y/l AA - 3JLO DuPont-11418 M UC- &O TRADE SECRET Study Title H-25425: Subchronic Toxicity 90-Day Gavage Study in Rats with One-Generation Reproduction Evaluations Volume 5 of 5 Laboratory Project ID: DuPont-11418 Test Guidelines: U.S.

A R A M - 34-^0 o 44 000399 .WASHINGTON WORKS TEFLON DIVISION 4RJ& - W f September 28, 1982 TO: R.

Afua.6- ltflf. 9 v M i * 68 000652 Job Code 8PE 08PF 08PH 08PI 08PJ 08PM 18PA 18PB 18PC 18PD 18PJ 18PK M echanics 1984 6.4 3.5 0.8 1.3 0.8 2.5 0.9 Average for Job 1985 1989-1990 4.9 4.4 3.2 2.2 2.4 0,7 0.4 1A 0,1 0.6 0.9 2.7 0.5 1.1 0.1 0.4 1995 2.5 2.9 1.7 2.0 0.5 1.7 2.3 1.6 3.3 0.1 0.7 2.1 1.0 ARX26- W q- i11rlii 000SS3

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Name: Carine Sakr, MD MPH 1 Robin Leonard, PhD 2 Mark Cullen, MD 1 R 6_ 36-^7 Program Affiliation: '"Yale Occupational and Environmental Medicine Program 2"Epidemiology Program at DuPont Haskell Laboratory for Health and Environmental Sciences Address: 135 College Street, 3rd floor New Haven, CT 06510 Phone: 856-816-1539 Fax: 203-785-7391 Email: carine.sakr @vale.edu TITLE Twenty-five year longitudinal study of serum total cholesterol related to a serum biomarker of exposure (serum perfluorooctanoate or PFOA) in a polymer production plant.

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Katherine E.

P-1 A ZZZ Q jm DuPont Haskell Global Centers for Health and Environmental Sciences ( f 1090 Elkton Road, P.O.

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Quantify Sample Report MassLynx 4.1 PFOA Analysis Dataset: C :\Mass Lynx\P FOA.

INTERIM REPORT # 9-Analvsis of Ground Water Samles STUDY TITLE Analysis of Perfluorobutanesulfonate (PFBS), Perfluorohexanesulfonate (PFHS), and Perfluorooctanesulfonate (PFOS) in Water, Soil, Sediment, Fish, Clams, Vegetation, Small Mammal Liver and Small Mammal Serum Using LC/MS/MS for the 3M Decatur Monitoring Program DATA REQUIREMENTS EPA TSCA Good Laboratory Practice Standards 40 CFR 792 STUDY DIRECTOR Jaisimha Kesari P.E., DEE Weston Solutions, Inc. 1400 Weston Way West Chester, PA 19380 Phone: 610-701-3761 INTERIM REPORT COMPLETION DATE January 9,2007 PERFORMING LABORATORY Exygen Research 3058 Research Drive State College, PA 16801 Phone: 814-272-1039 STUDY SPONSOR 3M Company 3M Building 0236-01-B-10 St.

y \ / U U . 06SI Life Cycle Waste Stream Estimates \j\JW August 2000 Ac3eChnMytattciartlmacleechadtWened"ruaiSfizssauetecalftanuSonrntediraxneetegaescmdtauinmtPEidevasretstfeiulmsuptuhoapmertleoymfscl"cuha,hroeydamriaonoitccefhfadaaelcsmAri:elpiipctUrioaiel.lrsSt2c.pa1oRnr,nede2tpel0faenr0raot0esmod.efbETppyrshootetBidemonauatbtctitjteaeellucl-eswtaivM1age9sete9.eom7fsoPtthrraeiiraastlmw1In:sosfrLtrkioitfuwmet-aebsototh huueEoFsonnifstrwdatiwsimvetme,aravatsaoiatetltpeeakrees,bescrin3auailMnitstwtotsytorauhhmospeeatfpxeseralpreyimnepmaarcnoiilpnhedrylitantemeiricmcnenieazfdefllaonaeutdrctciseaioeteldtnnicartgo.ismweiingnsSaseneeseaaeitrcsnfervuoidicanrnstaet3gdirnsvM,ejteuaatmh,smdmewgpaavmrnaoneorurueptslfunfotaoamtcrcfsctta3teurosusMerefr.iltinieaIn'egnsnsgsspptauolhrrormnoeoecdcpay1uuette9siiscaeoo9strd7nnssissmtdsseaiauupwnlbeberaoossstreuovedfvtqeistegtmuhhhrueeiaeeprnlnetgrpsteestrotsnooapegn1err9dcaa9ttmhsi7o.a,.ns pmcsrceptfmTsFiherntuuoxhrrihouseoonrlnpuoteumfcrldeacectyoeelhorwlulcttennclmuuhsltcylautyaaesryetrssetlsidssdsadeehvtsi.isaonerdssnode.todfbPawetTsspwleh"igttFymexohsruPahtrsOurepaehdatoFifiagscsecdaSilwsOmeeu,cgrhtatisuoopeeSttmsi,iihmesrqmuhttoorPtseeauloswunupdtcqFntiticlhovoamutatOoabt.hrealsiuthfeytaSvelmTiareysvotsraefnheoneiphietlosscstehletoarld,h(asienhysmitsn.ealonhrat,)nssepreevpfTt"rodlPsrchbbereu.hoiteoFieipsaomsiodlbleOsfrio"rtudenmetruohPgeSeceesiccarFniipstgenchnhtaonoOcraaaeadntaodtrnhliSmrdedt"nmidtyestfwhaadiesrpefprtecrfeeeciqoieeeialclortnwceursamleaebnsiidstitdtnedeetvaeaii-tmsituonsdaotcagd.eepanglsaeheecrdlPrsscgittanooeFabhhcoromtp"ldraaOasanseef"nedtlpaSralwCgtiasPotikhs.iisstruF8imneiesaulondRFsOltdmdsaonde1paet.Ssofshpthlq7soiwiaetnuououSafiItnnoemrntienn0tovedhnsds2cppalete.udeyaoiltroprllteiszofmIfogonrslhenodtuoencphypnuttsoerflhoedhtaiceaesrhberototnctmceoaaeettctiaas,tonldlnahsyiyrlreynsibseyisaenasntumoinsdcoacsmtoxiyeethhisphPaycnfg,parnealFPtrotttaadlhiOFsrdttodeteheOuunSapecdtSoyoityo.irfnatnre 3 Final Report Sulfonated Perfluorochemicals: U.S.

Ad a.a.6 - 0768 BIODEGRADATION (BOD/COD) TEST SUBSTANCE_______________________________________________ Identity: Mixture containing perfluorooctanesulfonate which may also be referred to as PFOS, FC-95, or as a component of FC-203FC. (1Octanesulfonic acid) (CAS # 2795-39-3).

-M A 2 6 - 0770 ACTIVATED SLUDGE RESPIRATION INHIBITION TEST T E S T SUBSTANCE__________________________________________________ Identity: Mixture containing perfluorooctanesulfonate which may also be referred to as PFOS, FC-95, or as a component of FC -203FC . (1Octanesulfonic acid) (CAS # 2795-39-3).

AR x a 6 - O g J-6 ACUTE TOXICITY TO FISH (FATHEAD MINNOW) JE ST.SUBSTANCE_________________________________________ Identity: A mixture containing perfluorooctanesulfonate, which may also be referred to as PFOS, FC-95, or as a component of FC-600. (1-Octanesulfonic acid, 1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8heptadecafluoro-, potassium salt, CAS # 2795-39-3) Remarks: The 3M production lot number was not noted.