using either the method set forth in paragraph A or paragraph B of this appendix or any other method which the employer can demonstrate to be equivalent in terms of reducing employee exposure to asbestos as defined and meets the requirements described in paragraph C of this appendix for those facilities in which no more than 5 pairs of brakes or 5whcilcuhtches are inspected disassembled reassembled and repaired per week the method set forth in paragraph D of this appendix may be used A Negative Pressure Enclosure Vacuum System Method 1 The brake and clutch inspection disassembly repair and assembly operations shall be enclosed to cover and contain the clutch or brake assembly and to prevent the release of asbestos fibers into the worker's breathing zone 2 The enclosure shall be sealed tightly and thoroughly inspected for leaks before work begins on brake and clutch inspection disassembly repair and assembly 3 The enclosure shall be such that the worker can clearly see the operation and shall provide impermeable sleeves through which the worker can handle the brake and clutch inspection disassembly repair and assembly The integrity of the sleeves and ports shall be examined before work begins asbestos fibers 4 A filtered vacuum shall be employed to maintain the enclosure under negative pressure throughout the operation Compressed may be used to remove or particles from the enclosure 5 The HEPA vacuum shall be used first to loosen the asbestos containing residue from the brake and clutch parts and then to evacuate the loosened asbestos containing material from the enclosure and capture the material in the vacuum filter 6 The vacuum's filter when full shall be first wetted with a fine mist of water then removed and placed immediately in an impermeable container labeled according to paragraph 4 of this section and disposed of according to paragraph k of this section 7 Any spills or releases of asbestos containing waste material from inside of the enclosure or vacuum hose or vacuum filter shall be immediately cleaned up and disposed of according to paragraph k of this section B Low Pressure Cleaning Method 1 A catch basin shall be placed under the brake assembly positioned to avoid splashes and spills 2 The reservoir shall contain water containing an organic solvent or wetting agent The flow of liquid shall be controlled such that the brake assembly is gently flooded to prevent the containing brake dust from becoming airborne 3 The aqueous solution shall be allowed to flow between the brake drum and brake support before the drum is removed 4 After removing the brake drum the wheel hub and back of the brake assembly shall be thoroughly wetted to suppress dust 5 The brake support plate brake shoes and brake components used to attach the brake shoes shall be thoroughly washed before removing the old shoes 6 In systems using filters the filters when full shall be first wetted with a fine mist of water then removed and placed immediately in an impermeable container labeled according to paragraph 4 of this section and disposed of according to paragraph k of this section 7 Any spills of containing aqueous solution or any containing waste material shall be cleaned up immediately and disposed of according to paragraph k of this section 8 The use of dry brushing during low pressure cleaning operations is prohibited C Equivalent Methods An equivalent method is one which has sufficient written detail so that it can be reproduced and has been demonstrated that the exposures resulting from the equivalent method are equal to or less than the exposures which would result from the use of the method described in paragraph A of this appendix For purposes of making this comparison the employer shall assume that exposures resulting from the use of the method described in paragraph A of this appendix shall not exceed 0.016 cc as measured by the OSHA reference method and as averaged over at least 18 personal samples D Wet Method 1 A spray bottle hose nozzle or other implement capable of delivering a fine mist of water or amended water or other delivery system capable of delivering water at low pressure shall be used to first thoroughly wet the brake and clutch parts Brake and clutch components shall then be wiped clean with a cloth 2 The cloth shall be placed in an impermeable container labeled according to paragraph 4 of the standard and then disposed of according to paragraph k of this section or the cloth shall be laundered in a way to prevent the release of asbestos fibers in excess of 0.1 fiber per cubic centimeter of air 3 Any spills of solvent or any asbestos containing waste material shall be cleaned up immediately according to paragraph k of this section 4 The use of dry brushing during the wet method operations is prohibited 2 of 3 9/18/2010 2:57 PM

Inspection ID Class I and II Well Inspection Form US Environmental Protection Agency - Region 4 Underground Injection Control Program 61 Forsyth Street SW, MC 9T25, Atlanta, Georgia, 30303 Phone: (404)562-9424 EPA Well ID#: F L S 1 1 3 0 0 6 7 Year-Month-Day: 2 0 2 2 - 0 9 - 1 3 EPA Permit # (or RA): 6 9 3 Page 1 Of 2 Inspector(s): Jason Rose ___________________ (lead), Page Cirillo_____________________________ Start Time: 7:33 AM ____ ____________________________________, ____________________________________ End Time: 7:45 AM_____ Facility Contact Information Facility Name: Blackjack Plant ____________________________________________________________________________ Street Address: 4940 Blackjack Plant Road _________________________________________________________________ City: Jay ____________________________ County: Santa Rosa _____________________ State: FL _____ Zip:32535 ___ Nature of Business: Oil and gas production__________________________________________________________________ Facility Owner/Operator: Black Creek Energy, LLC ____________________________ Phone: (601) 431-5386 __________ Email: harris.butler@butlerroyals.com ______________________________________________________________________ Facility Contact (if different): Michael Wetzel ___________________________________ Phone: (850) 324-6271 __________ O/O Mailing Address: 140 Virginia Street, Suite 402 __________________________________________________________ City: Richmond ______________________ County: NA_____________________________ State: VA _____ Zip: 23209 ___ Well Data from File Well Name & #: J.H.

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A R Z K > - 0 5 l5 MICROBIOS MICROTOX TOXICITY TEST TEST SUBSTANCE Identity: Perfluorooctanoic acid, ammonium salt; may also be referred to as P F O A ammonium salt, Ammonium perfluorooctanoate, PFO , FC-116, FC-126, FC-169, FC-143, or as a major component of FX-1003.

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AR226-2798 DuPont HLR 61-94 Study Title STATIC, ACUTE, ro-HOUR LC50 OF B-19704 TO BLUEGILL SUNFISB, Lepomis macrochirus Laboratory Project ID "askell Laboratory Report No. 61-94 Data Requirement United States Environmental Protection Agency 40 CFP 797.1400 Fish Acut'Toxicity Test Toxic Substances Control Act Author Keith B.

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AR226-3075 snidv Title Inhalation Toxicity Screen wi rf hnrtflP> Project.1C HL-1997-00600 Author David P.

AR226-3151 DuPont-3906 TRADE SECRET Study Title H-24256: Bacterial Reverse Mutation Test in Salmonella typhimurium and Escherichia coli Laboratory Project ID: DuPont-3906 Test Guidelines: U.S.