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K A M - lif-lf-r R.

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Proven Results.

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Precise Research.

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Wildlife International.

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3M General Offices AR226-1895 3M Center St.

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AR226-2051 BEST COPY AVAILABLE EID077205 EID 0 7 7 2 0 6

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0- 148.0 0- 309.0 0- 456.0 0 - 609,0 " Qz ID 2851.0 m 2589.2 m 2397.5 m 2310.1 ill Calibration Sample Name Weight (g BLANK XXXXXX) 148,0 1.0000 309.0 1.0000 450.0 1.0000 609.0 1.0000 765.0 1.0000 1000.0 1.0000 1508.0 1.0000 1713.0 1,0000 178B.0 1.0000 2275.0 1.0000 C-SPsak C-10 Peak Corrected | b Height Height c-a I Correlation 6818 235105 xxxxxxxx calc pk 428512 226285 421952 148.0 308043 237791 801150 281.0 1101968 221769 1095539 384.3 1432967 251095 1425688 500.1 1593255 260053 1585716 556.2 2033812 297132 2025199 2695213 223986 2688720 710.3 943.1 2956715 263653 2949072 1034.4 3129804 258813 3122301 1095.1 3755512 325203 3746085 1313.9 0 .0 b 1.0 Correlation C8 PPM calc pk 148.0 157.8 281.0 304.3 384.3 418.0 500.1 545.5 556.2 607.3 710.3 777.0 943.1 1033.3 1034.4 1133.8 1095.1 1200.7 1313.9 1441.7 13271.7 b 1.0 Correlation C8 PPM calc pk 157.8 162,5 304.3 320.6 418.0 443.4 545.5 581.1 607.3 647.9 777.0 831,2 1033.3 1107,9 1133.8 1216.5 1200.7 1288.8 1441.7 1549.0 32424.0 b 45663.6 i 1.0 Correlation 1.0 Correlation C8 PPM calc pk C8 PPM calc pk 162.5 320.6 443.4 16Z9 327.0 454.5 162.9 327,0 454.5 158.8 339.6 4B0.0 581.1 597.4 597,4 637.4 647.9 666.7 666.7 713.7 831.2 856.9 856.9 923.2 1107.9 1144.1 11144.1 1239,6 1216.5 1256.8 1256.8 1363.7 1288.8 1331.8 13318 144S.O 1549.0 1601.8 10018 174-J.o FP 1 FP 2 FP 3 FP 4 FP 5 FP 6 FP 7 FP 8 FP FP 10 FP 11 FP 12 FP 13 FP. 14 FP 15 FP 16 FP 17 FP 16 FP 19 FP 20 FP 21 FP 22 FP 23 0.5306 0.5750 0.5065 0.5217 0.5291 0,5956 0.6646 0.5183 0.5769 0.5649 0.5310 0.4958 0.5018 0.5064 0.5281 0.5117 0.5254 0.5367 0.5000 0.5530 0.5040 0.5030 0.5235 C-10 Peak Height Haight 365704 273494 707118 288431 509686 255687 124408 237885 468182 263369 92261 249360 794733 260443 866019 311955 832620 224096 623556 249217 442922 235366 686492 241814 785379 233470 149563 386431 162522 315010 67592 321813 84557 407816 310507 332929 243504 331220 376969 350166 126814 325285 83503 338561 195321 314340 Corrected | Qz 148.0 0 8 calc pk CSPPM 357776 125.5 236.5 698757 245.1 420.2 502274 176.2 347.8 117512 41.2 79.0 460547 161.5 305.3 85032 29.8 50.1 787183 276.1 415.4 856976 300.6 579.9 826124 289.8 502.3 616332 216.2 382.7 436085 153.0 288.1 879482 238.3 480.7 778611 273.1 544.2 138361 48.5 95.8 153390 53.8 101.9 58263 20.4 39,9 72735 25.5 48.6 300856 105.5 196.6 233902 82.0 164.1 366818 128.7 232.7 117384 41.2 81.7 73689 25.8 48.9 186209 65.313 127.63S 2 : 309,0 calc pk CSPPM 133.1 250.8 284.7 460.4 188.9 372.9 40.3 77.2 172.7 326.5 27.7 46.5 298.9 449.7 325.8 628.7 313.9 544.2 232.9 412.3 163.3 307.5 257.3 519.0 295.6 589.0 .48.3 95.4 54.1 102.5 17,4 34,0 23.0 43.7 111.1 206.9 85.2 170.4 136.5 246.9 40.2 79.8 23.3 44.2 66.790 130.52G Or 456.0 S i 609.0 calc pk C8PPM calc pk C8 PPM 135.7 255.8 135.1 254.6 277.9 483.3 282.7 4917 196.0 386.9 197.7 390.2 35.5 68.0 31.1 59.6 178.6 337.5 179.6 339.4 21.9 36.8 17.0 28.6 314.8 473.7 3210 4 3 3 .0 343.9 663.5 3512 077.6 331.0 573.8 337.8 585.6 243.5 168.4 431.1 317.1 247.0 169.0 437.3 318.3 269.9 544.3 274,4 553.4 311.2 44.2 620.2 87.3 317,3 40.1 79.2 50.5 10.8 16.8 112.0 84.0 139.6 35.4 95.5 2 1 .1 32.0 208.6 168.' 252.2 70.3 46.6 6.6 117 110.5 815 , 139.0 31.0 88.3 10.7 22.3 205.8 163.0 2514 618 17,2 32.6 64.143 125.353 1 2 .1 60.839 23,0 118.895 Qi 19/ .1 1/ JL -1 .9 332.9 o o l .0 loo.o 2816 o4o .o 2 3 .0 1010 RQ A \O ,0 "/ .3 AR226-2090 RJZ042298 765.0 Qz 1000.0 0- 1508.0 0- 1713.0 0- 1788.0 2097.3 m 1981.5 m 1754,7 m 1662.1 m 1639.1 88929.4 b 120271.9 b 203748.1 b 241791.6 b 251744.0 1.0 Correlation 1.0 correlation 1.0 co irelatior 1.0 correlation 1.0 CALIBRATION C8PPM c a lc pk C8 PPM c a lc p k C8PPM c a lc p k C8 PPM c a lc pk C8PPM NAME 158.8 152.2 152.2 124.4 124.4 108.4 108.4 103.8 103.8 339.6 343.6 343.6 340.5 340.5 338.5 336.5 335.2 335.2 480.0 492.2 492.2 508.2 508.2 513.7 513.7 514.8 514.8 637.4 658.8 658.8 696.4 69a4 712.3 712.3 716.2 716.2 713.7 739.5 739,5 787.6 787.6 808.6 806.6 813.8 813.8 923.2 961.3 961.3 1038.0 1038.0 1073.0 1073.0 1082.0 1082.6 1239.6 1296.2 1296.2 1416.1 1416.1 1472.2 1472.2 1486.8 1486.8 1363.7 1427.6 1427.6 1564.5 1564.5 1828.8 1828.8 1645.6 1645.6 1446.3 1515.0 1515.0 1863.2 1663.2 1733.1 1733.1 1751.3 1751.3 1743.8 1829.8 1829.8 2018.7 2018.7 2108.4 2108.4 2131.9 2131.9 148.0 309.0 450.0 609.0 765.0 1000.0 1508.0 1713,0 1788.0 2275.0 7350 E765.0 C8PPM c a lc 241.6 St p k C8 PPM c a lc 119.9 225.9 k pk C8PPM c a lc 87.8 165.4 pk C8PPM c a lc 69.8 131.5 St 1788.0 SAM PLE pk C8PPM NAME 64.7 121.9 F P 1 505.7 291.9 507.7 282.1 490.6 274.9 478.1 27Z7 474.3 FP 2 389.1 192,8 380.6 170.1 335.9 156.7 309.4 152.8 301.8 F P 3 28.1 -1.4 -2.7 -49.1 -94.2 -74.8 -143.3 -81.9 -157.0 FP 4 334.9 171.7 324.6 146.3 276.6 131.6 248.8 127.4 240.8 FP 5 -3.1 -17.8 -29.9 -67.7 -113.6 -94.3 -158.4 -101.7 -170.8 FP 6 501.0 706.6 336.6 371,8 506,4 717,3 332.5 372.3 500.3 718.2 328.1 370.1 493.7 714.1 326.7 369.2 491.5 FP 7 712.4 FP 8 609,3 356,2 617.5 354.7 614.8 351.6 609.4 350.4 607.4 FP 9 445.2 250.3 443.2 235.1 416.2 225.3 398.9 222.4 393.8 FP 10 311.7 159.4 300.1 132.4 249.4 116.9 220.1 112.5 211.8 FP 11 567.9 282.2 569.2 271.1 546.8 263.3 531.1 261.0 526.3 FP 12 655.3 332.2 662.1 327.6 65Z9 323.0 643.6 321.4 640.6 FP 13 46.5 9.1 18.0 -37.3 -73.6 -62.2 -122.9 -69.2 -136.6 FP 14 5B.2 16.7 31.6 -28.7 -54.3 -53.2 -100.7 -80.0 -113.6 FP 15 -28.6 -31.3 -61.2 -82.9 -162.0 -110.4 -215.8 -118.0 -230.7 FP 16 -14.7 -24.0 45.7 -74.7 -142.1 -101.7 -193.6 -109.2 -207.9 FP 17 188.3 91.1 189.8 55.3 103.1 35.5 66.2 30.0 55.8 FP 18 138.2 57.3 114.7 17.2 34.4 -4.7 -9.5 -10.9 -21.8 FP 19 239.6 124,4 225.0 92.9i 168.0 75.2 136.0 70.2 127.6 FP 20 26.9 -1.5 -2.9 -49.2!

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AR226-3004 DuPont HLR2S7-S4 HASKELL LABORATORY FOR TOXICOLOGY AND INDUSTRIAL MEDICINE STATIC.

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Study Sponsor: Issue Date: Document Reference No.: ELF ATOCHEM 25-Jan-95 53957 AR226-3009 Acute Toxicity to Daphnia Author(s): H.

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M M _ 3- DuPont Haskell Laboratoiy for Health and Environmental Sciences FROM: J.

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AR226-3342 Environmental fate studies o f fluorotelomer interm ediates used to produce surfactants and p o ifin e rs Bill Berti DuPont Central Research & Development Wilmington, Delaware USA Themiracles o f science Acknowledgements uNing Wang Daryl Cobranchi ^Barbara Larsen Bogden Szostek Mary Kaiser John Gannon Bob Buck Lisa Sulecki Pat Folsom Mark Starr Chien-Ping Kao Christopher Bowers Vladimir Capka (ffypoft Outline Background Intermediates and Products Overview of E-fate studies Physical-Chemical Properties Water solubility and Vapor Pressure . 6-2TBI, 8-2TBI, 6-2TBA, 8-2TBA Measured vs.