AR226-3166 ____________________ ____________________________ DuPont-4182 TRADE SECRET Study Title H-24159: Biopersistence Screening 10-Dose Oral Gavage Study in Rats Laboratory Project ID: DuPont-4182 Author: Carol Finlay, B.A.

f i k k U . in s ' 497 Supplement 1 DuPont-11418 TRADE SECRET Study Title H-25425: Subchronic Toxicity 90-Day Gavage Study in Rats with One-Generation Reproduction Evaluations Supplement 1 Laboratory Project ID: DuPont-11418 Te st Gu idelin es: U.S.

AR226-3346 Environmental Fate Studies of Fluorotelomer Intermediates and Fluorotelomer-based Surfactants and Polymers W.R.

36a 2 ADDENDUM NUMBER 1 TO THE SECOND SEMIANNUAL PROGRESS REPORT FLUOROCHEMICAL (FC) SITE RELATED ENVIRONMENTAL ASSESSMENT PROGRAM 3M COTTAGE GROVE, MN FACILITY March 2006 Prepared for 3M Company fiy WESTON SOLUTIONS, INC.

B 1100 AR226-3646 M M IIIH iH AtASSCH sm B1 1000 900 J& S 5 Glenwood Shale S t.

3M tipp. 3M Center St.

Jean B.

P-1 Taft/ Taft Stettinius & Hollister LLP 425 W alnut Street.

SEVERN TRENT LABORATORIES ANALYTICAL REPORT JOB NUMBER: 245781 Prepared For: Weston Solutions, Inc. 1400 Weston Way Building 5-2 West Chester, PA 19380-1499 Project: Confidential Decatur - FC Investigation Attention: Jai Kesari Date: 04/21/2006 Signature Name: Richard C.

AK.PA6 _ o7ll BIODEGRADATION (301E) TEST SUBSTANCE________________________________________________ Identity: A mixture containing perfluorooctanesulfonate, which may also be referred to as PFOS, FC-95, or as a component of FC-203. (1Octanesulfonic acid) (CAS # 2795-39-3).

V j-R _ O l S NITRIFICATION INHIBITION TEST SUBSTANCE______________________________________ Identity: Mixture containing perfluorooctanesulfonate, which may also be referred to as PFOS, FC-95, or as a component of FC-203CF-X or FC-203CF. (1-Octanesulfonic acid) (CAS # 2795-39-3).

M AS.6 - 0788 ACUTE TOXICITY TO AQUATIC INVERTEBRATES (SCUD) T EST SUBSTANCE___________________________________________ __ Identity: A mixture containing perfluorooctanesulfonate, which may also be referred to as PFOS, FC-95, or as a component of FC-206 or L3243. (1-Octanesulfonic acid) (CAS # 2795-39-3).

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if VsSb- V-. * 4 P R O l^ t4sa>_ M f.lt UNITED STATES ENVIRONMENTAL PROTECTION AGENCY WASHINGTON, D C. 20460 DEC - 9 2002 OFFICE OF PREVENTION; PESTICIDES AND TOXIC SUBSTANCES Dear Interested Party: eMMdo2a7xnet50hoacfd0pierlnn3uicredme,hdrmadfaeayl,1nAadgu,1lndiootuD,nutrpwsag2foeerca,0acoshcv0ale.mtkeos2muTdlyu)ruwh.blelpmegeTesloaleruefhlrtai,l9eenafisc,omssaefo2nlitunpnfh0arsitoaue0tnreerllo2dtesarl(uuols(aPre6plfneFade7pqtnAehleueFeleixxSiemnRrscpc)etelteeoscu7rcrnsohds2mhutnueea8eremibsle5mcdmp4fiuiicrcr)acsioo.oasteameplpsTslsisoyh,otitosnaiwnhoesfpesfdhotfreetdifiorhrmcneuadehDafliuliescfpenciroicugpienuntenbuailcdmoeilblhfuinlisSbbecichmseoeitagoehcrfnindroec3"tidmmas1ifnnlii,eesaegc2watnsansh0runioel0efuftilfi2easeFfcNrcee.layetectnundhwttfiroeiovenstrUr,eieaycowasleoenveRan(eiurRaSeJsotg(Naeui6ofin"lUs7entutshNeaF(phorSr)eRysyNocedfino8r1Ufa,ri1ucR0aaln1)ilcly4oys,,n tpeeEaschuoasnanetrbrpdvaltmiNiibieeeerlsnoirosisstnnposseEh-mihufrCeoiabgttdenohshmhnsenoeettsistflatpdheietlodeacorfPdoedtrcrttnourkoihloetcageniitsutshateiecmlsoncrucuutIudeionbltmoonemfmtncmtohbskmirAeetamentrekertgon,auidOetnttOlnisegaPtoi.cPvmPmnpyAaPTraeiCTowllk-llac2ye-ieob2ne0nbclfe0g0teosedt02ihmtriet2h-neeli0-maesgn0a0tec,e0t4ttwhcncr4w3oaoete3.swnnmr.ETeoiwbYmcPhnmea.eAoeeltafunlhpdoydDteaoucset.

r AG Fluoropolymers ASAHI GLASS FLUOROPOLYMERS USA, IMG AA8.