INTERIM REPORT # 10 - Analysis of Fish and Clam Samples STUDY TITLE Analysis of Perflnorobutanesulfonata (PFBS), Perfluorohexanesulfonate (PFHS), and Perflnorooctanesulfonate (PFOS) in Water, Soil, Sediment, Fish, Clams, Vegetation, Small Mammal Liver and Small Mammal Serum Using LC/MS/MS for the 3M Decatur Monitoring Program DATA REQUIREMENTS EPA TSCA Good Laboratory Practice Standards 40 CFR 792 STUDY DIRECTOR Jaisimha Kesari P.E., DEE Weston Solutions, Inc. 1400 Weston Way West Chester, PA 19380 Phone: 610-701-3761 INTERIM REPORT COMPLETION DATE May 09, 2006 PERFORMING LABORATORY Exygen Research 3058 Research Drive State College, PA 16801 Phone:814-272-1039 STUDY SPONSOR 3M Company 3M Building 0236-01-B-10 St.

26 _ 06& T BIODEGRADATION (BOD/COD) TEST SUBSTANCE _________________________________________ Identity: A mixture containing perfluorooctanesulfonate; may also be referred to as PFOS, FC-95, or as a component of FC-185F. (1Octanesulfonic acid) (CAS # 2795-39-3) Rem arks: The 3M production lot number was 1-2303.

Katherine E.

A R s.fi.6 _ \x q th Documents in TRP Database Source Title / D escription N o n -T R P Fluorinated Surfactants and Repellents (Kissa, 2001) Bioconcentration in Carp (study conducted for Japan METI) The First Environmental Survey of PFOS and Related Compounds in Japan Levels of PFOA and Other Related Compounds in the Blood of Japanese People 3M: Interactions of Fluorochemicals with Rat Liver Fatty Acid-Binding Protein 3M: Fluorochemicals in Human Blood (Dec. 2002) 3M: Branched vs.

SECTION IV - P PAGE P-7-32 OP P-7-40 TEFLON* POLYMERS DIVISION CATALOG OP CHEMICALS ~4/Z.2.Z6r /S&S April 10, 1981 70: .TEFLON PRODUCTION, TECHNICAL, MECHANICAL SUPERVISION '77"".*.

GLP10-01-02; Amended Interim Report 14 Analysis of PFBS, PFHS, and PFOS in Groundwater BFI Morris Farm Landfill - MArch 2011 GLP10-01-02: Interim Report 14 - Analysis of PFBS.

3M ENVIRONMENTAL LABORATORY REPORT NO.

T W RESEARCH Precise Research.

en RESEARCH Precise Research. .

INTERIM REPORT #25 - Analysis of Ground Water Samples STUDY TITLE Analysis of Perfluorobutanesulfonate (PFBS), Perfluorohexanesulfonate (PFHS), and Perfluorooctanesulfonate (PFOS) in Water, Soil, Sediment, Fish, Clams, Vegetation, Small Mammal Liver and Small Mammal Serum Using LC/MS/MS for the 3M Decatur Monitoring Program DATA REQUIREMENTS EPA TSCA Good Laboratory Practice Standards 40 CFR 792 STUDY DIRECTOR Jaisimha Kesari P.E., DEE Weston Solutions, Inc. 1400 Weston Way West Chester, PA 19380 Phone: 610-701-3761 INTERIM REPORT COMPLETION DATE November 22,2006 PERFORMING LABORATORY Exygen Research 3058 Research Drive State College, PA 16801 Phone:814-272-1039 STUDY SPONSOR 3M Company 3M Building 0236-01-B-10 St.

SOLUTIONS Weston Solutions, Inc. 1400 Weston Way P.O.

3M Environmental Laboratory P0003268; Interim Report#2 Analytical Report Analysis of PFBS, PFHS, and PFOS from 3M Decatur Offsite Sediment Samples Interim Report #2 MPI GLP Protocol Number P0003268 Data Requirement 40 CFR Part 792 Author Michelle D.

7$ ff Corporate Health Physics Corporate Industrial Hygiene & Ergonomics Corporate Occupational Medicine Corporat^pxicology 3M Department 3M Center, Building 220-2E-02 F t t - oioo.

A R 2 2 fe -C 7 Z )0 Battelle Field Sampling Procedures Review Columbus Georgia City Survey regarding Empirical Human Exposure Assessment Multi-City Study To Susan Beach - Project Lead 3M, ET & SS PO Box 33331 Building 2-3fc-09 St.

An Official Journal of the Society of Toxicology Supplem ent AR7XOI1X BEST COPY AVAILABLE A- TOXICOLOGICAL SCIENCES Formerly Fundamental and Applied Toxicology Academic Press 004204 Volume 42^ Number 1-S, March 1998 hiali levels of particulate matter.