Katherine E.

P-1 A ZZZ Q jm DuPont Haskell Global Centers for Health and Environmental Sciences ( f 1090 Elkton Road, P.O.

Quantify Sample Report MassLynx 4.1 PFOA Analysis Dataset: C :\Mass Lynx\P FOA.

INTERIM REPORT # 9-Analvsis of Ground Water Samles STUDY TITLE Analysis of Perfluorobutanesulfonate (PFBS), Perfluorohexanesulfonate (PFHS), and Perfluorooctanesulfonate (PFOS) in Water, Soil, Sediment, Fish, Clams, Vegetation, Small Mammal Liver and Small Mammal Serum Using LC/MS/MS for the 3M Decatur Monitoring Program DATA REQUIREMENTS EPA TSCA Good Laboratory Practice Standards 40 CFR 792 STUDY DIRECTOR Jaisimha Kesari P.E., DEE Weston Solutions, Inc. 1400 Weston Way West Chester, PA 19380 Phone: 610-701-3761 INTERIM REPORT COMPLETION DATE January 9,2007 PERFORMING LABORATORY Exygen Research 3058 Research Drive State College, PA 16801 Phone: 814-272-1039 STUDY SPONSOR 3M Company 3M Building 0236-01-B-10 St.

y \ / U U . 06SI Life Cycle Waste Stream Estimates \j\JW August 2000 Ac3eChnMytattciartlmacleechadtWened"ruaiSfizssauetecalftanuSonrntediraxneetegaescmdtauinmtPEidevasretstfeiulmsuptuhoapmertleoymfscl"cuha,hroeydamriaonoitccefhfadaaelcsmAri:elpiipctUrioaiel.lrsSt2c.pa1oRnr,nede2tpel0faenr0raot0esmod.efbETppyrshootetBidemonauatbtctitjteaeellucl-eswtaivM1age9sete9.eom7fsoPtthrraeiiraastlmw1In:sosfrLtrkioitfuwmet-aebsototh huueEoFsonnifstrwdatiwsimvetme,aravatsaoiatetltpeeakrees,bescrin3auailMnitstwtotsytorauhhmospeeatfpxeseralpreyimnepmaarcnoiilpnhedrylitantemeiricmcnenieazfdefllaonaeutdrctciseaioeteldtnnicartgo.ismweiingnsSaseneeseaaeitrcsnfervuoidicanrnstaet3gdirnsvM,ejteuaatmh,smdmewgpaavmrnaoneorurueptslfunfotaoamtcrcfsctta3teurosusMerefr.iltinieaIn'egnsnsgsspptauolhrrormnoeoecdcpay1uuette9siiscaeoo9strd7nnssissmtdsseaiauupwnlbeberaoossstreuovedfvtqeistegtmuhhhrueeiaeeprnlnetgrpsteestrotsnooapegn1err9dcaa9ttmhsi7o.a,.ns pmcsrceptfmTsFiherntuuoxhrrihouseoonrlnpuoteumfcrldeacectyoeelhorwlulcttennclmuuhsltcylautyaaesryetrssetlsidssdsadeehvtsi.isaonerdssnode.todfbPawetTsspwleh"igttFymexohsruPahtrsOurepaehdatoFifiagscsecdaSilwsOmeeu,cgrhtatisuoopeeSttmsi,iihmesrqmuhttoorPtseeauloswunupdtcqFntiticlhovoamutatOoabt.hrealsiuthfeytaSvelmTiareysvotsraefnheoneiphietlosscstehletoarld,h(asienhysmitsn.ealonhrat,)nssepreevpfTt"rodlPsrchbbereu.hoiteoFieipsaomsiodlbleOsfrio"rtudenmetruohPgeSeceesiccarFniipstgenchnhtaonoOcraaaeadntaodtrnhliSmrdedt"nmidtyestfwhaadiesrpefprtecrfeeeciqoieeeialclortnwceursamleaebnsiidstitdtnedeetvaeaii-tmsituonsdaotcagd.eepanglsaeheecrdlPrsscgittanooeFabhhcoromtp"ldraaOasanseef"nedtlpaSralwCgtiasPotikhs.iisstruF8imneiesaulondRFsOltdmdsaonde1paet.Ssofshpthlq7soiwiaetnuououSafiItnnoemrntienn0tovedhnsds2cppalete.udeyaoiltroprllteiszofmIfogonrslhenodtuoencphypnuttsoerflhoedhtaiceaesrhberototnctmceoaaeettctiaas,tonldlnahsyiyrlreynsibseyisaenasntumoinsdcoacsmtoxiyeethhisphPaycnfg,parnealFPtrotttaadlhiOFsrdttodeteheOuunSapecdtSoyoityo.irfnatnre 3 Final Report Sulfonated Perfluorochemicals: U.S.

, 3M Environm ental Technology and Services / f May 10, 2002 PO Box 33331 St.

AR226-1030A034 Study Title Microbial Metabolism (Biodegradation) of Perfluorooctane Sulfonate (PFOS) I.

May 1, 2001 CERTIFIED MAIL Document Processing Center (7407) (Attn: Section 8(e) Coordinator) Office of Toxic Substances US Environmental Protection Agency 401 M Street, SW Washington, DC 20460 Re: TSCA 8(e) NOTICE For: Acute Toxicity Honey Bee Studies on Perfluorooctane Sulfonate, potassium salt, CAS# 2795-39-3 Dear Sir: 3M is submitting the results from recent oral and contact acute toxicity tests performed with 1-octanesulfonic acid, l,1.2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-heptadecafluoro-,potassium salt (CAS No. 2795-39-3) - commonly referred to as PFOS - on honey bees.

ARH2 6 _ 0 6 3 7 ACUTE TO XICITY TO AQUATIC INVERTEBRATES (COROPHIUM VOLUTATOR) TEST SUBSTANCE_______________________________________________ Identity: A mixture containing perfluorooctanesulfonate, which may also be referred to as PFOS, FC-95 or as a component of FC-201AF. (1Octanesulfonic acid) (CAS # 2795-39-3).

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i 3M Gieneral Oftfices gHQ- OfOl - O i l 5 May 15,2001 3M Center St.

A A&6 - IIH-D Unclassified Organisation de Coopration et de Dveloppement Economiques Organisation for Economie Co-operation and Development ENV/JM/RD(2002)17/FINAL 21-Nov-2002 English - Or.

Andrea V.

I f DuPont Telom er Inform ation Meeting, M ay 2,2003 NAME O RGANIZATIO N A * . /$/& C o n t a in s N o C B I TELEPHONE # E-M AIL ADDRESS in r o r Kobe-W ^ m jlU U ktTc> (+t& ^~Q f< z x c f - ^ w _t I~ 3> U> uNul l/\fw<A- P z-i/ib g rth ;- h fL iA L& iu k.^ VO - V\l /| / Ia ' ,uT X } O** m ^ a A .

M M 6 _ 13> RECEIVED OPPTNCfC ZWJUL-7 AMII: 00 2 May 2003 ToWMUE1:2P.aaS0Ars.0yhEEiPFnnae.gvsnDttinoroson(ymMn, lmDvianaieCilnnaiCktaa2ol0Ad4Pev6reo70nt4eu0ce5t,iMoNn)WAgency From: Katie Smythe, on behalf of the Telomer Research Program Subject: TRP Document Submission cO0sstuo0un1bmd2mbim1eei.shtotanehTldlafhyveoteoksfenattohhlsrweeuemanETdPemaylAsoab8mrefi-oeee2snrrTiaRsneruceelbolsufmemosairiertoctrsnehtBudiPdnAtiroeoAlscgtdhorcmeahomoAninldgi(u(sTeCtcnrRtsaceFPtydin)v,bfCeoytHhrRtehotehefCceooHTlTrlRdoiROwP2PH.i2n)o6g.n[sTDCtuhoAdecSykf#iesntu6aIm7lD8rm:e-3paO9roi-rPe7tsPswTafor-he2ric0thh0e3is-sealso 231))) 4) 5) IAPAP8Sn-uhosq2rylsvuuiaisTfevbyiioecoeilluawdioRlsti-my8taCS,h-te2htarMaaenAbBmdCiilclcioVAirstoonytlahrfncpyiooourolfmhcP:rlo8raePol-Stu:2ropaserelTAsymArsetcuioAslueorsnssteameesyola(elO3fyarr8rB/ae-l2pEATo.Trloccetxosol)iolhclmoi/tleyMra-saBmFaAiaFxllueicadnonchDto-iool:MsneUiocMflrtopreasHthovomiodeleRt SevpeercsteruMmu,Wtataitoenr Wttmhheeeetfshwiaonmodauslelrdadenopadcopkrfptiersnte.dcfiiinlaegtessohaaltohvniangtgtwheeiatchrehtahsdeteurfduhylalssruetmhpeomrbta.erynPealfeniatdsoerfelaleatstehmdoerftiknonavolewrrevpiifeowyrtouoinfnctelhueeddesadtundtooytghoeetbrhjceeocrptiinyveosf, N(yCoouBnIeh)aouvfnetdhaeenryaTtdStaiCfcfhAice.udltfPiiellesesaoscpeoenlnetitanimgnetihnkefnoaortwmtaacithfioeydnoufcillhaeaismv. eedanaysqCuoenstfiiodnenstaiabloBututshineedsoscIunmfoernmtsatoiornif Best regards, TI RP Administrator