Phone Conversation Report f erni 0 / r wCOPi 3M 2?

Study Title Solubility of Perfluoro-1-octanesulfonyl Fluoride (P O S F) in W ater Data Requirement 40 CFR 160.105(b) Author Mark E.

/|R 1%-OS07 ACUTE TOXICITY TO AQUATIC INVERTABRATES (DAPHNIA MAGNA) TEST SUBSTANCE Identity: Perfluorooctanoic acid, ammonium salt; may also be referred to as PFOA ammonium salt, Ammonium perfluorooctanoate, PFO, FC- 116, FC-126, FC-169, or FC-143.

\Sl1& FINAL REPORT r-o 3 TJ TJ O 30 tin i to * r --*d} TJ 3: -`- c `r j r r i O C3 ro fs> O Bioconcentration test o f 2-perfluoroalkyl (C=4-16) ethanol [This test was performed using 2-{perfluorooctyl) ethanol (Test substance number K-1518)] in carp (Test number : 51518) Kurume Laboratory Chemicals Evaluation and Research Institute, Japan 000001*1 STATEMENT 51518 Kumme Laboratory Chemicals Evaluation and Research Institute, Japan Sponsor ASAHI GLASS Co., Ltd.

*R a 6 _ PERSONAL AND CONFIDENTIAL CC: J .

AA A 6 - ih0 TSCA NCIC Notification Form for CBI Documents Docket Number: ________________ Document Control Number: 7Document Date: ~ 63^3 o o q 5 S' ______________________________________ Document Type: F __________________ o- opmoNCu=O>> < r> "90 XT -- T *> o0 ron O cn ro O(TTChSFBeCTIdA)Sou,CAcnANudRDmeEreIQTnSUIteMIrcRPetEOfiSoSeEEnrSPe1nCA4cRoTIeMOfdINPtahRAbLOeoPTTvEEoeCNxiATsicLFcTRSlIOEauSMibmFsPeOtUdaRBnaLTscIHCecEsDoKICSnNCofOiLndWOteISNrnUoGtRilaAEAlNScDbCutWBs(ITiILnSLOeFCBsUTAsLA)iIUn.NNfEToADhUrUaTmHNtaODsteERiocRIZntEioDn RELEASE ORDISCLOSURE OFSUCHINFORMATION.

Fraunhofer ITEM Final Report 01 G 00 0 02 [Appendices G] 28 Day Repeated Dermal Contact Study of 3M Test Articles in Sprague-Dawley Rats Page 1 of 12 Appendix G: Amendments and Deviations (Copies) Fraunhofer ITEM Final Report 01 G 00 0 02 [Appendices G] 28 Day Repeated Dermal Contact Study of 3M Test Articles in Sprague-Dawley Rats Page 2 of 12 Study Plan Deviation Study No.: 01 G 00 0 02 Date: 8.5.00 Deviation No.: 1 S ubject: Fabric conditioning Page: 8 Paragraph: 5,3.2 Change: In addition to the description in the study plan (paragraph 5.3.2, page 8) the fabrics were pre-conditioned w ith deionisized w ater (spray application).

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AR226-2036 PECKSR 07/28/98 11:53 AM To: SZAKATBK, M1LLERSR , HALBERRM cc: PLAYTIS .

0- 148.0 0- 309.0 0- 456.0 0 - 609,0 " Qz ID 2851.0 m 2589.2 m 2397.5 m 2310.1 ill Calibration Sample Name Weight (g BLANK XXXXXX) 148,0 1.0000 309.0 1.0000 450.0 1.0000 609.0 1.0000 765.0 1.0000 1000.0 1.0000 1508.0 1.0000 1713.0 1,0000 178B.0 1.0000 2275.0 1.0000 C-SPsak C-10 Peak Corrected | b Height Height c-a I Correlation 6818 235105 xxxxxxxx calc pk 428512 226285 421952 148.0 308043 237791 801150 281.0 1101968 221769 1095539 384.3 1432967 251095 1425688 500.1 1593255 260053 1585716 556.2 2033812 297132 2025199 2695213 223986 2688720 710.3 943.1 2956715 263653 2949072 1034.4 3129804 258813 3122301 1095.1 3755512 325203 3746085 1313.9 0 .0 b 1.0 Correlation C8 PPM calc pk 148.0 157.8 281.0 304.3 384.3 418.0 500.1 545.5 556.2 607.3 710.3 777.0 943.1 1033.3 1034.4 1133.8 1095.1 1200.7 1313.9 1441.7 13271.7 b 1.0 Correlation C8 PPM calc pk 157.8 162,5 304.3 320.6 418.0 443.4 545.5 581.1 607.3 647.9 777.0 831,2 1033.3 1107,9 1133.8 1216.5 1200.7 1288.8 1441.7 1549.0 32424.0 b 45663.6 i 1.0 Correlation 1.0 Correlation C8 PPM calc pk C8 PPM calc pk 162.5 320.6 443.4 16Z9 327.0 454.5 162.9 327,0 454.5 158.8 339.6 4B0.0 581.1 597.4 597,4 637.4 647.9 666.7 666.7 713.7 831.2 856.9 856.9 923.2 1107.9 1144.1 11144.1 1239,6 1216.5 1256.8 1256.8 1363.7 1288.8 1331.8 13318 144S.O 1549.0 1601.8 10018 174-J.o FP 1 FP 2 FP 3 FP 4 FP 5 FP 6 FP 7 FP 8 FP FP 10 FP 11 FP 12 FP 13 FP. 14 FP 15 FP 16 FP 17 FP 16 FP 19 FP 20 FP 21 FP 22 FP 23 0.5306 0.5750 0.5065 0.5217 0.5291 0,5956 0.6646 0.5183 0.5769 0.5649 0.5310 0.4958 0.5018 0.5064 0.5281 0.5117 0.5254 0.5367 0.5000 0.5530 0.5040 0.5030 0.5235 C-10 Peak Height Haight 365704 273494 707118 288431 509686 255687 124408 237885 468182 263369 92261 249360 794733 260443 866019 311955 832620 224096 623556 249217 442922 235366 686492 241814 785379 233470 149563 386431 162522 315010 67592 321813 84557 407816 310507 332929 243504 331220 376969 350166 126814 325285 83503 338561 195321 314340 Corrected | Qz 148.0 0 8 calc pk CSPPM 357776 125.5 236.5 698757 245.1 420.2 502274 176.2 347.8 117512 41.2 79.0 460547 161.5 305.3 85032 29.8 50.1 787183 276.1 415.4 856976 300.6 579.9 826124 289.8 502.3 616332 216.2 382.7 436085 153.0 288.1 879482 238.3 480.7 778611 273.1 544.2 138361 48.5 95.8 153390 53.8 101.9 58263 20.4 39,9 72735 25.5 48.6 300856 105.5 196.6 233902 82.0 164.1 366818 128.7 232.7 117384 41.2 81.7 73689 25.8 48.9 186209 65.313 127.63S 2 : 309,0 calc pk CSPPM 133.1 250.8 284.7 460.4 188.9 372.9 40.3 77.2 172.7 326.5 27.7 46.5 298.9 449.7 325.8 628.7 313.9 544.2 232.9 412.3 163.3 307.5 257.3 519.0 295.6 589.0 .48.3 95.4 54.1 102.5 17,4 34,0 23.0 43.7 111.1 206.9 85.2 170.4 136.5 246.9 40.2 79.8 23.3 44.2 66.790 130.52G Or 456.0 S i 609.0 calc pk C8PPM calc pk C8 PPM 135.7 255.8 135.1 254.6 277.9 483.3 282.7 4917 196.0 386.9 197.7 390.2 35.5 68.0 31.1 59.6 178.6 337.5 179.6 339.4 21.9 36.8 17.0 28.6 314.8 473.7 3210 4 3 3 .0 343.9 663.5 3512 077.6 331.0 573.8 337.8 585.6 243.5 168.4 431.1 317.1 247.0 169.0 437.3 318.3 269.9 544.3 274,4 553.4 311.2 44.2 620.2 87.3 317,3 40.1 79.2 50.5 10.8 16.8 112.0 84.0 139.6 35.4 95.5 2 1 .1 32.0 208.6 168.' 252.2 70.3 46.6 6.6 117 110.5 815 , 139.0 31.0 88.3 10.7 22.3 205.8 163.0 2514 618 17,2 32.6 64.143 125.353 1 2 .1 60.839 23,0 118.895 Qi 19/ .1 1/ JL -1 .9 332.9 o o l .0 loo.o 2816 o4o .o 2 3 .0 1010 RQ A \O ,0 "/ .3 AR226-2090 RJZ042298 765.0 Qz 1000.0 0- 1508.0 0- 1713.0 0- 1788.0 2097.3 m 1981.5 m 1754,7 m 1662.1 m 1639.1 88929.4 b 120271.9 b 203748.1 b 241791.6 b 251744.0 1.0 Correlation 1.0 correlation 1.0 co irelatior 1.0 correlation 1.0 CALIBRATION C8PPM c a lc pk C8 PPM c a lc p k C8PPM c a lc p k C8 PPM c a lc pk C8PPM NAME 158.8 152.2 152.2 124.4 124.4 108.4 108.4 103.8 103.8 339.6 343.6 343.6 340.5 340.5 338.5 336.5 335.2 335.2 480.0 492.2 492.2 508.2 508.2 513.7 513.7 514.8 514.8 637.4 658.8 658.8 696.4 69a4 712.3 712.3 716.2 716.2 713.7 739.5 739,5 787.6 787.6 808.6 806.6 813.8 813.8 923.2 961.3 961.3 1038.0 1038.0 1073.0 1073.0 1082.0 1082.6 1239.6 1296.2 1296.2 1416.1 1416.1 1472.2 1472.2 1486.8 1486.8 1363.7 1427.6 1427.6 1564.5 1564.5 1828.8 1828.8 1645.6 1645.6 1446.3 1515.0 1515.0 1863.2 1663.2 1733.1 1733.1 1751.3 1751.3 1743.8 1829.8 1829.8 2018.7 2018.7 2108.4 2108.4 2131.9 2131.9 148.0 309.0 450.0 609.0 765.0 1000.0 1508.0 1713,0 1788.0 2275.0 7350 E765.0 C8PPM c a lc 241.6 St p k C8 PPM c a lc 119.9 225.9 k pk C8PPM c a lc 87.8 165.4 pk C8PPM c a lc 69.8 131.5 St 1788.0 SAM PLE pk C8PPM NAME 64.7 121.9 F P 1 505.7 291.9 507.7 282.1 490.6 274.9 478.1 27Z7 474.3 FP 2 389.1 192,8 380.6 170.1 335.9 156.7 309.4 152.8 301.8 F P 3 28.1 -1.4 -2.7 -49.1 -94.2 -74.8 -143.3 -81.9 -157.0 FP 4 334.9 171.7 324.6 146.3 276.6 131.6 248.8 127.4 240.8 FP 5 -3.1 -17.8 -29.9 -67.7 -113.6 -94.3 -158.4 -101.7 -170.8 FP 6 501.0 706.6 336.6 371,8 506,4 717,3 332.5 372.3 500.3 718.2 328.1 370.1 493.7 714.1 326.7 369.2 491.5 FP 7 712.4 FP 8 609,3 356,2 617.5 354.7 614.8 351.6 609.4 350.4 607.4 FP 9 445.2 250.3 443.2 235.1 416.2 225.3 398.9 222.4 393.8 FP 10 311.7 159.4 300.1 132.4 249.4 116.9 220.1 112.5 211.8 FP 11 567.9 282.2 569.2 271.1 546.8 263.3 531.1 261.0 526.3 FP 12 655.3 332.2 662.1 327.6 65Z9 323.0 643.6 321.4 640.6 FP 13 46.5 9.1 18.0 -37.3 -73.6 -62.2 -122.9 -69.2 -136.6 FP 14 5B.2 16.7 31.6 -28.7 -54.3 -53.2 -100.7 -80.0 -113.6 FP 15 -28.6 -31.3 -61.2 -82.9 -162.0 -110.4 -215.8 -118.0 -230.7 FP 16 -14.7 -24.0 45.7 -74.7 -142.1 -101.7 -193.6 -109.2 -207.9 FP 17 188.3 91.1 189.8 55.3 103.1 35.5 66.2 30.0 55.8 FP 18 138.2 57.3 114.7 17.2 34.4 -4.7 -9.5 -10.9 -21.8 FP 19 239.6 124,4 225.0 92.9i 168.0 75.2 136.0 70.2 127.6 FP 20 26.9 -1.5 -2.9 -49.2!

AR226-2606 [Andrew b Hartten ;" ii!

RECYCLED CD AR226-2687 AR226-2687 DuPont EMSE Report No. 18-02 Final Report Study Title Activated Sludge Respiration Inhibition Test of Telomer B 8-2 Alcohol (OECD 209) n.

AR226-2708 30 AR226-2708 American Society of Microbiology (ASM) Summary of DuPont Presentations Annual Meeting, 2004 Biotransformation Pathway(s) of the 14C-labeled Fluorotelomer 8-2 Telomer B Alcohol (8-2 TBA) in Acclimated Bacterial Culture Wang N .1, Buck R.C.3, Szostek B.2, Folsom P .

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AR226-2856 IFREB Institut Franais de Recherches et Essais Biologiques Centre de Lyon / Les Oncins IFREB ~ R 705221 EXEMPLAIRE N 3 PL 50 PAR VOIE ORALE CHEZ LE RAT TESTS DE TOLERANCE CHEZ LE LAPIN - INDICE 'IR R IT A T IO N OCULAIRE - IN D IC E D 'IR R IT A T IO N PRIMAIRE CUTANE Company Sanitized.