AR226-2809 DuPont-12988 TRADE SECRET Study Title H-24750: Static, Acute, 96-Hour Screening Test to Oncorhynchus mykiss Laboratoiy Project ID: DuPont-12988 A u t h o r s : Laurie D.

3M Company EPI-0027 Page 1 of 20 Final Report Epidemiology, 220-6W-08 Medical Department 3M Company St.

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3M 3M ENVIRONMENTAL LABORATORY PROJECT E05-0210; INTERIM REPORT #20 Interim Report #20: Analysis of Water Samples from Northern Alabama Potable Water Systems, February 2006 Study Title A n a lysis o f Per flu o r o b u ta n e s u lfo n a te (PFBS), Pe r flu o r o h e x a n e s u lfo n a te (PFHS), AND PERFLUOROOCTANESULFONATE (PFOS) IN WATER, SOIL, SEDIMENT, FISH, C la m s , V e g e t a t io n , S m all Ma m m a l Liver a n d S m all Ma m m a l S erum Usin g LC/MS/MS for the 3M Decatur Monitoring Program Data Requirement EPA TSCA Good Laboratory Practice Standards 40 CFR 792 Author Susan T.

ACUTE TOXICITY TO CHIRONOMUS TENTANS USING SPIKED SEDIMENT TEST SUBSTANCE_______________________________________________ Identity: Perfluorooctanesulfonate; may also be referred to as PFOS or FC-95. (1Octanesulfonic acid, 1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-heptadecafluoro-, potassium salt, CAS # 2795-39-3) Remarks: The test substance is a white powder.

3M General Offices 3M Center St.

Jean B.

P-1 Taft/ T a ft S te ttin iu s & H o lliste r LLP 4 2 5 W a ln u t S tree t, S uite 1 8 0 0 '' C in c in n a ti, OH 4 5 2 0 2 -3 9 5 7 / Tel. 5 1 3 .3 8 1 .2 8 3 8 / Fax; 5 1 3 .3 8 1 .0 2 0 5 / w w w .ta ftla w .c o m C incinnati / Cleveland / C olum bus / D ayton / Indianapolis / N orthern Kentucky / Phoenix / Beijing Ro be r t A.

INTERIM REPORT # 4 - Analysis of Surface Soil Samples STUDY TITLE Analysis o f Perfluorobutanesulfonate (PFBS), Perfluorohexanesulfonate (PFHS), and Perfluorooctanesulfonate (PFOS) in Water, Soil, Sediment, Fish, Clams, Vegetation, Small Mammal Liver and Small Mammal Serum Using LC/MS/MS for the 3M Decatur Monitoring Program DATA REQUIREMENTS EPA TSCA Good Laboratory Practice Standards 40 CFR 792 STUDY DIRECTOR Jaisimha Kesari P.E., DEE Weston Solutions, Inc. 1400 Weston Way West Chester, PA 19380 Phone:610-701-3761 .

INTERIM REPORT # 7-Analvsis of Soil Boring Samples STUDY TITLE Analysis of Perfluorobutanesulfonate (PFBS), Perfluorohexanesulfonate (PFHS), and Perfluorooctanesulfonate (PFOS) in Water, Soil, Sediment, Fish, Clams, Vegetation, Small Mammal Liver and Small Mammal Serum Using LC/MS/MS for the 3M Decatur Monitoring Program DATA REQUIREMENTS EPA TSCA Good Laboratory Practice Standards 40 CFR 792 STUDY DIRECTOR Jaisimha Kesari P.E., DEE Weston Solutions, Inc. 1400 Weston Way West Chester, PA 19380 Phone: 610-701-3761 INTERIM REPORT COMPLETION DATE October 27,2006 PERFORMING LABORATORY Exygen Research 3058 Research Drive State College, PA 16801 Phone: 814-272-1039 STUDY SPONSOR 3M Company 3M Building 0236-01-B-10 St.

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P-1 TSCADocument Processing Center Attn: Section 8(eVFYI yf fL 7 - 7 i- 3 7 3 S Attachment 2 p- 2 July 28,2006 Page 5 of 5 Axys Analytical Services Laboratory - Form 1A and Form 2 (2 pages) P-2 P-3 s r.......... 7 ' "r *'*.".* *'"' ______;______

Katherine E.