A R A M - 34-^0 o 44 000399 .WASHINGTON WORKS TEFLON DIVISION 4RJ& - W f September 28, 1982 TO: R.

Katherine .

226-3648 INTERIM REPORT #1 Analysis o f Oakdale W ater Samples STUDY TITLE Analysis o f Perfluorooctanoic Acid (PFOA), Perfluorobutanesulfonate (PFBS), Perfluorohexanesulfonate (PFHS), and Perfluorooctanesulfonate (PFS) in Water, Soil, Sediment, Fish, and Clams Using LC/MS/MS for the 3M Cottage Grove Monitoring Program DATA REQUIREMENTS EPA TSCA Good Laboratory Practice Standards 40 CFR 792 STUDY DIRECTOR Jaisimha Kesari P.E., DEE Weston Solutions, Inc. 1400 Weston Way West Chester, PA 19380 Phone: 610-701-3761 INTERIM REPORT COMPLETION DATE May 19, 2005 PERFORMING LABORATORY Exygen Research 3058 Research Drive State College, PA 16801 , Phone:814-272-1039 STUDY SPONSOR 3M Company 3M Building 0236-1-B-10 St.

P-1 Aetzb-nrf > 5 ^ 5 ACUTE TOXICITY TO THE OLIGOCHAETE WORM (Lumbriculus variegatus) TEST SUBSTANCE___________________________________________ Identity: Perfluorooctanesulfonate; may also be referred to as PFOS or FC-95. (1-Octanesulfonic acid, 1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8heptadecafluoro-, potassium salt, CAS # 2795-39-3) Remarks: The test substance is a white powder.

Katherine E.

3M General Offices 3M Center St.

INTERIM REPORT # 7-Analvsis of Soil Boring Samples STUDY TITLE Analysis of Perfluorobutanesulfonate (PFBS), Perfluorohexanesulfonate (PFHS), and Perfluorooctanesulfonate (PFOS) in Water, Soil, Sediment, Fish, Clams, Vegetation, Small Mammal Liver and Small Mammal Serum Using LC/MS/MS for the 3M Decatur Monitoring Program DATA REQUIREMENTS EPA TSCA Good Laboratory Practice Standards 40 CFR 792 STUDY DIRECTOR Jaisimha Kesari P.E., DEE Weston Solutions, Inc. 1400 Weston Way West Chester, PA 19380 Phone: 610-701-3761 INTERIM REPORT COMPLETION DATE October 27,2006 PERFORMING LABORATORY Exygen Research 3058 Research Drive State College, PA 16801 Phone: 814-272-1039 STUDY SPONSOR 3M Company 3M Building 0236-01-B-10 St.

Ak 2.6 - Q Z $ 0 ACUTE TOXICITY TO AQUATIC INVERTABRATES (DAPHNIA MAGNA) TEST SUBSTANCE____________________________________________ Identity: A mixture containing periluorooctanesulfonate, which may also be referred to as PFOS, FC-95, or as a component of FC-600. (1-Octanesulfonic acid, 1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8heptadecafluoro-, potassium salt, CAS # 2795-39-3) Remarks: The 3M production lot number was not noted.

AR Z 6 - 0 3 * 0 ACTIVATED SLUDGE RESPIRATION INHIBITION TEST TEST SUBSTANCE_______________________________________________ Identity: A mixture containing perfluorooctanesulfbnate, whichmay also be referred to as PFOS, FC-95, or as a component of FX-3104. (1Octanesulfonic acid) (CAS # 2795-39-3).

2 . 4 5 R C V t a -79 mm> tJTil.iSKEO'BO; E 1. d u P o n t d e N em o u r s & C o m p a n y IN C O R P O R A T E D W il m in g t o n .

STLS F V F R N TRENT STL Chicago 2-117 Rond Street University Park, IL 60466 Tel: 708 534 5200 Fax; 708 534 5211 www.stl-inc.com V E R N T R E N T L A B O R A T O R IE S A N A L Y T IC A L R E PO R T JOB NUMBER: 233.2 5 P r e p a r e d 'For : W e s t o n .

SEVERN TRENT STL STL Chicago 2417 Bond Street University Park, IL 60466 Tel; 708 534 5200 Fax; 708 534 5211 www.stl-inc.com S iqria L /v Name: Richard Ch WrighL T it.T.e ; P ro je c t Manage r E-Mail : r w r i g h t @ s t 1 - i n c .corn This Report Contains Leaders in Environmental Testing Da Le STL Chicago 2417 Bond Street University Park, IL 60466 PHONE: (70S) 534-5200 FAX. ,, : (708) 534-521:1 Pages Severn Trent Laboratories, Inc.

SEVERN TRENT LABORATORIES ANALYTICAL REPORT JOB NUMBER: 245318 Prepared For: Weston Solutions, Inc. 1400 Weston Way Building 5-2 West Chester, PA 19380-1499 Project: Confidential Decatur - FC Investigation Attention: Jai Kesari Date: 04/07/2006 Signature Name: Richard C.

C o n stru ctio n Materials Engineering ami Testing g E n vironm ental Engineering and Consulting G eotechnical Engineering m Analytical Sen dees m TRANSMITTAL TO: Weston Solutions, Inc._________ __ DATE: March 23. 2005______ P.O.

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