P ills b u ry W inthrop Shaw Pittm an^ srff January 5, 2006 > fi R 2300 N Street NW Washington, DC 20037-1128 rR 9-Si G _ Tel 202.663.8000 Fax 202.663.8007 www.pillsburyiaw.com ^ David E.

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INTERIM REPORT #27 - Analysis of Groundwater Samples STUDY TITLE Analysis of Perfluorobutanesulfonate (PFBS), Perfluorohexanesulfonate (PFHS), and Perfluorooctanesulfonate (PFOS) in Water, Soil, Sediment, Fish, Clams, Vegetation, Small Mammal Liver and Small Mammal Serum Using LC/MS/MS for the 3M Decatur Monitoring Program DATA REQUIREMENTS EPA TSCA Good Laboratory Practice Standards 40 CFR 792 STUDY DIRECTOR Jaisimha Kesari P.E., DEE Weston Solutions, Inc. 1400 Weston Way West Chester, PA 19380 Phone: 610-701-3761 INTERIM REPORT COMPLETION DATE February 9, 2007 PERFORMING LABORATORY Exygen Research 3058 Research Drive State College, PA 16801 Phone: 814-272-1039 STUDY SPONSOR 3M Company 3M Building 0236-01-B-10 St.

3M Specialty Materials 3M Center St.

3M ENVIRONMENTAL LABORATORY REPORT NO.

3M 3M ENVIRONMENTAL LABORATORY PROJECT E05-0210; INTERIM REPORT #20 Interim Report #20: Analysis of Water Samples from Northern Alabama Potable Water Systems, February 2006 Study Title A n a lysis o f Per flu o r o b u ta n e s u lfo n a te (PFBS), Pe r flu o r o h e x a n e s u lfo n a te (PFHS), AND PERFLUOROOCTANESULFONATE (PFOS) IN WATER, SOIL, SEDIMENT, FISH, C la m s , V e g e t a t io n , S m all Ma m m a l Liver a n d S m all Ma m m a l S erum Usin g LC/MS/MS for the 3M Decatur Monitoring Program Data Requirement EPA TSCA Good Laboratory Practice Standards 40 CFR 792 Author Susan T.

SEVERN TRENT LABORATORIES ANALYTICAL REPORT JOB NUMBER: 239579 Prepared For: Weston Solutions, Inc. 1400 Weston Way Building 5-2 West Chester, PA 19380-1499 Project: Confidential Decatur - FC Investigation Attention: Sue Stefanosky Date: 09/09/2005 Signature Name: Richard C.

Attachments to Letter to C.

Attachments to Letter to C.

ATTACHMENT TO LETTER TO C.

J M Oeneral Offices lTff JM Center St.

AR226-1030A039 BACK TO MAIN 3M Environmental Laboratory Report No.

ATTACHMENT TO LETTER OF JUNE 28, 2001 BACK TO COMPOUNDS 3M FLUOROCHEMICAL SUBMISSION TOXICOLOGY, EPIDEMIOLOGY AND MEDICAL SURVEILLANCE DOCUMENTS Click on Study Title to View Report COMPOUND-SPECIFIC STUDIES FOSA Perfluorooctanesulfonamide Pharmacokinetic 1.

BACK TO MAIN SOIL ADSORPTION TEST SUBSTANCE Identity: Perfluorooctanesulfonate; may also be referred to as PFOS or FC-95. (1Octanesulfonic acid, 1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-heptadecafluoro-, potassium salt, CAS # 2795-39-3) Remarks: The test substance is a white powder.

BACK TO MAIN STABILITY IN WATER (PHOTOLYSIS) TEST SUBSTANCE_______________ Identity: Remarks: N-ethylperfluorooctane sulfonamidoethanol; may also be referred to as N-EtFOSE alcohol. (1-Octanesulfonamide, N-ethyl-1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-heptadecafluoro-N-(2hydroxyethyl)-, CAS # 1691-99-2).