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GLP10-01-02: Interim Report 26 - Analysis of PFBS, PFHS, and PFOS in Surface Water Samples Collected at Bert Jeffries Landfill in Decatur, AL in February 2012 Study Title Analysis of Perfluorooctane Sulfonate (PFOS), Perfluorohexane Sulfonate (PFHS) and Perfluorobutane Sulfonate (P FBS ) in G roundwater, Soil and Sedim ent fo r the 3M D ecatur Phase 3 Site-Related Monitoring Program Data Requirement EPA TSC A Good Laboratory Practice Standards 40 CFR Part 792 Study Director Jaisim ha Kesari P.E., DEE W eston Solutions, Inc. 1400 W eston W ay W est Chester, PA 19380 Phone: 610-701-3761 A u th o r Susan W olf 3M Environm ental Laboratory Interim Report Com pletion Date Date of signing Perform ing Laboratory 3M Environmental Health and Safety Operations Environmental Laboratory 3M Center, Bldg 260-05-N-17 St.

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BAKT MAIN 3M Environmental Laboratory BaciCopyof wtaBHaHv r SJlOO M ethod D e t e r m in a t io n o f P e r fl u o r o o c t a n e SULFONATE (PFO S), P e r f l u o r o o c t a n e SULFONYLAMIDE (PFO SA ), AND PERFLUOROOCTANOATE (POAA) IN WATER BY LlQUIDSo u d E x tr a c tio n and H ig h -P e r fo r m a n c e L iq u id C h ro m a to g ra ph y /T a n d em M a ss Sp e c t r o m e t r y (H PLC/M S/M S) M ethod N um ber: ETS-8-154.0 A doption Dote: / looq A uthor: K risten J.

ENVIRONMENTAL PHYSICAL/CHEMICAL, FATE, EFFECTS AND MONITORING STUDIES COMBUSTION BACK TO COMPOUNDS STUDY TITLE LABORATORY OR DATE AUTHOR COMPLETED TYPE Environmental Fate and Transport Executive Summary Flurochemical Decompostion Processes.

Quality Assurance Project Plan Multi-City Study Sampling Task (N100672) BACK TO MAIN Amendment 2 to Revision No.: 1 Effective Date: July 20, 1999 Page 1 o f \ l Amendment 2 to the Quality Assurance Project Plan and Associated SOP's for Empirical Human Exposure Assessment Multi-City Study Sampling Task To July 23,1999 Prepared by Battelle Marine Sciences Laboratory 1529 West Sequim Bay Road Sequim, WA 98382 360-681-3660 APPROVALS 3 ifd Gunster Sampling Task Leader Rosanna Buhl Battelle Sampling Task QA Officer 3 * 1 QMA* tjtyL de'----- --- ^ MMaarrcciaNishiolra y ^ Buaaititcenllce rPiruojjceucat iMvianuagceir 0 ^ u s a n Abogy Battelle Program QA Officer ___ jz iii Date 7 8-a~7-qq Date j/so /o / Date ns#5 *>/ **,+ < * * 1 ^ Date -f S y - t.