Document zzbj84Na8mXGDnzadZGvBmQ9R
CG 3:
f ODE. RT-761-D F
JAN , ,, Ib82
A&ibQ -
< DAIC ) ^.OT NUMBER5
/#*3t EST. WT. 214* LBSS.
PREPARATION NOTE Ss
PROCESSED < ) R1-761-D <0>
AFPROVED BY CWK 1 -12-02
TYPED RY JMH
\y STANDftKP HRS. . 7.?
, TIME at j.
1 Ja T..j L2JTJZ.
rs SS =5 S3 SKffS S2 Of SSIS S&' J#SB$ JSt35 S3ftSSTW*
e**r ijrfittta
S>3ft SS3SSb'S&S3S^s Jk SS%= -- = = S.
NON BLEEDING
EQUIP I
I USE
N-COBE
MENT i
1
i-"
NAHE. WATCHUNG RED B
I LBS I-------- I
NOTE- BATCH MUST BE PRESSED PROMPTLY TO
j i nv_ ic ir* f'o Nr1 rTAc" ir rn.. u l i
iRir II h .AJI RLE WITHIN 5 '-IT AF TE F iF i 1 Ni..
ili
PRESS rf*LL BE READY _______ M/P^^ SUP
START MAKING ________M/MAKG SUPV
ACCT LBS
PREP 1
NOTE: RUN >5m WATER ENTO V-904. rUMP WATER FROl V-904 THRU DISIMBUIOR. IF WATER DOES I NOT COME OLJT OF ALL DISrF\T3UTQR HOLES WITH I FULL FORGE, NOTIFY SUPERVISOR.
I ^T{ rRECORD:.^..BATCHES SINCE-SPARKLER LAST CLEANED. AFTER 4 BATCHES, CLEAN, DRESS SPARKLER & PRE-COAT WITH 15* DICALITE, FILTER AID OBTAIN FOR SI 2 2-CHLORQ~4~AMIN0TOLUENE-3SULFONIC ACID OBTAIN FOR S28 3-HYDR0XY-2-NAPHTH0IC .A I CD INSTALL DV G CV RECORDER & CONTROLLER CHART!
777-A ic
740-C
.8.2-C
mw
RUN 1 7" < 1 ?0G) WATER INTO
HEAT TO
.9,3/p1,
L^QC0-100 DEG F
>PH>ADD IN 1-2 MIN DRESINATE XX
115
99-A
115
^T^ADD IN 1-2 MIN DRESINATE X
52 530-A
52
STIR 5 MIN & RECORD: PH__^.l?.<9.5-ie.5>
STIR 20 MIN OR LONGER TO DISSOLVE FOR'S 31
NOTE: NOTIFY PRESS ROOM BEFORE ROPING OFF
AREA UNDER V 922
922 3'
\jrfT\s RUN 39 <803 G) WATER INTO V 922
!
r!>T WEIGH SODIUM HYDROXIDE INTO V-926 ?* RUN IN |
m
I \JT\ TURN ON AGITATOR & STEAM & DUMP IN FROM S 21
r 12-CHL.0R0-4-
LOT
*100%
%|
t ] AMINGTOLUENE-
__&2_____
I
I, is-s u l f o n ic I J&CID.
i
----- JBt&L. !
1.1-B*jyDUWP IN ACTIVATED CARBON;//I
|1>^TxtfUMP IN FILTER AID
I
|JJP>-HEAT TO 212-214 DEG F
WATCH FOAM
|
\A4>\ RECORD: BY__jri__<MUST BE +>
ASSUME 50% |
lin STIR 30MIN AT 212-214.*F THEN SHUT OFF STEAM |
[ I WATCH FOAM RECORD SPARKLE PRESSURE__L._PSI I
I : i IF NOT ZERO, NOTIFY SUPERVISOR.
|
V 7-D 740-C
228 1157
pm*
1 | I
113-B 777-A
7-D
\
25 10
i
t >AK ING INSTRUCTION.,' BATCH
Eai`iP KENT
1 PAGE 2 GF 3 CG 32 CODE RT-761-D
C3NT
1 CIRCULATE 15 MIN OR LONGER AT 170-195 H" 1
|
I I THRU SPARKLER UNTIL SOL'N IS CLEAR,
,
I I MAINTAIN AT 170-1 <?5*F FOR S22. RECORD-
t
JrSKkRl
TOTAL MIN_/Jl __ CLARITY__c/fl_ I
| RECORD: HT^3.__F & RECjfjL,,..F
|
I1
r M-r'oi)E ItHHNN
J LBS
cv T"r UN"5,_(455 G) WATER~INTO~V-"
4
!>W (58 G) WATER INTO V 4M/CV f0$
~\
li^} WHEN S 18 COMPLETE, PUMP IN V 922 THRU
|
I I .SPARKLER. MAINTAINJ/-922 AT 190-195JDEG F j
1 I RECORD : START
, TOTAL :MlN_ifcl___ 1
MISC.
T2^^3'wEIGH_S0i)IUN~NlTRfTE"'lN_PT~F0R~S40 777
T~T~
WEIGH SODIUM NITRITE DRUM FOR 547
_. j
M_,,,,JAd&l -J1&.
MEASURE 4e__UNITS IN V-928 FOR S38
HYDROCHLORIC ACID
M,,*,,,,_, *$.%tt$3L
y&6 1--POTT 66* C1720G) WATER INTO V902
2? I WEIGH SODIUM HYDROXIDE IN V~*74 t, RUN IN
M
DUMP IN FROM S 3
LOT
^HYDROXY ~2~NAi`HTH01C
ACID
GH 1-HYDR0XY-2-MAPHTH0IC ACID ON .
E & ADD
LOT_____ f&J.
TO 70~9#F S, STIR 10 MIN TO DISSOLVE
SJ-HRRY TRISULPHOIL SOAP D IN 30G WATER &
OUR INTO V902
`' '
STEAM EJECT IN V 921/931 FROM S 9
;'?2 ?, KWHEN S 23 COMPLETE, SHUT OFF PUMP N INSERT I
'/CV
FOOT PLUG IN V 922
i
8 Igafil RUN IN 12" (247 G) WATER & HEAT' TO 180-190 j
f UDEG F. CIRCULATE IS MIN THRU SPARKLER
i
\WF\ WHEN S33A COMPLETE PUMP V 922 THRU SPARKLER 1
T I INTO V 904
t
13At TT RUN Hi 5* (103G) WATE^ INTO V--922 & HEAT TO I
t L-+90- 195 F CIRCULATE 15 MIN THRU SPARKLER 1
EMP V-922.THRU SPARKLER INTO V-904/CV
I
EN MT BLOW OUT SPARKLER INTO V-904/CV
i
AI A49/CV TO 165-170XF FOR S38
1
725-A i 41 ? V.
725-A | I" '
44
28-D I 557
**.***". *^'1 **'" i
!: 7-D | '732
82-C i 1038
!ji
i 180-C i
17
I
i 3 9-A | 105
cv -9 *
NOTE: IF N-740-C SOL'N WAS PUMPED DIRECTLY
1 PROM SPARKLER TO CV AT s`S -cx. > 33B, 34B I i ~'MT 1 S33
TAt ( WHEN S3o 'COMPLETE, PUMP V904 AT 165~170*F
I i rHf J LMrERSURFACE DISTRIBUTOR INTO CV AFAP .
I -Hu: `-n'ri) RECORD START______ L ..TOTAL MTN,_^._|
I
U RUN-IN N28D HYDROCHLORIC ACID FROM S25 INTO!
I
>PAP (12-15?1IN) MAINTAIN AT 185~i70*F ADJ TO 48" (4536 G) AT 32-38 DEG F
I p- I H9X330I
57-A
RUN IN
. --A FROM S 23 AFAP (5-10 MINJ6RINSE IN PT
STIR 10 rilfi AT 32-38 DEG F MAINTAINING
J
}
SODIUM NT TRITE
M_ _ ,_________ V, I________ ! 725-A
KI_
'+)
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DUP050110551
tIAKZNG INSTRUCTIONS :BATCH UNIT
EG*JIP ' MENT
| PAGE 3 OF 3
CG 32 CODE RT-761-D
1 USE I N-CODE (0) ! LBS i
ACCT LBS
CV ? CUNT
-I^PS^K^MP IN CALCIUM CHLORIDE
IN STRONTIUM NLTRAIE
*fjL&tlMP IN BARIUM SULFATE
4
LAa-nr 1|
ADD FOR MAIMTAIN'ING COUPLING
32-38
DEG
F
DURING
902 JW<| PUUE N-725-A SODIUM NITRITE FROM S24 INTO 10 ^,^<^902 K8 Ffig^UMP IN AMMONIUM CHLORIDE
11164 i 1 255 ! 1 137 !
1I 140X3301
i 1 1 193
1 1 I
20-A 246B,E
65-A
1164 255 137
57-A )js&c
v:;.-
165-A
.
198
IMMEDIATELY COUPLE DV THRU UNDERSURFACE
DISTRIBUTOR INTO CV IN 18-22 MILNIN
fjAJNTAIN DV AT 32-JBJDEG F
<3l A
RfeCPRD: START/i^gg:, TOTAL MIN
I
STIR 15 MIN',*.
_
RECORD
, DIAZO______ :__(->
|
PH_2#_*J(10*0-10.5) 4. IF NECESSARY, ADJ TO I
PH 10.0-10.5 6 RECORD PH__s^WlJr SODIUM
|
HYDROXIDE
' ASSUME 50%I_
J
YjDROCHLORIC ACID
ASSUME 32% | _ ______I
l IGH IN DRUM 4, POUR IN I OCTANOL
| 39 J
TO 174-176*F IN 70-75 MIN AT150*F
I
TURN ON WATER SPRAYS 1 1/4 TURN^-
I
CORD; HTjI.Mj X REC_/Z2__F
I
IR 30 MIN AT 174-176 DEG F
|
AFTER 10 HIOJ4 STIR,
|
RECORD: T'HjSUzi(9.5-10.0) AND I NECESSARY1
2ADJ TO PH 9.5-10.0 RECORD: PH___ * - .
I
^^IUMv HYd ROXIDE
ASSUME 50%
PH ABOVE 10.0 DO NOT ADJUST
WHEN S54 COMPLETE, FLOOD TO 180-190" .
<+/- 18000G) AND STOP AGITATOR 6 TURN OFF
WATER" SPRAYS.
WHEN INSTRUCED BY PROCESSING AREA HALFWAY
THRU PRESSING
<1 > DUMP IN I OCTANOL <2) STIR 5 MIN
I 10
(3) ADVISE PROCESSING TO RESUME PRESSING
7-D 28-B 588-A
7-D US' I
5Q8-A | 10
START
OPTR
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