3M FLUOROCHEMICAL SUBMISSIONS February, 2002 - May, 2004 INDEX OF 3M'S 2002-2004 AR-226 DOCKET SUBMISSIONS BY DATE Back to Menu February 2003 Click on Study Title to View Report February 13,2003 February 13, 2003 Submission Cover Letter Final Report, A Pharmacokinetic Study of Potassium Perfluorooctanoate in the Cynomolgus Monkey, P.E.

SPrimedica Argus Research Laboratories, Inc. 90S Sheehy Drive, Building A Horsham, PA 19044 Telephone: (215) 443-8710 Telefax: (215)443-8587 REPORT AMENDMENT 1 12 OCTOBER 2000 PROTOCOL 418-009 COMBINED ORAL (GAVAGE) FERTILITY, DEVELOPMENTAL AND PERINATAL/POSTNATAL REPRODUCTION TOXICITY STUDY OF N-ETFOSE IN RATS FINAL REPORT Attached is the corrected Text Figure 1 to the above-referenced final report.

Larry K.

DuPont-15302 Study Title Ammonium Perfluorooctanoate: Age Effect on the PFOA Plasma Concentration in Post-Weaning Rats Following Oral Gavage T est Guidelines: None applicable Author: Paul M.

/)Rm-OHI Submitted to : BIOSEARCH, INC. p.o. box 8598 Philadelphia, Pennsylvania 19101 te leph one: (215) 848-4499 3M Company 3M Center S t .

/ N frU -0 5 2 .5 ACUTE TOXICITY TO FISH TEST SUBSTANCE_______________________________________________ Identity: Perfluorooctanoic acid, ammonium salt; may also be referred to as PFOA ammonium salt, Ammonium perfluorooctanoate, PFO, FC116, FC-126, FC-169, FC-143 or as the major component of FC1015.

"Rogar J.

4 A te & 'i t 3 J1R ENVIRONMENTAL LABORATORY REPORTNO.

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AR226-2088 EID078449 RJZ004538 SITE: flHHMIl.Al.: j DATES NO.OF OMEGA re ho uirwvop caudi en SAUPI PR PROS

232.1 441572.0. 4346794.0 441577.11,4346769.53 441582.21.4346745.05 441587.32.4346720.58 441592.42.4346696.11 441597.53.4346671.63 441601.0. 4346655.0 441579.88.4346641.63 441558.75,4346628.26 441537.63.4346614.89 441522.0. 4346605.0 441503.0. 4346601.0 441483.86,4346584.91 441464.73,4346568.83 441445.59,4346552.74 441434.0. 4346543.0 441448.9,4346522.92 441457.0. 4346512.0 441444.34,4346490.44 441431.68.4346468.89 441420.0. 4346449.0 441401.14.4346432.59 441382.28,4346416.18 441363.42.4346399.77 441344.56,4346383.36 441325.69,4346366.95 441320.0. 4346362.0 441324.51,4346337.41 441329.02,4346312.82 441333.54,4346288.23 441338.05.4346263.64 441340.0. 4346253.0 441364.75.4346256.51 441389.51.4346260.01 441414.26.4346263.52 441439.01.4346267.02 441463.77.4346270.53 441488.52.4346274.03 441513.27.4346277.54 441538.02.4346281.04 441562.78.4346284.55 441587.53.4346288.05 441612.28.4346291.56 441637.04.4346295.06 441661.79.4346298.57 441686.54.4346302.07 441711.3.4346305.58 441736.05.4346309.08 441760.8.4346312.59 441785.55.4346316.09 441810.31.4346319.6 441835.06,4346323.1 441859.81.4346326.61 441884.57.4346330.12 441909.32.4346333.62 441912.0. 4346334.0 441908.73.4346358.78 441905.45.4346383.57 44905.0,4346387.0 AR226-2167 EID447781 . 441929.58,4346391.54 441954.17.4346396.09 441978.75.4346400.63 442003.33,4346405.18 442027.92.4346409.72 442052.5,4346414.27 442077.08,4346418.81 442101.67.4346423.36 442126.25.4346427.9 442143.0. 4346431.0 442146.0. 4346416.0 442170.16.4346422.44 442176.0. 4346424.0 442180.0. 4346402.0 442204.18.4346408.36 442228.35.4346414.72 442252.53.4346421.09 442275.0. 4346427.0 442272.99,4346451.92 442270.97.4346476.84 442268.96,4346501.76 442267.0. 4346526.0 442291.43,4346531.29 442315.87.4346536.58 442340.3.4346541.87 442364.74,4346547.16 442389.17.4346552.44 442413.61.4346557.73 442438.04.4346563.02 442462.47,4346568.31 442486.91.4346573.6 442498.0. 4346576.0 442493.0. 4346589.0 442517.57.4346593.6 442542.14,4346598.21 ' 4 4 2 5 6 6 . 7 2 , 4 3 4 6 6 0 2 . 8 1 442591.29,4346607.42 442615.86.4346612.02 442640.43.4346616.63 442665.01,4346621.23 442689.58.4346625.84 442714.15.4346630.44 442738.72,4346635.05 442763.3,4346639.65 442787.87,4346644.25 442812.44,4346648.86 442837.01,4346653.46 442861.58.4346658.07 442886.16,4346662.67 442910.73,4346667.28 442935.3.4346671.88 442959.87,4346676.49 442984.45.4346681.09 443009.02.4346685.7 443033.59.4346690.3 443048.0. 4346693.0 443043.47.4346717.59 443041.0. 4346731.0 443065.57,4346735.61 EID447782 443090.14,4346740.22 443114.71,4346744.84 443139.28.4346749.45 443163.85,4346754.06 443188.43,4346758.67 443213.0. 4346763.28 443237.57,4346767.89 443262.14,4346772.51 443286.71,4346777.12 443311.28.4346781.73 443335.85.4346786.34 443360.42,4346790.95 443366.0. 4346792.0 443361.52.4346816.59 443357.04,4346841.19 443352.55,4346865.78 443348.07.4346890.38 443343.59,4346914.97 443339.11.4346939.57 443334.62,4346964.16 443330.14.4346988.76 443327.0. 4347006.0 443302.48.4347010.86 443277.96.4347015.73 443253.43.4347020.59 443228.91.4347025.46 443206.0. 4347030.0 443181.38.4347034.34 443156.76,4347038.69 443155.0. 4347039.0 443130.04,4347037.64 443105.07,4347036.28 443080.11.4347034.92 443055.15.4347033.57 443030.18,4347032.21 443008.0. 4347031.0 442996.0. 4347028.0 442971.0. 4347028.16 442946.0. 4347028.31 442921.0. 4347028.47 442896.0. 4347028.63 442871.0. 4347028.78 442846.0. 4347028.94 442836.0. 4347029.0 442825.0. 4347030.0 442800.03.4347028.86 442775.05.4347027.73 442750.08.4347026.59 442737.0. 4347026.0 442716.0. 4347032.0 442691.26.4347028.38 442666.53.4347024.77 442641.79,4347021.15 442617.05,4347017.54 442592.31.4347013.92 442586.0. 4347013.0 442574.0. 4347015.0 442560.0. 4347012.0 442545.0. 4347018.0 442520.1,4347015.79 442495.2,4347013.57 442470.29.4347011.36 442445.39,4347009.15 442420.49,4347006.93 442395.59,4347004.72 442370.69.4347002.51 442365.0. 4347002.0 442357.0. 4347005.0 442350.0. 4346997.0 442329.0. 4346996.0 442315.0. 4346995.0 442302.0. 4346990.0 442285.0. 4346985.0 442260.02,4346985.96 442259.0. 4346986.0 442252.0. 4346983.0 442227.7,4346977.11 442219.0. 4346975.0 442194.88.4346968.42 442186.0. 4346966.0 442161.12.4346963.51 442156.0. 4346963.0 442131.44.4346958.36 442106.87,4346953.71 442082.31,4346949.07 442057.74.4346944.42 442033.18.4346939.78 442008.61,4346935.14 441984.05,4346930.49 441959.48,4346925.85 441955.0. 4346925.0 441930.39,4346920.61 441905.78,4346916.21 441881.17,4346911.82 441871.0. 4346910.0 441860.0. 4346910.0 441848.0. 4346898.0 441832.0. 4346895.0 441820.0. 4346891.0 441804.0. 4346886.0 441780.19,4346878.39 441756.37.4346870.79 441732.56,4346863.18 441732.0. 4346863.0 441708.82,4346853.63 441685.64,4346844.26 441685.0. 4346844.0 441663.0. 4346841.0 441640.0. 4346841.0 441619.52,4346826.66 441610.0. 4346820.0 441595.0. 4346819.0 441585.0. 4346808.0 441572.0. 4346794.0

AR226-2174 DISPERSION MODELING PROTOCOL Fluoropolymers Plant-A PFO Emissions DuPont Washington Works Prepared by: .

AR226-2363 )i Detecting and Quantifying Low Levels of Fluoropolymer Polymerization Aids - A Guidance Document t Fluoropolym er M anufacturers G roup (FM G ) - T echnical W orking G roup (TW G ) - A n alytical W orking G roup (AW G ) T he Society o f the P lastics Industry, Inc. 1801 K Street, NW , Suite 600K W ashington, DC 20006-1301 S EXP000571 T h is p a g e le ft in te n tio n a lly b lan k .

AR226-2399 COMMUNITY STATUS VATER AIR SOLID VASTE 10635-1 - 03/08/69 - WBC:kt EID951507 RJZ009905 WASHINGTON WORKS OFF-PLANT EMISSIONS POUNDS C-8 1983 1986 ' 1988 WATER 21,700 19,100 23,300 AIR 12,700 16,200 26,200 PRODUCT 8,000 8,300 11,300 OFF-PLANT DISPOSAL 7,700 TO CW - WWTP TO LETART LANDFILL 8,300 9.000 2.000 50,100 51,900 71,800 RJZ009906 10635-2 - 03/01/19 - WIC:kst EID951508 C-8 LEVELS IN DRINKING WATER DISTANCE FROM NO. 5 OUTFALL (MILKS) PPB 1984 1987 1988 PARKERSBURG 7.50 UPSTREAM ND ND -- WASH WORKS 0.50 UPSTREAM ND ND ND LUBECK WATER DISTRICT 0.25 DOWNSTREAM 0.25 DOWNSTREAM 1.1 1.9 1.8 1.5 1.9 1.4 LITTLE HOCKING 3.00 DOWNSTREAM 0.6 ND ND RAVENSWOOD 29.0 DOWNSTREAM ND ND = NOT DETECTABLB RJZQ9907 10635-3 - 03/08/89 - WIC:kat EID951509 WASHINGTON WORKS C '8 ANNURL M E A N OONCEN T R A T /O N C A S E 1 - 1983 806<500ZftI EID951510 C-8 ENVIRONMENTAL PROGRAMS WATER CLOSURE OF SUPERNATE PONDS TIMING 4Q88 PURCHASE OF LUBECK WATER COMPANY - CLOSING TURN OVER TO DuPONT 3Q89 4Q91 REPLACEMENT OF C-8 IN FBP WITH TBSA POSSIBLE C-8 RECOVERY FROM FBP EFFLUENT 19X IN 1988 IN PROGRESS AIR FINE POWDER DRYER RECOVERY PROJECT UPDATE FENCE LINE MONITORING 4089 4Q89 RJZ009909 10635-4 - 03/08/09 - WKCkst EXD951511