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Telom er Research Program AR226-1423 Report Title: 1-Decanol, 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoroAcute Immobilisation Test (48h) to Daphnia magna STRAUS Limit Test with the Water Accommodated Fraction (WAF) Author(s): Martina Noack RECEIVED OPPT NCIC 2003 July 18 12:00PM Contractor: Dr.

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PERFLUOROOCTANESULFONATE, POTASSIUM SALT (PFOS): A FLOW-THROUGH BIOCONCENTRATION TEST WITH THE BLUEGILL (Lepomis macrochirus) FINAL REPORT WILDLIFE INTERNATIONAL, LTD.

Group Summary P Generation Group Group 1 Group II Group III Group IV Group V NUMBER OF DAYS OF DATA COLLECTION NUMBER OF DAYS IN ESTRUS % OF DAYS IN ESTRUS 21 g 43% 21 8 41% 21 9 42% 21 8 39% 21 9 42% NUMBER OF DAYS IN % OF DAYS DIESTRUS IN DIESTRUS NUMBER OF % OF DAYS DAYS IN IN PROESTRUS PROESTRUS 9 41% 9 45% 9 45% 10 45% 9 43% 3 16% 3 14% 3 13% 3 15% 3 15% "N" FOR MEAN CYCLE MEAN CYCLE NUMBER OF LENGTH LENGTH CYCLES 30 4.3 4.6 30 4.0 4.6 28 4.1 4.3 30 4.3 4.4 29 4.1 4.6 P Generation nimal I 13801 13802 13803 13804 13805 13806 13807 13808 13809 13810 13811 13812 13813 13814 13815 13816 13817 13818 13819 13820 13821 13822 13823 13824 13825 13826 13827 13828 13829 13830 13831 13832 13833 13834 13835 13836 13837 13838 13839 13840 13841 13842 13843 13844 13845 13846 13847 13848 13849 13850 Group 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 MEAN CYCLE LENGTH 3.75 3.20 3.75 3.67 3.75 5.33 4.00 4.25 4.25 4.25 4.50 9.00 4.00 5.00 5.00 4.33 4.00 4.00 4.00 4.00 4.25 4.00 4.00 3.40 4.67 3.75 4.25 3.75 4.00 4.00 3.67 4.25 4.00 3.75 4.00 4.00 4.00 4.50 3.75 4.33 3.75 4.00 4.25 3.75 4.00 4.00 4.00 4.00 4.00 4.25 NUMBER OF CYCLES 5.00 6.00 5.00 4.00 5.00 3.00 5.00 4.00 5.00 5.00 4.00 2.00 5.00 4.00 4.00 5.00 5.00 5.00 5.00 4.00 5.00 5.00 5.00 6.00 5.00 5.00 5.00 4.00 4.00 5.00 5.00 5.00 5.00 5.00 5.00 2.00 5.00 2.00 5.00 5.00 4.00 4.00 5.00 4.00 4.00 5.00 4.00 5.00 5.00 6.00 13851 13852 13853 13854 13855 13856 13857 13858 13859 13860 13861 13862 13863 13864 13865 13866 13867 13868 13869 13870 13871 13872 13873 13874 13875 13876 13877 13878 13879 13880 13881 13882 13883 13884 13885 13886 13887 13888 13889 13890 13891 13892 13893 13894 13895 13896 13897 13898 13899 13900 13901 13902 CO CO CO P Generation 2 3.25 6.00 2 3.75 5.00 2 4.00 4.00 2 4.00 5.00 2 3.75 5.00 2 3.75 4.00 2 4.50 4.00 2 4.00 5.00 2 3.80 5.00 2 4.25 5.00 3 5.00 3.00 3 3.75 5.00 3 4.00 5.00 3 4.67 4.00 3 4.00 4.00 3 4.67 3.00 3 4.00 5.00 3 3.75 5.00 3 4.00 5.00 3 4.00 4.00 3 3.75 5.00 3 3.75 5.00 3 4.00 5.00 3 5.00 3.00 3 4.00 4.00 3 3.75 4.00 3 4.25 4.00 3 4.25 5.00 3 4.00 6.00 3 4.00 4.00 3 5.00 4.00 3 4.00 5.00 3 3.75 5.00 4.00 5.00 #DIV/0!

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BACK TO MAIN 3M FLUOROCHEMICAL SUBMISSION TOXICOLOGY, EPIDEMIOLOGY AND MEDICAL SURVEILLANCE August 2005 Click on Study Title to View Report August 12, 2005 Analytical Report, "Initial Quantitative Screening of Commercial Lots of Human Se rum Obtained in 2004 for Endogenous Fluorochemicals Using Protein Precipitation and Liquid Chromatography/Tandem Mass Spectrometry," 3M Environmental Laboratory, Project No.

/IfttiG -cm R OCTANOUW ATER PARTITION COEFFICIENT TEST SUBSTANCE_____________________________________________________ Identity: N-ethylperfluorooctane sulfonamidoethanol; may also be referred to as N-EtFOSE Alcohol or FM-3422. (1-Octanesulfonamide, N-ethyl1 ,1 ,2 ,2 ,3 ,3 ,4 ,4 ,5 ,5 ,6 ,6 ,7 ,7 ,8 ,8 ,8 -h e p ta d e c a flu o ro -N -(2 -h y d ro x y e th y l)-, CAS # 1691-99-2) Rem arks: Material is an off-white, waxy solid.

A R # 6- o m it ACTIVATED SLUDGE RESPIRATION INHIBITION TEST TEST SUBSTANCE Identity: [2-(N-Ethylperfluorooctanesulfonamido) ethyl acrylate: may also be referred to as B1228, D-1, EtFOSEA, or FX-13. (2-Propenoic acid, 2[ethyl[heptadecafluorooctyl)sulfonyl]amino]ethyl ester, CAS # 423-825) Remarks: Material is an amber solid.

Aime-wR 3M Company EPI-0003 Page 1 of 25 FINAL REPORT Epidemiology Medical Department 3M Company 220-3W-05 St.

CHRONIC TOXICITY TO FISH TEST SUBSTANCE Identity: Perfluorooctanoic acid, ammonium salt; may also be referred to as 78.03, PFOA ammonium salt, Ammonium perfluorooctanoate, PFO, FC-116, FC-126, FC-169, or FC-143.

ACTIVATED SLUDGE RESPIRATION INHIBITION TEST SUBSTANCE Identity: Perfluorooctanoic add, ammonium salt; may also be referred to as PFOA ammonium salt, Ammonium perfluorooctanoate, PFO, FC116, FC-126, FC-169, orFC-143.