AR 226-035 SUMMARY OF HISTOPATHOLOGICAL EXAMINATIONS OF FATHEAD MINNOW (Pimephales promelas) EXPOSED TO 78.01 FOR 30 DAYS. p M - 3 V'Z"*-' RESEARCH REPORT SUBMITTED TO 3M COMPANY ST.

0710 BIODEGRADATION (BOD/COD) TEST SUBSTANCE Identity: A mixture containing perfluorooctanesulfonate, which may also be referred to as PFOS, FC-95, or as a component of FC-203. (1Octanesulfonic acid) (CAS # 2795-39-3).

A im & -0 0 0 7 2 14 Absorption of FC-95- C xn Rats After a Single Oral Dose October 26, 1979 Conducted at: During: Conducted by: Report by: Reviewed by: Riker Laboratories, Inc.

BACK TO MAIN Centre Analytical Laboratories, Inc. 3048 Research Drive State College, PA 16801 www.centrelab.com ^P h on e : (814)231 -8032 Fax: (814) 231 -1253or (814) 231 -1580 Analytical Report Fluorochemical Characterization of POTW Effluent Cleveland, Tennessee (W1973) Centre Analytical Laboratory Report No. 023-0141 (Revision 1) Revision Date 3/26/01 Testing Laboratory Centre Analytical Laboratory, Inc. 3048 Research Drive State College, PA 16801 3M Environmental Laboratory Contact Kent R.

ACUTE TOXICITY TO BLUEGILL SUNFISH TEST SUBSTANCE______________________________________________ Identity: Perfluorooctanesulfonate; may also be referred to as PFOS or FC-95. (1-Octanesulfonic acid, 1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8heptadecafluoro-, potassium salt, CAS # 2795-39-3) Remarks: The test substance is a white powder (3M Lot 583) of uncharacterized purity.

AR226-3375 HASKELL LABORATORY Common Nam e: Ammonium Perfluorooctanoate (C-8) Chem ical N am e: O ctanoic acid, pentadecafluoro-, ammonium salt CAS Registry N o.: 3825-26-1 Chem ical Structure: O v Physical Properties: CF3-CF2-CF2-CF2-CF2-CF2-CF2-C -0^ N H 4^ ;^ Form : M olecular W eight: B oiling Point: M elting Point: D en sity : W hite powder 431 /Sublimes @ 110C --- --- ' .; ' i; /^ Community Exposure Guideline 0.0003 m g/m 3 (24-hour TW A) General Toxicity Ammonium perfluorooctanoate (C-8) has moderate acute oral toxicity w ith an LD50 in rats o f 470 m g/kgJ I M ^ | l 98 lb ).

BACK TO MAIN BIODEGRADATION (Pure Microbial Cultures) TEST SUBSTANCE________________ Identity: Perfluorooctanesulfonate; may also be referred to as PFOS or FC-95. (1-Octanesulfonic acid, 1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8heptadecafluoro-, potassium salt, CAS # 2795-39-3) Remarks: The 3M production lot number was 217 (TN-A-2130).

AR RR6 - 0768 ACUTE TOXICITY TO AQUATIC INVERTEBRATES (DAPHNIA MAGNA) TEST SUBSTANCE________________________________________________ Identity: A mixture containing Perfluorooctanesulfonate, which may also be referred to as PFOS, FC-95, or as a component of FC-206A. (1Octanesulfonic acid) (CAS # 2795-39-3).

AKA.a.6 . 0 6 3 0 ACUTE TO XIC ITY TO FISH TEST SUBSTANCE_______________________________________________ Identity: A mixture containing perfluorooctanesulfonate, which may also be referred to as PFOS, FC-95, or as a component of FC-201. (1Octanesulfonic add, perfluoroalkyl sulfonate salts (5) + (5140P)) (CAS # 2795-39-3) Rem arks: The 3M production lot number was Lot 1.

ARX&-0370 SOIL ADSORPTION TEST SUBSTANCE Identity: N-methylperfluorooctane sulfonamldoethanol; may also be referred to as N-MeFOSE Alcohol, FC-790, or FM-3925. (1Octanesulfonamide, N-methyl-1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8heptadecafluoro-N-(2-hydroxyethyl)-, CAS # 24448-09-7) Remarks: Material is an off-white, waxy solid.

T- 3 ?

AR226-1974 > ss VQ!

/\RXl(rOl93 Submitted to : BIO SEA RC H , INC.

A h * 2.6 - 0 7 S Z ACUTE TOXICITY TO FISH (RAINBOW TROUT) TEST SUBSTANCE_______________________________________________ Identity: A mixture containing perfluorooctanesulfonate, which may also be referred to as PFOS, FC-95, or as a component of FC-206 or L3243. (1-Octanesulfonic acid) (CAS # 2795-39-3).

B IO D EG R A D A T IO N (301E) TEST SUBSTANCE Identity: A mixture containing perfluorooctanesulfonate, which may a lso be referred to a s P F O S , FC -95, or a s a com ponent of FC -3017. (1Octanesulfonic a d d ) (C A S # 2795-39-3).