M 236 - O 77#- ACUTE TOXICITY TO FISH (FATHEAD MINNOW) TEST SUBSTANCE___________________________________________ _ Identity: Mixture containing perfluorooctanesulfonate which may also be referred to as PFOS, FC-95, or as a component of FC-203FC. (1Octanesulfonic acid) (CAS # 2795-39-3).

M & a .G - O l Z BIODEGRADATION (BOD/COD) TEST SUBSTANCE________________________________________________ Identity: A mixture containing perfluorooctanesulfonate, which may also be referred to as PFOS, FC-95, or as a component of FC-603F. (1Octanesulfonic acid) (CAS # 2795-39-3).

#. i - / 3/z Tom Cortina <cortina@alcaIde-fay.com> on 04/30/2003 11:02:02 AM Please respond to Tom Cortina <cortina@alcalde-fay.com> To: oppt.ncic@epamail.epa.gov cc: Mary Dominiak/DC/USEPA/US@EPA Subject: Submission to AR 226 April 30, 2003 SUBJECT: Submission to AR 226 Attached is an overview of the mechanics of film formation of aqueous film-forming foam (AFFF) fire fighting agents.

AA 6 - TSCA NCIC Notification Form for CBI Documents Docket Number: fl-'fi ____________ Document Control Number: ( Document Date: r ?

Maa& - IM3 8 TSCA NCIC Notification Form for CBI Documents Docket Number:_____ R H . ____________ Document Control Number: ^ 3 c3 o o o d o Document Date: ___________ Document Type: D & c f r F ________________ fC&CO=*->> <c_z O "O ymo CO --imi'" w V :rc -D O m ZK 0 o TO X" ro Th e d o c u m e n t r e f e r e n c e d a b o v e is c la im e d a s c o n fid e n tia l b u s in e s s in fo r m a tio n (CBI) u n d e r Se c t io n 14 o f the To x ic S u b s tan c es C o n tro l A c t (TSCA).

3 GLP10-01-02 Interim Report 05: Analysis for PFOS, PFHS and PFBS in Avenue A Soils and Sediments Collected June/Julv 2010 Study Title 3M Environmental Laboratory Analytical Protocol GLP-10-01-02: Analysis of Perfluorooctane Sulfonate (PFOS), Perfluorohexane Sulfonate (PFHS) and Perfluorobutane Sulfonate (PFBS) in Groundwater, Soil and Sediment for the 3M Decatur Phase 3 Site-Related Monitoring Program Data Requirement EPA TSCA Good Laboratory Practice Standards 40 CFR Part 792 Study Director Jaisimha Kesari P.E., DEE Weston Solutions, Inc. 1400 Weston Way West Chester, PA 19380 Phone: 610-701-3761 Principle Analytical Investigator Cleston C.

A im & -0 0 0 7 2 14 Absorption of FC-95- C xn Rats After a Single Oral Dose October 26, 1979 Conducted at: During: Conducted by: Report by: Reviewed by: Riker Laboratories, Inc.

ARM-Ool'l Study Protocols/Proposals of Ongoing Research 1.

Quality Assurance Project Plan M ulti-City Study Sampling Task (N1Q0672) R226-0077 Amendment 1 to Revision No. : 1 Effective Date: Junel6, 1999 Page 1 o f3 Amendment 1 to the S j 'S S Quality Assurance Project Plan and Associated SOP's for Empirical Human Exposure Assessment Multi-City Study Sampling Task To (Confidential) June 16,1999 Prepared by Battelle 397 Washington Street Duxbury, MA 02332 (781) 934-0571 APPROVALS Donald Gunster Sampling Task Leader Rosanna Buhl Battelle Sampling Task QA Officer -- Marcia Nishioka ' Battelle Project Manager ---- Date Date .7/ .y ?

Acute Orel Toxicity Screen with T--30670OC in Albino Bats j:xfim I<nr'iti: N o .

3M Medical Department Study: T-6295.7 Report No.

AR226-1030A026 BACK Study Title Characterization Study of PFOS, Primary Standard - Test Control Reference # T C R -0 0 0 17-046 ` Ph ase: Solubility of PFOS in Natural S eawater and an A queous Solution o f 3.5% Sodium Chloride Data Requirement 40 CFR 160.105(b) Author Mark E.

BACK TO MAIN Battelle Field Sampling Procedures Review Columbus Georgia City Survey regarding Empirical Human Exposure Assessment Multi-City Study To Susan Beach - Project Lead 3M, ET & SS PO Box 33331 Building 2-3E-09 St.

ENVIRONMENTAL PHYSICAL/CHEMICAL, FATE, EFFECTS AND MONITORING STUDIES DEA Salt of Perfluoro(ethylcyclohexyl) Sulfonate backtocompounds S TU D Y TITLE Physical/Chemical Properties CS-2070/CS-2151 Solubility LABORATORY OR AUTHOR DATE COMPLETED TYPE 3M C om m ercial C hem icals laboratory 08/03/81 Robust Sum mary, Letter Report O ctanol/W ater Distribution C oefficient of C S-2070 Estim ation of W ater S olubility of FC-90 D eterm ination of Melting Point of C S-2070 Environmental Fate and Transport 3M C om m ercial C hem icals laboratory 3M E nvironm ental lab 3M E nvironm ental lab Biosorption of CS-2151 (C S-2070) 3M E nvironm ental lab C hem ical Oxygen Dem and of CS-2151 and Biodegradation of CS-2151 (CS2070) 3M E nvironm ental lab 08/03/81 08/24/82 07/29/81 Robust Sum mary, Letter Report Robust Summary, C alculations Robust Sum mary, Letter Report 08/25/81 08/31/81 Robust Summary, Technical Report Sum m aries Robust Summary, Technical Report ENVIRONMENTAL PHYSICAL/CHEMICAL, FATE, EFFECTS AND MONITORING STUDIES DEA Salt of Perfluoro(ethylcyclohexyl) Sulfonate S TU D Y TITLE LABORATORY OR AUTHOR DATE COMPLETED Ecotoxicity Elements TYPE A quatic Toxicity Testing: C S-2151, Lot 3 (LR 6260S ) 3M E nvironm ental lab 11/19/80 Robust Sum m ary, Techni cal Report Sum m ary Daphnid Bioassay: CS-2151, Lot 3 (LR -6457S) 3M E nvironm ental lab 02/05/81 Robust Sum m ary, Techni cal Report Sum m ary A cute Effect of CS-2151 on M icrobial Respiration 3M E nvironm ental lab 08/24/81 Robust Sum m ary, Techni cal Report Sum m ary

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