Haskell Laboratory for Toxicology and Industrial Medicine January 4,2002 AR226-3215 TO: ( Milot Developmental Toxicity Study in Rats cc: L.

3M Environmental Laboratory FinalReport-AnalyticaSltudy Single-DoseIntravenousPharmacokineticStudy ofT-6053 inRabbits In-VivoStudyReferenceNumber: HWI#6329-136 Study Number: AMDT-010495.1 TestSubstance:FC-99 (T-6053) Name and AddressofSponsor: 3M SCD Division 367 Grove Street St.Paul,NIN 55106 Name and Address ofTestingFacility: 3M EnvironmentalTechnology& Services 935 Bush Avenue St.Paul,MN 55106 Method Numbers AMDT-M-1-0, AMDT-M-2-0, AMDT-M4-0, AMDT-M-5-0, AMDT-M-8-0, and Revisions: Thermal ExtractioonfFluorideby Means of a Modified Dohnnann DX2000 OrganicHalideAnalyzer-Liver FluorideMeasurement by Means ofan Orion EA940 Expandable Ion Analyzer ExtractionofFluorochemicalsfrom RabbitLiver Analysisof RabbitLiverExtractforFluorochemicalsUsing ElectrospmyMass Spectrometry Analysisof FluorideUsing the SkalarSegmented Flow Analyzer with Ion SelectivEelectrode InitiatioDnate: See attachedprotocol Author:James D.

Dr.ChadesReich ExecutiveVice President December 15,2000 3M SpecialNtbyterial Mw*ets 3M CenterB,uilding220 St.Paul,MN 55144-1000 6517330439 651575 8001 Fax CERTIFEED NUIL Document ProcessingCenter(7407) ATTN: Section8(e)Coordinator OfficeofPollufioPnrevenfionand Toxics US EnvironmentalProtecfioAngency 401 M Strea@SW_ Washington,DC 20460 Re: TSCA 8(e)NoticeforPerfluorooctanSeulfonylFluoride-basePdroductionProcesses Dear Sir: PursuanttoSection8(e)oftheToxic SubstancesControlAc@ 3M isreportingthedraftresults of an updateof a retrospecticvoehortmortalitsytudyofworkersattheDecatur,Alabama manufacturingfacilityT.he studyupdatewas performedby theUniversityof Mnnesota!

p. 1 ~-~,ata6~ ~687 INTERIM REPORT #23 Analysis of Sediment Sample s STUDY TITLE Analysis of Perfluorooctanoic Acid (PFOA) in Water, Soil, Sediment, Fish, Clams, Vegetation, Small Mammal Liver and Small Mammal Serum Using LC/MS/MS for the 3M Decatur Monitoring Progra m DATA REQUIREMENTS EPA TSCA Good Laboratory Practice Standards 40 CFR 792 STUDY DIRECTOR Jaisimha Kesari P .E., DEE Weston Solutions, Inc. 1400 Weston Way West Chester, PA 19380 Phone: 610-701-376 1 MERIjVI REPORT COMPLETION DATE May 2, 2006 PERFORMING LABORATOR Y Exygen Research 3058 Research Drive State College, PA 1680 1 Phone : 814-272-1039 STUDY SPONSOR 3M Company 3M Building 0236-01-B-10 St.

INTERIM REPORT #22 - Analvsis of Soil Samples STUDY TITLE Analysis of PerfluorooctanoicAcid (PFOA) in Water, Soil, Sediment, Fish, Clams, Vegetation, Small Mammal Liver and Small Mammal Serum Using LCMSMS for the 3M Decatur Monitoring Program DATA REQUIREMENTS EPA TSCA Good Laboratory Practice Standards 40 CFR 792 STUDY DIRECTOR Jaisimha Kesari P.E., DEE Weston Solutions, Inc. 1400 Weston Way West Chester, PA 19380 Phone: 610-701-3761 INTERIM REPORT COMPLETION DATE September 22,2006 PERFORMING LABORATORY Exygen Research 3058 Research Drive State College, PA 16801 Phone: 814-272-1039 STUDY SPONSOR 3M Company 3M Building 0236-01-B-10 St.

"McCrea, Deborah" <mccrea@taftlaw .com> 10/30/2009 12 :15 PM To cc bcc Subject NCICOPPT@EPA P "Bilott, Robert A."

spf Sa {N773 2per MR 54374 UNITED STATES ENVIRONMENTAL PROTECTION AGENeY AR226_ 1093 WASHINGTON, D.C. 20460 AR 2E np Dear Interested Party: On March 28, 2002, EPA made available copies in PDF file format (389KB)ofthe Draft aHnwasazsraaermdtehAntststeiDsssimdieoincotunmOefonPftertifnlcEulPourdAoeodfcatenaneroioocrfAPcionildhlue(tPitFoonOxAPa)rpepAveenandrtiiInotsgnSoaannltdsp,Tagoperwea8p.aireEsdPecbAtyihotanhse2bR0iescokfomtehe document, "Production of PFOA and its Salts."

commen Ger aria Le Rao5sr1einvar4e.snBe3oa0rme TAFT, STETTINIUS & HOLLISTER LLP 425 WALNUT STREET, SUITE 1800 CINCINNATI, OHIO 45202-3957 eaxa Sissaratos wwtata com ARL26 -- aol iE sSuommsEmnee a 1187 October 25. 2002 TELECOPY AND REGULAR US.

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Telomer Research Program AR226-1424 Report Title: 1-Decanol, 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoroFish (Zebrafish), Acute Toxicity Test, Static, 96h, Limit Test with the Saturated Solution RECEIVED OPPT NCIC 2003 July 18 12:00PM Author(s): Dirk Scheerbaum Contractor: Dr.

AR226-1433 DR.U.NOACK-LABORATORIUM FR ANGEWANDTE BIOLOGIE 1-Decanol, 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10heptadecafluoro- Terrestrial Plants Toxicity, Seedling Emergence according to OECD Guideline 208 (Draft July 2000) Sponsor Telomer Research Project ASAHI GLASS CLARIANT DAIKIN INDUSTRIES LTD DUPONT RECEIVED OPPT NCIC 2003 July 18 1:09PM Author Silke Fiebig Test Facility DR.U.NOACK-LABORATORIUM FR ANGEWANDTE BIOLOGIE Kthe-Paulus-Str. 1 D-31157 Sarstedt Laboratory Project ID Project-No. 020719CK Study-No.

AT3TMACFHLMUEONRTOCTHOELMEITCTAELRSOUFBMMIaSySI1, 2ON008 BIBLIOGRAPHY OF PUBLISHED LITERATURE AElmepxlaonydeeersBoHf,a OPlesrefnluGorWo,ocBtuarnreissulJpMh,onMyalndFleulorJiHd,eaMnadnuMfaancdteulriJnSg(F2a0c0i3l)i.ty.MoOrctcaulpi.tyEonfviron Md. 60:722-729.