M &Z6 - ACUTE TOXICITY TO FISH (FATHEAD MINNOW) TEST SUBSTANCE___________________________________________ Identity: A mixture containing perfluorcoctanesulfonate, which may also be referred to as PFOS, FC-95, or as a component of FC-600. (1-Octanesulfonic acid, 1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8heptadecafluoro-, potassium salt, CAS # 2795-39-3) Remarks: The 3M production lot number was 628.

M AL6 - O Z ^ O ACTIVATED SLUDGE RESPIRATION INHIBITION TEST TEST SUBSTANCE________________________________________________ Identity: A mixture containing perfluorooctanesulfonate, which may also be referred to as PFOS, FC-95, or as a component of FX-601. (1Octanesulfonic acid) (CAS # 2795-39-3).

Or ePcPeIiMv eCdIC 2000OCT 21 Ail IQ: 31 Contain NO GB!

30 June 2003 To: Mary F.

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NOTICE: The information provided to the agency contains information that 3M voluntarily has submitted as part of our continuing discussions with the EPA regarding fluorochemistry.

GLP10-01-02; Interim Report 19 Analysis of PFBS, PFHS, and PFOS in Water Samples Off-Site BP Property - July 2011 GLP10-01-02: Interim Report 19 - Analysis of PFBS.

3M ENVIRONMENTAL LABORATORY REPORT NO.

ty Proven Results.

INTERIM REPORT #29 - Reanalvsis of Soil and Sludge Samples STUDY TITLE Analysis of Perfluorobutanesulfonate (PFBS), Perfluorohexanesulfonate (PFHS), and Perfluorooctanesulfonate (PFOS) in Water, Soil, Sediment, Fish, Clams, Vegetation, Small Mammal Liver and Small Mammal Serum Using LC/MS/MS for the 3M Decatur Monitoring Program DATA REQUIREMENTS EPA TSCA Good Laboratory Practice Standards 40 CFR 792 STUDY DIRECTOR Jaisimha Kesari P.E., DEE Weston Solutions, Inc. 1400 Weston Way West Chester, PA 19380 Phone: 610-701-3761 INTERIM REPORT COMPLETION DATE August 27, 2007 PERFORMING LABORATORY MPI Research, Inc. 3058 Research Drive State College, PA 16801 Phone:814-272-1039 STUDY SPONSOR 3M Company 3M Building 0236-01-B-10 St.

STL Burlington Colchester, Vermont Sample Data Summary Package SDG: 117633 STLS E V E R N TRENT November 30, 2006 Mr.

ARa%-olHl 3M MEDICAL DEPARTMANT CORPORATE TOXICOLOGY To: John Butenhoff Andrew Seacat From: Marvin Case Date: 5 April 2000 Subject: Liver Slide Review I have completed my microscopic review of the liver sections of the 14-week sacrifice rats on the PFOS chronic study.

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Pathology and Toxicology Riker Laboratories, Inc.