GLP10-01-02.

GLP10-01-02; Interim Report 37 - Analysis of PFBS, PFHS, and PFOS in Water Samples Collected at the Former Bert Jeffries Property in Decatur, AL - October 2012 Study Title Analysis of Perfluorooctane Sulfonate (PFOS), Perfluorohexane Sulfonate (PFHS) and Perfluorobutane Sulfonate (PFBS) in Groundwater, Soil and Sediment for the 3M Decatur Phase 3 Site-Related Monitoring Program Data Requirement EPA TSCA Good Laboratory Practice Standards 40 CFR Part 792 Study Director Jaisimha Kesari P.E., DEE Weston Solutions, Inc. 1400 Weston Way West Chester, PA 19380 P hone:610-701-3761 Author Susan W olf 3M Environmental Laboratory Interim Report Completion Date Date of signing Performing Laboratory 3M Environmental Health and Safety Operations Environmental Laboratory 3M Center, Bldg 260-05-N-17 St.

3M ENVIRONMENTAL LABORATORY REPORT NO.

ACUTE TOXICITY TO FISH TEST SUBSTANCE Identity: Perfluorooctanesulfonate, DEA salt; may also be referred to as PFOS DEA salt, FC-99, or 3M Sample No. 2. (1-Octanesulfonic acid, 1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-heptadecafluoro-, compd. with 2,2'-iminobis[ethanol] (1:1), CAS # 70225-14-8) Remarks: Test sample is a mixture of the test substance in water (approximately 25% test substance and 75% water).

T - 3 *1 1 1 t & - O Z23 \ /'- ' 28 Dermal Percutaneous Absorption Study with FC-128 in Albino Rabbits Experiment No.

Acute Oral Toxicity Screen with T-3065COC in Albino Bats a S iV' ,$ ^ < sj u v-^V Kxpr'ri.incnt No. : Conducted At: Dates Conducted: Conducted By: 0981AR0145 Safety Evaluation Laboratory Riker Laboratories, Inc.

A R Z 2 6 'G > Z & International Research and Development Corporation SPONSOR: COMPOUND: SUBJECT: 3M Company FM-3422 Ninety Day Subacute Rat Toxicity Study.

HAZLETON LABORATORIES AM ERCA.M C. 3301 KINSMAN BLVD., P.O.

C O R N IN G Hazleton ft l' /-* v' MUTAGENICITY TEST ON T-6358 f| v ' .V IN AN IN VIVO MOUSE MICRONUCLEUS ASSAY FINAL REPORT AUTHOR Hemalatha Murli, Ph.D.

TECHNICAL REPORT SUMMARY BACK TO MAIN D a tu 8/25/81 TO: TECHNICAL COMMUNICATIONS CENTER - 201-2CN (lnil>nrt;int I f report sprinted on both sides o f paper, send two copies to TCC.)

Quality Assurance Project Plan Multi-City Study Sampling Task (NJ00666) BACK TO MAIN Revision No. : 1 Effective Date: M ay 14, 1999 Page i o f iv Quality Assurance Project Plan for Empirical Human Exposure Assessment Multi-City Study Sampling Task To May 14,1999 Prepared by Battelle 397 Washington Street Duxbury, MA 02332 (781) 934-0571 APPROVALS Sampling Task Leader Rosanna Buhl Battelle Sampling Task QA Officer __f l / ; JtjJy/,ATJl& Marcia Nishioka * Battelle Project Manager Susan bbgy Battelle Program QA Officer Date Date q n /n Date s litto Date Date Quality Assurance Project Plan Multi-City Study Sampling Task (N100666) Joseph Fiksel Marcia Nishioka Suan Abbgy Donald Gunster Rosanna Buhl Wayne Trulli Scott Macomber Chris Gagnon Kelly Irizarry Robert Mandeville Richard Restucci Kim Andrews Distribution List BACK TO MAIN Revision No.: 1 Effective Date: May 14, 1999 Page ii o f v BACK TO MAIN Quality Assurance Project Plan Multi-City Study Sampling Task (N100666) Revision No.: 1 Effective Date: May 14, 1999 Page iii o f v CONTENTS 1.

BACK TO MAIN Centre Analytical Laboratories, Inc. 3048 Research Drive State College, PA 16801 www.centrelab.com ^P hone: (814) 231-8032 Fax: (814) 231-1253 or (814) 231-1580 Analytical Report Fluorochemical Characterization of Surface Water Samples Decatur, Alabama (W1979) Centre Analytical Laboratory Report No. 023-014B (Revision 1) Revision Date 3/21/01 Testing Laboratory Centre Analytical Laboratory', Inc. 3048 Research Drive State College, PA 16801 3M Environmental Laboratory Contact Kent R.

BACK TO MAIN Centre Analytical Laboratories, Inc. 3048 Research Drive State College, PA 16801 www.centrelab.com ^P h on e : (814) 231 -8032 Fax: (814) 231 -1253 or (814) 231 -1580 Analytical Report Fluorochemical Characterization of Sediment, POTW Sludge, and Landfill Leachate Samples Port St.

ENVIRONMENTAL PHYSICAL/CHEMICAL, FATE, EFFECTS AND MONITORING STUDIES N-EtFOSE ALCOHOL backtocompounds P h ysical/C h em ical S TU D Y TITLE LABORATORY OR AUTHOR DATE COMPLETED TYPE C haracterization Study ETFO SE-O H, test Control R eference #SE-035.

BACK TO MAIN - 1- PERFLUOROOCTANESULFONATE AND RELATED FLUOROCHEMICALS IN OYSTER, CRASSOSTREA VIRGINICA, FROM THE GULF OF MEXICO AND CHESAPEAKE BAY John P.