ARllt-03G6 Attached are comments on the 3M Technical Report "Analytical Methodology and Support.

CHRONIC TOXICITY TO FISH TEST SUBSTANCE Identity: Perfluorooctanoic acid, ammonium salt; may also be referred to as 78.03, PFOA ammonium salt, Ammonium perfluorooctanoate, PFO, FC-116, FC-126, FC-169, or FC-143.

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/H U 7 t03M3> BIOACCUMULATION TEST SUBSTANCE Identity: N-Ethylperfluorooctanesulfonamide; may also be referred to as U1464, EtFOSA, EtPOSA, F-6309, or FX-12. (1Octanesulfonamide, 1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8heptadecafluoro-N-ethyl-, CAS # 4151-50-2) Remarks: Material is a white solid of uncharacterized purity.

ft R W 6 - O M H 5 SrtduAfoud BIO-TEST laJymJjwM,, She. 1810 F R O N T A G E R O A D N O R TH B R O O K .

0710 BIODEGRADATION (BOD/COD) TEST SUBSTANCE Identity: A mixture containing perfluorooctanesulfonate, which may also be referred to as PFOS, FC-95, or as a component of FC-203. (1Octanesulfonic acid) (CAS # 2795-39-3).

AfLza.G _ 0274 ACUTE TOXICITY TO FISH (FATHEAD MINNOW) TEST SUBSTANCE_________________________________________ Identity: A mixture containing perfluorooctanesulfonate, which may also be referred to as PFOS, FC-95, or as a component of FC-780B. (1Octanesulfonic acid) (CAS # 2795-39-3).

M S.a.6 - 0& 7.

A k SUL6 - 0 7 9 5 SUMMARY FOR WORK PERFORMED FOR THE GERMAN GOVERNMENT AGENCY FOR MILITARY TECHNOLOGY AND PROCUREMENT ON FIRE EXTINGUISHING FOAM COMPOUNDS FROM MULTIPLE COMPANIES TEST SUBSTANCE________________________________________________ Identity: A mixture containing Perfluorooctanesulfonate, which may also be referred to as PFOS, FC-95, or as a component of FC-206. (1 -Octanesulfonic acid) (CAS # 2795-39-3).

Interoffice Correspondence H.E.

M AS.6 - 0788 ACUTE TOXICITY TO AQUATIC INVERTEBRATES (SCUD) T EST SUBSTANCE___________________________________________ __ Identity: A mixture containing perfluorooctanesulfonate, which may also be referred to as PFOS, FC-95, or as a component of FC-206 or L3243. (1-Octanesulfonic acid) (CAS # 2795-39-3).

R K i-O II ACUTE TOXICITY TO FISH TEST SUBSTANCE Identity: Perfluorooctanesulfonate, Ammonium salt; may also be referred to as PFOS NH4+ salt or FC-93. (1-Octanesulfonic acid, 1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-heptadecafluoro-, ammonium salt, CAS #29081-56-9) Remarks: Test sample was taken from 3M production lot #1.

Covance Studies The attached report summarizes the results from the assessment of mitochondrial bioenergetics of hepatic mitochondria isolated from rats treated for 3 weeks with one of 4 doses (plus control) of dietary FC10.

M 6_ 0737 MICROBIAL INHIBITION (DEHYDROGENASE ACTIVITY) TEST SUBSTANCE__________________________ Identity: A mixture containing perfluorooctanesulfonate, which may also be referred to as PFOS, FC-95, or as a component of FC-206A. (1Octanesulfonic acid) (CAS # 2795-39-3).

nc-oio-j CHRONIC TOXICITY TO EARLY LIFE STAGE OF FISH TEST SUBSTANCE Identity: Perfluorooctanesulfonate; may also be referred to as 14C78.02, PFOS or FC-95. (1-Octanesulfonic acid, 1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-heptadecafluoro-, potassium salt, CAS #2795-39-3) Remarks field: The test substance is a white powder.