Document zzJJ0783Y6jM94xQ6VR6kN597
SEVERN TRENT
STL
STL Chicago 2417 Bond Street University Park, IL 60466
Tel; 708 534 5200 Fax; 708 534 5211 www.stl-inc.com
S iqria L
/v
Name: Richard Ch WrighL
T it.T.e ; P ro je c t Manage r
E-Mail : r w r i g h t @ s t 1 - i n c .corn
This Report Contains
Leaders in Environmental Testing
Da Le STL Chicago 2417 Bond Street University Park, IL 60466
PHONE: (70S) 534-5200 FAX. ,, : (708) 534-521:1
Pages
Severn Trent Laboratories, Inc.
WET CHEMISTRY DATA PACKAGE CONFIDENTIAL DECATUR - FC INVESTIGATION
JOB# 233695
Data Summary............................................................... 1 Chain of Custody......................................................... 26 Case Narrative............................................................. 33 Raw Data...................................................................... 35
STL Chicago is part of Severn Trent Laboratories, Inc.
S A M P L E '1 N f D R M A T I O N Date: 02/06/2005
Job Number. 233695 Customer... Weston Solutions, Inc. Attn...... Jai Kesari
Project Number....... Customer Project ID... Project Description.,.
20004891
CONFIDENTIAL DECATUR Confidential Decatur - FC Investigation
Laboratory Sample ID
233695-1 233695-2 233695-3 233695-4 233695-5 233695-6 233695-7 233695-8 233695-9 233695-10 233695-11 233695-12 233695-13 233695-14 233695-15 233695-16 233695-17 233695-18
Customer sampleId ' DF09-GW-131R-0-041020 DF09-GW-131S-0-041020 DF06-GW-132R--04102 DFQ6-GU-132S-Q-04102Q DF06-GW-133R-0-041020 DF06-GW-133S-0-041020 DF14-GW-136R--40121 DF14-GW-136S-0-040121 DF14-GW-136L-0-040121 DF14-GW-137S-0-040121 DF14-GW-137L-0-040121 DF8b-GW-134R-Q-040121 DF8b-GW-134S-0-040121 DF5b-GW-135R-0-040121 DFSb-GW-135S-0-040121 DF8b-GW-135L-0-040121 DF09-GW-130R-Q-040121 DF09-GW-13QS-0-040121
! Sample Matrix
pate sampled
Water
01/20/2005
Water
01/20/2005
Water
01/20/2005
Water
01/20/2005
Water
01/20/2005
Water
01/20/2005
Water
01/21/2005
Water
01/21/2005
Water
01/21/2005
Water
01/21/2005
Water
01/21/2005
Water
01/21/2005
Water
01/21/2005
Water
01/21/2005
Water
01/21/2005
Water
01/21/2005
Water
01/21/2005
Water
01/21/2005
Sampled 12:20 12:35 14:20 14:15 14:45 14:50 08:20 08:25 08:30 08:00 08:10 09:55 09:45 09:30 09:10 09:20 10:25 10:15
Pate!; Received' 01/22/2005 01/22/2005 01/22/2005 01/22/2005 01/22/2005 01/22/2005 01/22/2005 01/22/2005 01/22/2005 01/22/2005 01/22/2005 01/22/2005 01/22/2005 01/22/2005 01/22/2005 01/22/2005 01/22/2005 01/22/2005
Received 10:00 10:00 10:00 10:00 10:00 10:00 10:00 10:00 10:00 10:00 10:00 10:00 10:00 10:00 10:00 10:00 10:00 10;00
STL Chicago
Page 1
1
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Nuifcer: 233695
"istofSHr Weston Solutions^.. Inc.
.
Customer SanrpLe ED: DF09-GW-13TR-Q-041020 Date Sampled.......:01/20/2005 Tin Sampled.......:12:20 Sample Matrix......:Water
TEST METHOD-
;P A R A M E ! E R / TEST D E S C R I P T I O N
160.t
Solids, Total Dissolved (TDS) Solids, Total Dissolved (TDS)
160.2
Solids, Total Suspended (TS5) Solids, Total Suspended (TSS)
LABORATORY
TEST
RESULTS
PROJECT:. iEEWRIBENnffliiBeomJR:-.
Laboratory Sample ID: 233695-1 Dote Received...... : 01/22/2005 Time Received....... : 10:00
Date:02/04/2005 ATTN: Jai Cesari
SAMPLE-RESULT Q FLAGS 340 5.0
WOL 8.4 4.0
RL10
5.0
) - T p il o t i o n J-;; u b i t s ;-; ;b a t e h ;m
;DATE/I (HE T E C H
mg/L
140702
:01/27/O5 1110 jmk
mg/L 140323 :01/25/05 1205 jmk
STL Chicago
* In Description = Dry Ugt.
Page 2
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Humber: 233695
^CUSTOMER;'ifeston Solutione/dnc.-!
Customer Sample ID: DF09-GW-1315-0-041020 Date Sampled..... : 01/20/2005 Time Sampled..... : 12:35 Sample Matrix.... : Water
LABORATORY
TEST
RESUL T S
PROJECT'%CONE fBEMTIAL:DECATUR? i:?
Laboratory Sample ID: 233695-2
Date Received....
01/22/2005
Time Received....
10:00
Date:02/04/2005 ATTW.;.. Jai Kesari-.-
* In Description = Dry Ugt,
Page 3
STL Chicago is part of Severn Trent Laboratories, Inc.
Job N u n b e r: 233695
a fS ie W E R j-ife?-tfi S o lu t io n s , in e .
C u s t o m e r S a m p l e ID: D F 0 6 - G U -13 2 R - 0 - 0 4 10 2 0 Date Sampled...... :01/20/2005 Time Sampled...... :14:20 Sample M a t r iK ............ : W ater
TESfiTtfOO
iMBlMTfl/E&T- ^ S C R I P T ! OU
160.1
Solids, Total Dissolved (TDS) Solids, Total Dissolved (TDS)
160.2
Solids, Total Suspended (TSS) SoLids, Total Suspended (TSS)
TT
LABORATORY
TEST
RESULTS
PROJECT r CONFIDEM L DECATUR
Laboratory Sample ID: 233695-3 Date Received...... : 01/22/2005 Time Received....... : 10:00
D a te :02/ 04/2005 . ATTN: J a rE e s a ri
SA MP LE -RESULT-
FLAGS '
66
a.o
-HOL8.4 4.0
'BL' 10 5.0
d il u t raw UNITS BATCH- pFi::-ATE/i;illE-. TECH
mg/L
140702
01/27/05 1116 jmk
mg/L
140323
01/25/05 1208 jmk
STL Chicago
In Description = Dry Ugt,
Page 4
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Humber: 233695
ii.CUSTGMRYiHMtm^SaLutons/ilhi: : :': -
Customer Sample 3D: DF06-GU-132S-0-041020 Date Sampled.......:D1/2G/2005 Time Sampled.......:14:15 Sample Matrix..... :Water
!
LABORATORY
TEST
RESULT
: F^PJET:.CONFIDENTIALBECAW-;C;;T;\:\\ ;
Laboratory Sample ID: 233695-4 Date Received.........:01/22/2005 Time Received.........:10:00
Date:02/04/2005
. ATTN: .. Jsi; Kesari
SOTHflD.
;PARARE TEEt/TEST: 'DESCR IPT-ION'
160.1
Solids, Total Dissolved (TDS) Solids, Total Dissolved (TDS)
160.2
Solids, Total Suspended (TSS) Solids, Total Suspended (TSS)
SAMPLE RESULT
ELASS:
220
4.5
RDL 8.4 4.0
RL DILUTION W IT S - BATCH' >DT iPATE/TTME. TECH
10
mg/L
140702
01/27/05 m e Jmk
5.0
mg/L
140323
01/25/05 120?!jmk
STL Chicago
* In Description = Dry Ugt.
Page 5
STL Chicago is part of Severn Trent Laboratories, Inc.
Job (Jifnber: 233695
-CUsraraR:--Weston' s o lu t io n s , .mt;.
Customer Sample ID: DF06-GU-133R-Q-041020 Date Sampled..... : 01/20/2005 Time Sampled..... : 14:45 Sample Matrix.... : Water
. TEST METHOD ;
:: PARAHE7ER/iESTDESCRIPTION-
160.1
Solids, Total Dissolved (TDS) Solids, Total Dissolved (TDS)
160.2
Solids, Total Suspended (TSS) Solids, Total Suspended ITSSJ
o
LABORATORY
TEST
RESULTS
' ' PROJECT: CDMF IK N T IA L ' D ECATUR ' '
Laboratory Sample ID: 233695-5 Oate Received____ 01/22/2005 Time Received...... : 10:00
Date:02/04/2005 ATTS.i..-.Jsi-.Kssari:..
. "j" SARPLE'-RESULT"- B it LAGS:i L
32 8.4
5.0 U
4,0
10 5.0
TLtmti ...UMTS.-.. BATCH DT .DATE/TIHE.;;.. 3TECIT
1
mg/L 140702
01/27/05 1121 jmfc
1
mg/L 140323
01/25/05 1210 Jmk
STL Chicago
* In Description = Dry tfgt.
Page 6
STL Chicago is part o-f Severn Trent Laboratori es, Inc.
Job Number: 233695
CUSTDHERr Ve&t n. SciLuti hsj. The
Customer Sample ID: DF06-GW-133S-0-041020 Date Sampled..... : 01/20/2005 Time Sampled..... : 14:50 Sample Matrix.,__ : Water
"TEST METODO 160.1
160.2
PARATIER/TEST DESCRIPTION
SoL ids. Total Dissolved CTDS) Solids, Total Dissolved CTOS)
Solids, Total Suspended CTSS) Solids, Total Suspended CTSS)
O
LABORATORY
TEST
RESULTS
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID: 233695-6 Date Received...... : 01/22/2005 Time Received...... : 10:00
Date:02/04/2005 ' ATTN:; Jai IessrT.........
f SffldPOE-RESULT"' Q T LAGS- ::ol: aa 8.4 14 4.0
DILUTION ;WflTS;;:; TBATCS: DT Ix m i e / n n e ::::-.TECH
10 1
rng/L 140702
01/27/05 1 123 jmk :
5.0 1
mg/L 140323
01/25/05 1212 jmk
STL Chicago
* In Description = Dry Wgt.
Page 7
STL Chicago is part of Severn Treni Laboratories, Ine.
Job Nimber: 233695
CLfSTCiHER'jWeston
'
Customer SaripLe ID: DF14-GW-136R-O-04O121 Date Sampled...... :01/21/2005 Time Sampled...... :08:20 Sample Matrix..... :Hater
LABORATORY
TEST
RESULTS
PROJECT! TQNfICEttTlAL DECATUR-.
Laboratory Sample ID: 233695-7 Date Received........ :01/22/2005 Time Received........ :10:00
Date:02/04/2005 ATTN: . jt KessfrC
..TEST METHOD-;;- /;;;;;;; ;p a r .a h e t e r /t e s t d e s c R p t i e h . . ':::.
160.1
Solids, Total Dissolved (TDS) Solids, Total Dissolved (TDS)
160.2
So Lids, Total Suspended (TSS) Solids, Total Suspended (TSS)
:-;S^ l :'r )l:. ::. ELftGS ' 88 110
8.4 4.0
: RL
DILUTION- ; .;Cjh T &;;;;;b a t Off: m : R-MTE/TIME- TECH
10 1
mg/L 140702
01/27/05 1126 j'mk
5.0 1
mg/L 140323
01/25/D5 1213 jmk
* 1rs D e s c rip tio n = Dry U gt.
Page 8
________ l
STL Chicago
STL Chicago is part of Severn Trent Laboratories, Inc. Job Muirber: 233695
LABORATORY
TEST
RESULTS
Date:02/04/CH>5
STL Chicago is part of Severn Trent Laboratories, Inc. -- - --------
Job Nunber: 233695
"CUSTOMERS ^s ton- Solutiofi/' ine* ''
Customer Sample ID: DF14-GU-136L-0-040121 Date Sampled...... :01/21/2005 Time Sampled...... :08:30 SampLe Matrix..... :Water
^TEST'-METCC'
PA&METiR/TEST-DESIBIPTIQK-'
160.1
Solids, Total Dissolved ITDS] Solids, Total Dissolved tTDS>
160.2
Solids, Total Suspended (TSSJ Solids, Total Suspended CTSS)
LABORATORY
TEST
RESULTS
'' PROJECT !'CONf IBEHTIAL '13ECA7L3R
Laboratory Sample ID: 233695-9 Date Received....... : 01/22/2005 Time Received....... : 10:00
Date:02/04/2005 ATTN: Jai ICesri............
:-S^WHi--RESULT-;-. a FLAGS
.'h d l -
170 8.4
14 4.0
RL d i l u t i o n :
:MTH-: :.-.d a t e /t t m e -.::- '1ECR:
10 1
mg/L
140702
01/27/05 1131 jmk
5.0 1
mg/L
T40323
01/25/05 1216 jmk
STI. Chicago
* In Description = Dry Wgt.
Page 10
STL Chicago is part of Severn Trent Laboratories, Enc.
Job Number: 233695
OJSTOHER:' .WstPH- :Spluti 6ns ,;Ihp -!
Customer Sample ID Date Sampled..... Time Sampled..... Sample Matrix....
DF14-GU-137S-0-04121 01/21/2005 08: DO
H ater
TEST METSQfr-
MRAMETEfc/T EST:DESCR PHOtt
160.1
Solids, Total Dissolved (TDS) Solids, Total Dissolved (TDS)
160.2
Solids, Total Suspended iTSS) Solids, Total Suspended iTSS)
LABORATORY
TEST
RESULTS
PROJECT ::COM FIO EMTI AL 'D ECATUR
Laboratory Sample ED 233695-10 Date Received...... 01/22/2005 Time Received...... 10: DO
Date:02/04/2005 ATTN-: 'Ji -Kesar i-:
SAMPLE! RESULT
jFLAGS:
220
20
WL 8.4 4.0
ri:
iDtLUTTOtt HITS
b a t c h : ar date/ time:: T1H-3
10
mg/L 140702
01/27/05 1134 jmlc
5.0
mg/L 140323
01/25/05 1217 jmfc
ST1. Chicago
* In Description = Dry Ugt.
Page 11
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Ntuiber: 233695
CUSTOMER: Weston S o tu tiw ie , Tnt*
Customer Sample ID: DF14-GU-137L-0-040121 Date Sampled...... :01/21/2005 Time Sampled...... :D8:1G Sample Matrix..... :Vater
t e s t :m e t h c d :
.PARAMETER/TEST; DESCRIPTIOM
160.1
Solids, Total Dissolved (TDSJ Solids, Total Dissolved (TDS)
160.2
Solids, Total Suspended <TSS) Solids, Total Suspended (TSSJ
LABORATORY
TEST
RESULTS
' '''PROJECT: COUFiDEMT LAL DECATUR
Laboratory Sample ID: 233695-11 Date Received...... : 01/22/2005 Time Received...... : 10:00
SAMPLE RESULT-
FLAGS'
220
5.0
MDL 8.4 4.0
ELL 10 5.0
Date:02/04/2005 ATTN: Jaf -Kesp-i
ri
DTW I T S ; BATCH ;
d a t e /t i m e ; TECH
mg/L 140702
01/27/05 1137 jmfc
mg/L 140323
01/25/05 121&Ijmk
STL Chicago
* In Description = Dry Ugt.
Page 12
rTi
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Nunber: 233695
:;:;{^STWEft:--!iiies:tn::5Ptuitions, Irte* ;
Customer Sample ID: DF8b-GU-l34R-0-040121 Date Sampled..... : 01/21/2005 Time Sampled..... : 09:55 Sample Matrix.....: Water
test hethbg
160.1
160.2
. PARAHETEFi/TESI DESCRIPTION :..
Solids, Total Dissolved CTDS) Solids, Total Dissolved CTDS)
Solids, Total Suspended CTS5) Solids, Total Suspended (TSS)
LABORATORY
TEST
RESULTS
; HRJECT: CtSJfIO ENT LAL HCTUR
Laboratory Sample ID: 233695-12 Date Received........ :01/22/2005 Time Received........ :10:00
Date:02/04/2005 Kesari
SAHPLE. TESl&T Aliali LAGS
1S0
12 i! ji |
. .i'.C R C ; DILUTION .;yn i.Ts ; ;;b a t c h ;; DT- DATELINE' TECH
8.4
10 1
mg/L
140702
D 1/27/05 1139 jmfc
4.0
5.0 1
mg/L
140323
01/25/05 1220 jmfc
STL Chicago
* In Description = Dry Wgt.
Page 13
STL Chicago is part of Severn Trent Laboratories, Ine.
Job Number: 233695
:.;;USTaiERr-.Hst<n S o t u t ie f / ilnEr/;; .
''
Customer Sample ID: DFSb-GU-134S-O-Q40121
Date Sampled..
01/21/2005
Time Sampled..
09:45
Sample Matrix.
Water
TEST' METHOD'.
eARHSi/S- D S C R I PTTOH
160.1
Solids, Total Dissolved (TDS) Solids, Total Dissolved (TDS)
160.2
Solids, Total Suspended (TSS) Solids, Total Suspended CTSS)
LABORATORY
TEST
RESULTS
' PROJECT:-:COMFi&eiiTiAl:-.DECATUR
Laboratory Sample ID 233695-13 Date Received...... 01/22/2005 Time Received....... 10:00
Date:02/04/2005
SAMPLE RESULT
44
5.0
FLAGS '
'HDL
e.4 4.0
RL 10
5.0
DILUTION ;UMTS;.';'['BAT CR' fit-: m t e /h m e : TC0
rng/L 140702
01/27/05 1142 jmfc
1
mg/L 1403 23
01/25/05 1221 jmk
* In Description = Dry Ugt.
Page 14
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Humber: 233695
CUSTOMER;-;!Weston Solijtaos -,Ibi?-
Customer Sample ID Date Sampled..... Time S am pled............ Sample Matrix....
D FBb-GW-135R--040121 01/21/20D5 09:30 Water
TEST' .METHOD-.
PRA Efc/TEST iDESCRIPTIOff.
160.1
Solids, Total Dissolved (T0SJ SoLids, Total Dissolved (TDS)
160.2
Solids, Total Suspended CTSSJ Solids, Total Suspended <TSS)
Vi
LABORATORY
TEST
RESULTS
.p r o j e c t iiie d n pi d e n t i a l .d e c a t u r
Laboratory Sample ID: 233695-14 Date Received...... : 01/22/2005 Time Received....... : 10:00
Date:02/04/2005 ftTTN;.- JST Kesari-
SAWLE' RESULT-
FLAGS
94
24
:WBL
8.4 4.0
RL DTLUT'iCW ' UWIT-S-- BATCH DT DATE/TIME- TECH
10 5.0
mg/L 140702 mg/L 140323
01/27/05 1144 jmk
01/25/05 1222 jmk
STL Chicago
* In Description = Dry Wgt.
Page 15
STL Chicago is part of Severn Trent Laboratories, Inc.
Job llmtber: 233695
.;E^TCRR:::-est6n:Solutions, Inc.-
.....
Customer Sample ID: DF6b-GU-135S-0-4D121 Date Sanpled...... :01/21/2005 Time Sampled...... :09:10 Sample Matrix..... :Water
TEST'METHOD 160.1
160.2
PARAMETER/TEST IDESCRIPTl:
Solids, Total Dissolved (TDS) Solids, TotaL Dissolved (TDS)
Solids, TotaL Suspended (SS) Solids, TotaL Suspended iTSSJ
LABORATORY
TEST
RESULTS
'PROJECTCONFIDENTIAL DECATUR'
Laboratory Sample ID : 233695-15
Date Received...... : 01/22/2005 Time Received...... : 10:00
Date:02/04/2005 ATTil:.-.Jai Jisari.-
SAMPLE RESEJLT ifl TLAGS i' 270
;MDL::
6.4
670 13
RL- DILUTION' ;u h i TS.;- ;BATCH DT ' BATE/TIWE- TECH
10 1
mg/L 140702
01/27/05 1147 jmk
17 1
mg/L 140323
01/25/05 1223 jmk
* In Description = Dry Wgt.
Page 16
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Nimber: 233695
CUSTOMER :- ;W eston : SoLut i n ia ; ; il n e .
Customer Sample ID Date Sampled..... Time SanpLed..... Sample Matrix....
D FSb-GU-135L-0-040121 01/21/2005 09:20 Water
/TEST-METHOD
PARAMETER/TEST- iDESCfi l 1/JM
160.1
Solids, Total Dissolved (TDSJ Solids, Total Dissolved (TDS)
160.2
Solids, Total Suspended (TSS) Solids, Total Suspended (TSS)
LABORATORY
TEST
RESULTS
.PROJECT:!CONFIDEM.IAL DECATUR-;!
Laboratory Sample ID 233695-16 Date Received...... 01/22/2005 Time Received...... 10:00
Date:02/04/2005 ATTK: J3i r e s a r t
SAMPLE-RESULT
FLAGS'.
190
8.0
-mi
8.4 4.0
-.rl:
10 5.0
oi-Ltmow--:- twiTs' -BATCH- DT ;d a t e /t THE TECH
png/L 14D702
01/27/05 1150 jmfc
mg/L
140323
01/25/05 1225 jmfc
STL Chicago
* In Description = Dry Wgt.
Page 17
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 233695
iElfSTOMER: West on!:Soluti orisi;;!Jne-.
Customer Sample ID: DT09-GU-130R-0-040121 Date Sampled...... :01/21/2005 Time Sampled...... :10:25 Sariple Matrix..... :Water
LABORATORY
TEST
RESULTS
; PROJE 0T;! COM F.IESN l! IL DECSTR
Laboratory Sample ID: 233695-17 Date Received...... : 01/22/2005 Time Received....... : 10:00
Date:02/04/2005 ATTM:- ' Jai Kesari!
S T L Chicago
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Nunber: 233695
:: USTORER i-:Uest cri;Sdtutf m p >..fhp..
Customer Sample ID: DFD9-GW-130S-0-040I21 Date Sampled..... : 01/21/2005 Time Sampled..... : 10:15 Sample Matrix.... : Water
'T1T-;METH0C- CX;".!;' PAR&MEl Eft/TEST. DESCHIPTIGtf;'
160.1
Solids, Total Dissolved (TDS) Solids, Total Dissolved {TDS)
16D.2
Solids, Total Suspended {TSS> Solids, Total Suspended CTSS)
O'
LABORATORY
TEST
RESULTS
Laboratory Sample ID: 233695-1S Date Received...... : 01/22/2005 Time Received...... : 10:00
Date:02/04/2005 ATTHi Jat Kesari ! ! ! !
SAMPLE:RESULT;' :q FLAGS: ;;:i ;i : r L ; :
1200
B.4
30 4.0
: :rll-.
d i l u t i o n ; y HEi.Ts;:; :b a t c h : DT BATE/TIHE;' TECH.
10 1
mg/L
140702
D1/27/D5 1155 jmk
5.0 1
mg/L
140323
01/25/05 1227 jmk
STL Chicago
* In Description = Dry Wgt.
Page 19
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 233695
LABORA TORY
CHRONICLE
Date: 02/04/2005
c u s t o m e r ::;/Wes.tpn;.solutions, me .
PROJECT ! COMFIOENTJ AL OECATUFi:..: : : : : : t t m - jai- tt^ssri::
Lab ID: 233695-1 METHOD
160.1 160.2
client ID: DF09-GW-131R-0-041020 DESCRIPTION Solids, Total Dissolved (TDS) Solids, Total Suspended (TSS)
Lab ID: 233695-2 METHOD
160.1 160.2
client ID: DF09-GW-131S-0-041020 DESCRIPTION Solids, Total Dissolved (TDS) Solids, Total Suspended (TSS)
Lab ID: 233695-3 METHOD
160.1 160.2
Client ID: DFQ6-GW-132R-D-04102 DESCRIPTION
Solids, Total Dissolved (TDS) SoLids, Total Suspended (TSS)
Lab ID: 233695-4 METHOD
160.1 160.2
Client ID: DF06-GW-132S-Q-D41Q2D DESCRIPTION Solids, Total Dissolved (TDS) SoLids, Total Suspended (TSS)
Lab ID: 233695-5 METHOD
160.1 160.2
CLient ID: DF6-GU-133R--041020 DESCRIPTION Solids, Total Dissolved (TDS) SoLids, Total Suspended (TSS)
Lab ID: 233695-6
METHOD 160.1 160.2
CLient ID: DF06-GU-133S-0-04102Q
DESCRIPTION Solids, Total Dissolved (TDS) SoLids, Total Suspended (TSS)
Lab ID: 233695-7 METHOD
160.1 160.2
Client ID: DF14-GW-136R-0-040121 DESCRIPTION
Solids, Total Dissolved (TDS) SoLids, Total Suspended (TSS)
Lab ID: 233695-6 METHOD
160.1 160.2
CLient ID: DF14-GW-136S-0-D4D121 DESCRIPTION Solids, Total Dissolved (TDS) SoLids, Total Suspended (TSS)
Lab ID: 233695-9 METHOD
160.1 160.2
CLient ID: DF14-GW-136L-0-040121 DESCRIPTION
SoLids, Total Dissolved (TDS) SoLids, Total Suspended (TSS)
Lab ID: 233695-10 Client ID: DF14-GW-137S-0-04121
METHOD
DESCRIPTION
160.1
SoLids, Total Dissolved (TDS)
160.2
SoLids, Total Suspended (TSS)
Lab ID: 233695*11 CLient ID: DF14-GU-137L-0-Q4Q121
METHOD
DESCRIPTION
160.1
SoLids, Total Dissolved (TDS)
160.2
SoLids, Total Suspended (TSS)
Lab ID: 233695-12 CLient ID: DFBb-GW-134R-0-Q4Q121
METHOD
DESCRIPTION
160.1
Solids, Total Dissolved (TDS)
Date Recvd: 01/22/2005 Sample Date: 01/20/2005
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 140702 140702
01/27/2005 1110
1 140323 140323
01/25/2005 1205
DILUTION
Date Recvd: 01/22/2005 Sample Date: 01/20/2005
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 140702 140702
01/27/2005 1113
1 140323 140323
01/25/2005 1207
DILUTION
Date Recvd: 01/22/2005 Semple Date: 01/20/2005
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 140702 140702
01/27/2005 1116
1 140323 140323
01/25/2005 1208
DILUTION
Date Recvd: 01/22/2005 Sample Date: 01/20/2005
RUN# BATCH# PREP BT #() 1 140702 140702
DATE/TIME ANALYZED 01/27/2005 1118
1 140323 140323
01/25/2005 1209
DILUTION
Date Recvd: 01/22/2005 sample Date; 01/20/2005
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 140702 140702
01/27/2005 1121
1 140323 140323
01/25/2005 1210
DILUTION
Date Recvd: 01/22/2005 Sample Date: 01/20/2005
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 140702 140702
01/27/2005 1123
1 140323 140323
01/25/2005 1212
DILUTION
Date Recvd: 01/22/2005 Sample Date: 01/21/2005
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 140702 140702
01/27/2005 1126
1 140323 140323
01/25/2005 1213
DILUTION
Date Recvd: 01/22/2005 Sample Date: 01/21/2005
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 140702 140702
01/27/2005 1129
1 140323 140323
01/25/2005 1214
DILUTION
Date Recvd: 01/22/2005 Sample Date: 01/21/2005
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 140702 140702
01/27/2005 1131
1 140323 140323
01/25/2005 1216
DILUTION
Date Recvd: 01/22/2005 Sample Date: 01/21/2005
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 140702 140702
01/27/2005 1134
1 140323 140323
01/25/2005 1217
DILUTION
Date Recvd: 01/22/2005 Sample Date: 01/21/2005
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 140702 140702
01/27/2005 1137
1 140323 140323
01/25/2005 1218
DILUTION
Date Recvd: 01/22/2005 Sample Date: 01/21/2005
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 140702 140702
01/27/2005 1139
DILUTION
STL Chicago
Page 20
20
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 233695
LABORATORY
CHRONICLE
Date; 02/04/2005
CUSTOMER* Westqn;Solutions,, ine-.
!ffcJRCT: CONFIDENTIAL DECATUR
:ATThii Jai KcsaH!
Lab ID: 233695-12 Client ID: DF8b-GW-134R-0-040121
METHOD
DESCRIPTION
160.2
Solids, Total Suspended (TSS)
Lab ID: 233695-13 Client ID: DF8b-GW-134S-0-040l2l
METHOD
DESCRIPTION
160.1
SoLids. Total Dissolved (TDS)
160.2
Solids, Total Suspended (TSS)
Lab ID: 233695-14 Client ID: DFBb-GW-135R-0-Q40121
METHOD
DESCRIPTION
160.1
Solids, Total Dissolved (TDS)
160.2
Solids, Total Suspended (TSS)
Lab ID: 233695-15 Client ID: DF8b-GW-135S-0-040121
METHOD
DESCRIPTION
160.1
Solids, Total Dissolved (TDS)
160.2
SoLids, Total Suspended (TSS)
Lab ID: 233695-16 Client ID: DF8b-GW-135L-0-040121
METHOD
DESCRIPTION
160.1
SoLids, TotaL Dissolved (TDS)
160.2
SoLids, TotaL Suspended (TSS)
Lab ID: 233695-17 Client ID: DF09-GW-130R-0-Q40121
METHOD
DESCRIPTION
160.1
Solids, TotaL Dissolved (TDS)
160.2
Solids, TotaL Suspended (TSS)
Lab ID: 233695-18 Client ID: DF09-GW-13S-0-040121
METHOD
DESCRIPTION
160.1
Solids, TotaL Dissolved (TDS)
160.2
Solids, TotaL Suspended (TSS)
Date Recvd: 01/22/2005 Sample Date: 01/21/2005
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 140323 140323
01/25/2005 1220
DILUTION
Date Recvd: 01/22/2005 Sample Date: 01/21/2005
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 140702 140702
01/27/2005 1142
1 140323 140323
01/25/2005 1221
DILUTION
Date Recvd: 01/22/2005 Sample Date: 01/21/2005
RUN# BATCH# PREP BT #CS)
DATE/TIME ANALYZED
1 140702 140702
01/27/2005 1144
1 140323 140323
01/25/2005 1222
DILUTION
Date Recvd: 01/22/2005 Sample Date: 01/21/2005
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 140702 140702
01/27/2005 1147
1 140323 140323
01/25/2005 1223
DILUTION
Date Recvd: 01/22/2005 Sample Date: 01/21/2005
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 140702 140702
01/27/2005 1150
1 140323 140323
01/25/2005 1225
DILUTION
Date Recvd: 01/22/2005 Sample Date: 01/21/2005
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 140702 140702
01/27/2005 1152
1 140323 140323
01/25/2005 1226
DILUTION
Date Recvd: 01/22/2005 Sample Date: 01/21/2005
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 140702 140702
01/27/2005 1155
1 140323 140323
01/25/2005 1227
DILUTION
STL Chicago
Page 21
21
Job Number.: 233695 c u s t o m e r :1:Weston St ut ions t Inc.
QIJflL 1 T Y C O N T R O L R E S U L T S
Report Date.: 02/04/2005
i ; ; e e t :::eNIbMTlAL d e c a u r :: :::-. . .ATTN;:j;;sari:;^
Test'Method.
;T 6Q ,lX :
i. Method Descript i on:-.!:! Solids,! Total^Dissolved (TDS)
;.vSoijds-;- T o ta l- i soI vedi (TDS).;
Batch'. . i h:- >v:. ' -140702: ;:; .......qui prtierit! Ctte .; ; !:.!
! . - . . . . Analy ^i.T : Te&tTd/i^TDiS:.:
QC Lab ID
Reagent
Units
QC Result
QC Result
True Value Orig. Value QC Calc. F * Limits
Date Time
MB 140702-001 LCS 140702-002 I04LSTTS1 MD 233695-18 MS 233695-16 I04LSTTS1
mg/L mg/L mg/L
mg/L
8.40000 U 268.00000 1230.00000 1524.00000
250.00000 250.00000
8.40000 U 1224.00000 1224.00000
107 0.5
120
01/27/2005 1100
% 80-120 01/27/2005 1103
R 20.0
01/27/2005 1157
4 % 75-125 01/27/2005 1200
Test Method....... : 160.2-
.Mathd r e s c r i p t i on., : : S a lid a jo tja t ; suspended';(i,
:p-ar.gm^tgir>.^ -- n-...-t Solida Tolt^V Stis'poded
;.;.;.; a - t c h -_:i.i.J ; ; -qiifriiftl; Q^ -
. :i'!.!:-.:
Anygtv. -;. imlt ':!
t est Tode.; i T ss' ;:
QC Lab ID
Reagent
Units
MB 140323-001
mg/L
LCS 140323-002 I05ASTSS1B mg/L
MD 233695-18
mg/L
MS 233695-18 I05ASTSS2B mg/L
QC Result
QC Result
2.68000 U 194.50000 30.50000 126.00000
True Va Lug Orig. Value QC Calc. F * Limits
Date Time
200.00000 100.00000
4.00000 U
30.50000 30.50000
97
0.0 96
% 80-120
R 20.0 % 75-125
01/25/2005 1200 01/25/2005 1201 01/25/2005 1229 01/25/2005 1230
STL Chicago
Page 2Z
* %=% REC, R=RPD, A=ABS Dl'ff., D=% Diff,
22
Q U A L \ T Y A S S U R A N C' E" M E T H 0 L S'
E. T E R E N C E S . A ;:w:0; N O T e;'s:
Report Date: .O'V. 4/25
REPORT COMMENTS 1) All pages of this report ere integral parts of the analytical data. Therefore, this report should
be reproduced only in its entirety. 2) Soil, sediment and sludge sample results are reported on a "dry weight" basis except when analyzed for
landfilL disposal or incineration parameters. All other solid matrix samples are reported on an "as received" basis unless noted differently. 3) Reporting limits are adjusted for sample size used, dilutions and moisture conteht if applicable. 4) The test results for the noted analytical method(s) meet the requirements of NELAC. Lab Cert. ID# 100201 3) According to 40CFR Part 136.3, pH, Chlorine Residual and Dissolved Oxygen analyses are to be performed immediately after aqueous sample collection. When these parameters are not indicated as field (e.g. pH Field) they were not analyzed immediately, but as soon as possible on laboratory receipt,
Glossary of flags, qualifiers and abbreviations (any number of which may appear in the report) Inorganic Qualifiers (Q-Column) U Analyte was not detected at or above the stated limit. < Not detected at or above the reporting limit. J Result is less than the RL, but greater than or equal to the method detection limit. E Result is less than the CRDL/RL, but greater than or equal to the IDL/MDL. S Result was determined by the Method of Standard Additions. F AFCEE: Result is less than the RL, but greater than or equal to the methoddetection limit. Inorganic Flags (Flag Column)
ICV,CCV,ICB,CCB,ISA,I SB,CRI,CRA,MRL: Instrument related QC exceed the upper or Lower control Limits. * LCS, LCD, MD: Batch QC exceeds the upper or lower control Limits. + MSA correlation coefficient is less than 0.995. 4 MS, MSD: The analyte present in the original sample is 4 times greater than the matrix spike concentration; therefore, controL limits are not applicable. E SQ: Serial dilution exceeds the controL limits. H MB, EB1, EB2, EB3: Batch QC is greater than reporting Limit or had a negative instrument reading lower than the absolute value of the reporting limit. N MS, MSD: Spike recovery exceeds the upper or lower controL limits. W AS(GFAA) Post-digestion spike was outside 85-115% control LimitsOrganic Qualifiers (Q - Column) U Analyte was not detected at or above the stated limit. ND Compound not detected. J Result is on estimated value below the reporting Limit or a tentatively identified compound (TIC), Q Result was qualitatively confirmed, but not quantified. C Pesticide identification was confirmed by GC/MS. Y The chromatographic response resembles a typical fuel pattern. Z The chromatographic response does not resemble a typicaL fuel pattern. E Result exceeded calibration range, secondary dilution required. F AFCEE:Result is an estimated value below the reporting Limit or atentativelyidentified compound (TIC) Organic Flags (FLags Column) B MB: Batch QC is greater than reporting Limit. * LCS, LCD, ELC, ELD, CV, MS, MSD, Surrogate: Batch QC exceeds theupper or lowercontrol limits. EB1, EB2, EB3, MLE: Batch QC is greater than reporting Limit A Concentration exceeds the instrument calibration range a Concentration is below the method Reporting Limit (RL) B Compound was found in the blank and sample. D Surrogate or matrix spike recoveries were not obtained because the extract was diluted for analysis; also compounds analyzed at a dilution will be flagged with a D. H Alternate peak selection upon analytical review I Indicates the presence of an intorfonce, recovery is not calculated. M Manually integrated compound. P The Lower of the two values is reported when the % difference between the results of two GC columns is
Page 23
STL Chicago
23
q u a l i t y a s s u r a m c E ; -.-M.-'.--.li.=:H:f- i> 5^: R E F E R E N C E S AND N 0 T S ..... ...... ... Report Date: 02/04/2005
greater then 25%.
Abbreviations
AS Post Digestion Spike (GFAA SampLes - see Noto 1 below)
Batch Designation given to identify a specific extraction, digestion, preparation set, or analysis set
CAP Capillary Column CCB Continuing Calibration Blank
ccv Continuing Calibration Verification
CF Confirmation analysis of original Cl Confirmation analysis of A1 or D1
C2 Confirmation analysis of A2 or D2
C3 Confirmation analysis of A3 or D3
CRA Low Level Standard Check - GFAA; Mercury
CRI Low Level Standard Check - ICP
CV CaliIbrat ion Verification standard
D iL Fee Dilution Factor - Secondary dilution analysis
DI Dilution 1
D2 Dilution 2
D3 Dilution 3
DLFac Detection Limit Factor
DSH Distilled Standard - High Level
DSL Distilled Standard - Low Level
DSM Distilled Standard Medium Level
EB1 Extraction Blank 1
EB2 Extraction Blahk 2
EB3 DI Blank
ELC Method Extracted LCS
ELD Method Extracted LCD
ICAL
Initial calibration
ICB Initial Calibration Blank
1CV Initial Calibration Verification
IDL Instrument Detection Limit
ISA Interference check sample a - ICAP
1SB Interference Check Sample B - ICAP
Job NT The first six digits of the sample ID which refers to a specific client, project and sample group
Lab ID An 3 number unique Laboratory identification
LCD Laboratory Control Standard Duplicate
LCS Laboratory Control Standard with reagent grade water or a matrix free from the analyte of interest
MB Method Blank or CPB) Preparation Blank
MD Method Duplicate
MDL Method Detection Limit
MLE Medium Level Extraction Blank
MRL Method Reporting Limit Standard
MSA Method of Standard Additions
MS Matrix Spike
MSD Matrix Spike Duplicate
ND Not Detected
PREPF Preparation factor used by the Laboratory's Information Management System (LIMS)
PDS Post Digestion Spike ClCAP)
RA Re-analysis of original
A1 Re-analysis of DI
A2 Re-analysis of D2
A3 Re-ana lysis of D3
RD Re-extraction of dilution
R Re-extraction of original
RC Re-extract ion Confirmation
RL Reporting Limit
RPD Relative Percent Difference of duplicate (unrounded) analyses
RRF Relative Response Factor
RT Retention Time
Page 24
STL Chicago
24
0. U A L I T V A S'S U
kCE M
R E F R N C S
kD N0
Report Date: 02/04/2005
H D D S: S..
RTW Retention Time Window Sample ID A 9 digit number unique for each sample, the first
six digits are referred as the job number
see Seeded Control Blank
so Serial Dilution (Calculated when sampLe concentration exceeds 50 times the MDL)
UCB Unseeded Control Blank
ssv Second Source Verification Standard
SLCS
Solid Laboratory Control Standard(LCS)
PHC pH Calibration Check LCSP pH Laboratory Control Sample
LCDP
pH Laboratory Control Sample Duplicate
HDPH
pH Sample Duplicate
MDFP
Flashpoint Sample Duplicate
LCFP
Flashpoint LCS
Gl Gelex Check Standard Range 0-1
G2 Gelex Check Standard Range 1-10
G3 Gelex Check Standard Range 10-100
G4 Gelex Check Standard Range 100-1000
Note 1: The Post Spike Designation on Batch QC for GFAA is designated with an "S" added to the current
abbreviation used. EX. LCS S=LCS Post Spike (GFAA); HSS=MS Post Spike (GFAA)
Note 2: The MD calculates an absolute difference (A) when the sample concentration is less than 5 times the
reporting limit. The control limit is represented as +/' the RL.
STL Chicago
Page 25
CHAIN OF CUSTODY
CHAIN OF CUSTODY / ANALYSIS REQUEST FORM
Severn Trent Laboratories
T: 708-534-5200
F: 708-534-5211
2417 Bond Street
University Park, IL 60466
PAGE / Of 3
PROJECT INFORMATION Client: Weston Solutions, Inc.
1400 Weston Way, Bldg. 5-2 West Chester, PA 19380 T: 610-701-3761 F: 610-701-7401
Project Manager: Jar Kesari email: i.kesari weston solution s.co m
Project Name: Reference No:
Decatur, Alabama 02181-129-081-0001
ANALYSES REQUESTED
Sampler:
A. Murphy, B Wesley 256-552-6189
P.O. #: Quotation #:
SAMPLE ANALYSIS
ExyLIMS #
Client Sample Identification
DF09 GW 131R
041020
DF09 GW 131S
041020
DF06 GW 132R
041020
DF06 GW 132S
041020
DF06 GW 133R
041020
DF06 GW 133S
041020
Collection
Date 2Q-Jan-05 20-Jan-0 5 20-Jan-05 20-Jan-05 20-Jan-05 20-Jan-05
Collection
Time
12:20 12:35 14:20 14:15 14:45 14:50
zoo. O3oe
Sample
Matrix
WATER WATER WATER WATER WATER WATER
Comments
X X
CHAIN OF CUSTODY
Rei inguistyScLBxCi
Date
fV
Cooler ID No.:
Time
Received By: Fed Ex
Cooler Temp. (C): Date Time
//
PROJECT REQUIREMENTS
Results Deadline:
Laboratory Report Options: Sample Results Only Add Case Narrative Add Quality Control Summary Add Calibration Summary Add Raw Data Other:
CHAIN OF CUSTODY/ ANALYSIS REQUEST FORM
Severn Trent Laboratories
T: 703-534-5200
F: 703-534-5211
2417 Bond Street
University Park, IL 60466
PAGE Z of 3
PROJECT INFORMATION Client: Weston Solutions, Inc.
1400 Weston Way, Bldg. 5-2 West Chester, PA 13380 T: 610-701-3761 F: 610-701-7401
Project Manager: Jai Kesari email: i.kesariSweston so lution s.co m
Project Name: Reference No:
Decatur, Alabama 02181-129-081-0001
ANALYSES REQUESTED
Sampler:
E. Caldwell, B. McCaniess 256-552-6139
P.O.#: Quotation #:
SAMPLE ANALYSIS
ExyLIMS #
T J. r
Client Samp e Identification
DF14 GW 136R 0 040121
DF14 GW 136S
040121
DF14 GW 136L
040121
DF14 GW 137S
040121
DF14 GW 137L
040121
Collection
Date
21-Jan-05 21-Jan-05 21-Jan-05 21- Jan-05 2 1-Jar-05
Collection
Time 3:20
3:25 3:30 8:00 8:10
O
oo. co ZO
Sample Matrix
WATER
WATER
WATER
WATER
WATER
Comments Low Range Spikes Low Range Spikes Low Range Spikes Low Range Spikes Low Range Spikes
</> O H
X
X X
CO
CHAIN OF CUSTODY
Cooler ID No.:
ReJinquisf& jfrBy : -- tv _ * ' <
Date Time
f j / ' ' /
Received By: Fed Ex
Cooler Temp. (C):
pate Time
1/
7-^od
PROJECT REQUIREMENTS
Results Deadline:
Laboratory Report Options: Sample Results Only Add Case Narrative Add Quality Control Summary Add Calibration Summary Add Raw Data Other:
STL Chicago
CHAIN OF CUSTODY / ANALYSIS REQUEST FORM
U
Severn Trent Laboratories
T: 708-534-5200
F: 708-534-5211
2417 Bond Street
University Park, IL 60466
PAGE 3 of s
PROJECT INFORMATION Client: Weston Solutions, Jnc.
1400 Weston Way, Bldg. 5-2 West Chester, PA 19380 T: 610-701-3761 F: 610-701-7401
Project Manager: Jai Kesari email: i.kesa ri(o5westonso Iuti ons .com
Project Name: Reference No:
Decatur, Alabama 02181-129-081-0001
ANALYSES REQUESTED
Sampler:
A. Murphy, B Wesley 256-552-6189
P.O. #: Quotation #:
SAMPLE ANALYSIS
ExyLIMS #
M
/5
Client Sample Identification
DFSb GW 134R
040121
DFSb GW 134S
040121
DFSb GW 135R
040121
DFSb GW 135S
040121
DFSb GW 135L
040121
DF09 GW 130R
040121
DF09 GW 130S
040121
Collection
Date
21-Jan-05 21-Jan-05 21-Jan-05 21-Jan-05 21-Jan-05 21-Jan-05 21-Jan-05
Collection
Time
9:55 9:45 9:30 9:10 9:20 10:25 10:15
X
X X
zao. oco
Sample M atrix
WATER
WATER
WATER
WATER
WATER
WATER
WATER
Comments High Range Spikes High Range Spikes High Range Spikes High Range Spikes Low Range Spikes High Range Spikes High Range Spikes
CO
X
CHAIN OF CUSTODY
Relnquisjrd By^
Date,
Cooler ID No.:
Time f
Received By: Fed Ex
Cooler Temp. (C): Date Time
PROJECT REQUIREMENTS
Results Deadline:
Laboratory Report Options: Sample Results Only Add Case Narrative Add Quality Control Summary Add Calibration Summary Add Raw Data Other:
STL Chicago
STL Chicago Internal Sample Custody Transfer Record
Sample Lot#:_____ ___________________________
Client:
^
Sample No. i/ - z u
Analysis
75"5 /f/?<> 7iV ///? S
'' ^
Relinquished by:
Received by:
Date
yf_____________
.'i //
t-*V( f _
/-&Y ____ h ? j
*
Time
Comments
CHI-22-11 -001/C-1/99
rpjsckl
Job Sample Receipt Checklist Report
Job Number,: 233695
Location.: 57222 Check List Number.: 1
Description,:
Customer Job ID.... :
Job Check List Date.: 01/24/2005
Project Number.: 20004891 Project Description.: Confidential Decatur FC Investigation
Customer...... : Weston Solutions, Inc.
Contact.: Jai Kesari
Questions ?
(Y/N) CormiEhts
V2
Date of the Report..: 02/04/2005 Project Manager.... : rew
Chain* of "Custody Present?.................. .
.Y
Were samples dropped off at or picked up by STL?. . N
Custody seal on shipping container?............. . Y
...If "yes", custody seal intact?................ . Y
Custody seals on sample containers?.............. . N
...If "yes", custody seaL intact?................
Samples iced?.....,... .......................
Y
Temperature of cooler acceptable? <4 deg C +/- 2) . Y 3.2
SampLes received intact (good condition)?....... . Y
Volatile samples acceptable? (no headspace)..,.,.
Correct containers used?......................... . Y
Adequate sample volume provided?................. . Y
Samples preserved c o r r e c t l y ? . _____.......---- . Y
Samples received within holding^time?............ . Y
Agreement between COC and sample labels?........ . Y
Radioactivity at or below background levels?....- . Y
A Sample Discrepancy Report CSDR) was needed?___ . N
If samples were shipped was there an air bill #?. . Y
Sample Custodian Signature/Dato.................. . Y
F5age 1
STL Chicago
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STL C h ic a g o
CASE NARRATIVE
STL Chicago Wet Chemistry Case Narrative
Client; Job #:
W e s t o n Solutions, inc*
233695
Date Rec'd: 01/22/05
1. This narrative covers the analysis o f the samples in the above Job # for TSS and TDS by the methods cited on the Laboratory Test Results pages.
2. The analysis was done within the F.PA holding times. Refer to the Laboratory Chronicle Page for dates of sampling, receipt, and analysis.
3. The method blanks were less than the reporting limits.
4. The LCS recoveries were within acceptance limits.
5. The matrix QC done on sample 233695-18 was within control limits. See the Quality Control Results page for details of all matrix QC and non-matrix QC,
Wet Chemistry Section Manager
STL Chieggo
Date
34
RAW DATA
*** RUN LOG
***
CV2 ) 2/4/05 9:5B
STL Chicago
36
*** QC Summary
ft**
(V2 1
Solids, Total Dissolved (TDS)
Method Code..: 160.1 Batch Code,..: 140702 Status....... : RVUD
Batch Date...: 01/31/05 Batch Time...: 1425 User Name :jmk
QC Code........: STD Calc Code...... : TDS Location Code..: 57222
Grp Snip Sample ID
Pat Test Result
Known
OriginaL
1 1 ___MB__
7 TDS 4
12
LCS I04LSTTS1 1
1 23 233695_18__MD__22
7 TDS 7 TDS
268 1230
250
4 1224
1 24 233695J8_MS_I04LSTTS1_22
7 TDS 1524
250
1224
Report Date: 2/4/05 9:58 Equipment Code.: Import Code....;
Alternate QC Rea F QC Res
107 0.5 120 4
F
S'J L C h icag o
Page 1
37
*** RAU TEST PATA
***
(V2 )
Solids, Total Dissolved (TDS)
Method Code.. 160. 1 Batch Code... 140702 Status...... FtVWD
Batch Date.. 01/31/05 Batch Time.. .: 1425 User Name..T.: jmk
SAMPLE:
Grp Pos Sample ID
11
MB
12
LCS I04L5TTS1 1
1 3 233690 4
1 4 233690 5
1 5 233695 1
1 6 233695 2
1 7 233695 3
1 S 233695 4
1 9 233695 5
1 10 233695 6
1 11 233695 7
1 12 233695 8
1 13 233695 9
1 14 233695 10
1 15 233695 11
1 16 233695 12
1 17 233695 13
1 15 233695 14
1 19 233695 15
1 20 233695 16
1 21 233695 17
1 22 233695 18
1 23 233695 18 MD 22
1 24 233695 18 MS I04LSTTS1 22
Oc code...
STD
CaLe Code. .... : TDS
Locati Oh Code..: 57222
Di luti on
ID Text
IWGT
9
56.8473 53.9439 56.2312 50.1897 50.7190 73.2682 75.0538 50.4202 52.6617 55.1546 56.1498 54.4000 57.5849 77.2503 54.6896 55.6092 55.8765 52.7254 75.9411 51.5218 79.0490 78.0249 75.7677 78.2704
Rsport Date: 2/4/05 9:58
Equipment Code.: Import Code
UT1
9
56.8474 53.9570 56.25B2 50.2082 50.7356 73.2716 75.0570 50.4308 52.6636 55.1593 56.1545 54.4060 57.5934 77.2609 54.7004 55.6178 55.8785 52.7303 75.9437 51.5310 79.0536 78.0863 75.8294 78.3470
UT2
9
56.8475 53.9573 56.2580 50.2080 50.7358 73.2714 75.0571 50.4310 52.6633 55.1590 56.1542 54.4061 57.5932 77.2611 54.7005 55.6180 55.8787 52.7301 75.9438 51.5312 79.0538 78.0861 75.8292 78.3466
UT3 9
STL Chicago
Page 1
38
* * * RAU TEST DATA
***
Solids, Total Dissolved (TDS)
Method Code..; 160.1 Batch Code,,,: 140702 Status___ r.. : RVWD
Batch Date.. : 01/31/05 Batch Time.. : 1425 User Name... : jmk
SAMPLE:
Grp Pos sample ID
11
MB
12
LCS I04LSTS1 1
1 3 233690 4
1 4 233690 5
1 5 233695 1
1 6 233695 2
1 7 233695 3
1 0 233695 4
1 9 233695 5
1 10 233695 6
1 11 233695 7
1 12 233695 8
1 13 233695 9
1 14 233695 10
1 15 233695 11
1 16 233695 12
1 17 233695 13
1 18 233695 14
1 19 233695 15
1 20 233695 16
1 21 233695 17
1 22 233695 18
1 23 233695 18 MD 22
1 24 233695 18 MS I4LSTTS1 22
QC Code..
: STD
Cale Code
: TDS
Location Code..: 57222
Di luti on
ML mL
TDS mg/L
50 4 50 268 50 536
50 366 50 336
50 64
50 66 50 216 50 32
50 88
50 68 50 122 50 166
50 216 50 218
50 176 50 44
50 94
10 270
50 133 50 96
50 1224 50 1230 50 1524
(V2 )
Report Date: 2/4/05 9;58
Equipment Code. Import Code--
FUGT 9
56.8475 53.9573 56.2580 50.2080 50.7358 73.2714 75.0571 50.4310 52.6633 55.1590 56.1542 54.4061 57.5932 77.2611 54.7005 55.6180 55.8787 52.7301 75.9438 51.5312 79.0538 78.0861 75.8292 78.3466
STL Chicago
-- Page 2
39
Start Time; End Time:
Tf Lf )t&p
f o 7o 2 -
STL Chicago ITS / ITOS / IS180 / IVDS / ITVS
Page # Book# LabNet Batch#
92
Circle Method Used:
Calculations: TDS / TS / S180
A, TDS E 160,1; SM 2540C B IS160 (ROE) - E 160,1 (Field Filtered)
mg/l - ( A - B) / Cx 1,000,000 mg/L = (gross(g) - tare(g)] / vol(ml) x 1,000,000
C. TS-E 160.3; SM 2540B
D. VDS/TVS - E 160.1 and 160.4; SM 2540E Calculations; VDS/TVS
E. Drinking Wat^r/
mg/L = (A^- DD))// C xX 1,D000C,000
A " Petri Dish 4 Dry Residua Wt. (g)
8 =P*tn Dl*h Tare Wt. (g)
C -Sample Volume (ml)
0 Petri Diah+Rwidue after ignition (g
Balance #; Desiccator #i - W -
Muffle Furnace#: Furnace Temp.:
\
3rd TDS/ T5
Test Crud. Sample Tare 1st 2nd A or D 13180 VDS/TVS % Ree,
Sample#
Code ID vol.
B
A
A (Circle) Result Result RPD
(ml) (8) (s) (g) (a) (mg/L) (mg/L)
-LCSJ
<1 w t f o - y
-,
2.
Y
--- ^
J
. m L sm
fa te ? ? i
I S ) \ Q > J tr\ M d r% S *> n m
3, t y m n
n W Vl
7 U 7 //T
j -L *. 2 \ 7 f j n n 1 S t ? o 7 r , o t 7 / \
xM L S
SSbJ/tiSMxti \Se,n/d\
2.
V V
V /m
\ ix u n \ \ M \
\ n Ir
W. m x \
\Sfwm V i M d \ < H M l \
ltd.
- /y r -/i
'/. i
i . _ l # f l s y S iJ3 r Y S io T i\ $ ia % n
\ J f \/G X A /1! \ 7 f( H 3 l i
i _ m ' i o S l r t / t 'S IA V o f J V h !
j | i_
\ A f i/jx o Jj
i i' !
.
'H \
V f 1.
'l fi j
-u t \
A/
IJ m m
J s
iS o i vo ur
W M 7 M iW
H M m s U i n f i m x itx \
IlS r t % V ! 7 v \ m
l
J
i
U -!
;;
!.. ! .. .
:;
T k /A T
Sample # w m tr r
;-
j
\ \j
Spiking Levels (mg/L)
S K L_
L
1^ i 1
; : !
i i i
Stock Soin. 1ID# (LCS/MSV,
li ;i Il
Y f/X/
i
TW
:
S piking C alculation: Cone, of Stk. Soin, x Vol, of 5tk Soin, added fmLsi
Val. of S im ple used (m L)
ics
Analyst Signatur^
Date:
7 (>
Reviewer Signature:
3 7Date; A
`
CHk2M2-02S/^10/0l:
Solids, Total Suspended (TSS) Method Code..: 160.2 Batch Code...: 140323
*** RUN LOG
***
rss
0/2 )
Status....... : RVWD Batch Date...: 01/26/05 Batch Time...: 1016
User Name...... : jmk QC Code....... : STD Calc Code..... : TSS
TEST CODE
T S
S
2/4/05 10:00
Latatien Code** Equipment Code. Import Code___
57222
SAMPLE: Grp Pos SampLe ID
11
___MB__
12
___LCS_I05ASTSSlB_1
13
2 3 37 5 J____
14
2 3 3 7 0 6 J ____
15
2 3 36 95 1____
16
233695_2____
17
233695_3____
18
233695_4u___
19
233695_5____
1 10 233695^6____
1 11 233695_7____
1 12 2 3 36 95 8____
1 13 2 3 36 95 9____
1 14 233695_10____
1 15 23369511____
1 16 233695 12
1 17 23369513____
1 18 23 3695J4____
1 19 233695J5____
1 20 233695_16^___
1 21 23369517____
1 22 233695J 8____
1 23 233695^18__MD__22
1 24 233695J 8__MS_J05ASTSS2B,,22
Di lut ion
o04
OLTL in
TEST POS 7 Date / Time 1/25/05 1200 0
0 1/25/05 1203 0 1/25/05 1204 0 1/25/05 1205 0 1/25/05 1207 0 1/25/05 1208 0 1/25/05 1209 0 1/25/05 1210 0 1/25/05 1212 0 1/25/05 1213 0 1/25/05 1214 0 1/25/05 1216 0 1/25/05 1217 0 1/25/05 1218 0 1/25/05 1220 0 1/25/05 1221 0
1/25/05 1222 0 1/25/05 1223 0 1/25/05 1225 0 1/25/05 1226 0 1/25/05 1227 0 1/25/05 1229 0 1/25/05 1230 0
-
.... --
-- ....
... ..... ....
STL Chicago
Page 1
--
41
*** QC summary
**#
(V2 )
Solids, Total Suspended (TSS)
Method Code.. : 160.2 Batch Code.,,r: 140323 Status...... : RVWD
Patch Date.. : 01/26/05 Batch Time.. : 1016
User Name... : jmk
QD Code....... : STD Calc Code..... : TSS
Location Code.. : 57222
Grp Smp Sample ID
Pos Test ResuLt
Known
Original
1 1 ___MB__
7 TSS 0.33
1 2 ___LCSJ05ASTSS1BJ
7 TSS 194.50
200
0.33
1 23 233695J 8__MD__22
7 TSS 30.50
30.50
1 24 233695 18_MS_I 05AST$S2B_2Z
7 TSS 126.00
100
30.50
Report Date: 2/4/05 IOOO Equipment Code Import Code.Tr
Alternate QC Res F OC Res F
97 0.0 96
STL C hicago
Page 1
42
ftft* RAW TEST DATA
<V2 )
Solids, Total Suspended (TSS)
Method Code Batch Code. Status....
160.2 140323 RVWD
Batch Date.. .: 01/26/05 Batch Time.. 1016 User Name... .; jmk
SAMPLE:
Grp Pos Sample ID
11
MB
12
LCS I05ASTSS1B 1
1 3 233705 1
1 4 233706 1
1 5 233695 1
1 6 233695 2
1 7 233695 3
1 8 233695 4
1 9 233695 5
1 10 233695 6
1 11 233695 7
1 12 233695 8
1 13 233695 9
1 14 233695 10
1 15 233695 11
1 16 233695 12
1 17 233695 13
1 18 233695 14
1 19 233695 15
1 20 233695 16
1 21 233695 17
1 22 233695 18
1 23 233695 18 MD 22
1 24 233695 18 MS I05ASTSS2B 22
QC Code....... : STD Calc Code..... : TSS Location Code..: 57222
Dilution
ID Text
IWGT 9
0.1142 0.1141 0.1068 Q.1078 0.1138 0.1154 0.1139 0.1089 0.1078 0.1078 0.1147 0.1148 0.1076 0.1134 0.1082 0.1143 0.1082 0.1091 0.1087 0.1162 0.1080 0.1144 0.1160 0.1133
Report DBte: 2/4/05 10:00
Equipment Code.: Import Code--- :
WT1
9
0.1143 0.1531 0.1086 0.1085 0.1147 0.1173 0.1155 0.1097 0.1081 0.1105 0.1373 0.1155 0.1104 0.1173 0.1091 0.1166 0.1085 0.1141 0.1493 0.1179 0.1086 0.1207 0.1220 0.1260
WT2
9
0.1143 0.1530 0.1084 0.1086 0.1148 0.1176 0.1155 0.1098 0.1082 0.1106 0.1371 0.1156 0.1105 0.1174 0.1092 0.1167 0.1085 0.1140 0.1490 0.1178 0.1085 0.1205 0.1221 0.1259
UT3 9
STL Chicago
Page 1
43
A A A RAW TEST DATA
***
<V2 )
Solids, Total Suspended (TSS)
Method Code..: 160.2 Batch Code... : 140323 status....... : RVWD
Batch Date.. : 01/26/05 Batch Time.. : 1016
User Name... : jmk
SAMPLE:
Grp Pos Sample ID
11
MB
12
LCS I05ASTSS1B 1
1 3 233705 1
1 4 233706 1
1 5 233695 1
1 6 233695 2
1 7 233695 3
1 8 233695 4
1 9 233695 5
1 10 233695 6
1 11 233695 7
1 12 233695 8
1 13 233695 9
1 14 233695 10
1 15 233695 11
1 16 233695 12
1 17 233695 13
1 18 233695 14
1 19 233695 15
1 20 233695 16
1 21 233695 17
1 22 233695 18
1 23 233695 18 MD 22
1 24 233695 18 MS I05ASSS2B 22
: STD Calc code....... : TSS Location code.. : 57222
Dilution
ML mL
TSS mg/L
300 0.33 200 194.50 200 8.00 200 4.00 200 5.00 200 11.00 200 8.00 200 4.50 200 2.00 200 14.00 200 112.00 200 4.00 200 14.50 200 20.00 200 5.00 200 12.00 200 1.50 200 24.50 60 671.67 200 8.00 200 2.50 200 30.50 2Q0 30.50
100 126.00
Report Date: 2/4/05 10:00
Equipment Code.: Import Code___ :
FUGT g
0.1143 0.1530 0.1084 0.1086 0.1148 0.1176 0.1155 0.1098 0.1082 0.1106 0.1371 0.1156 0.1105 0.1174 0.1092 0.1167 0.1085 0.1140 0.1490 0.1178 0.1085 0.1205 0.1221 0.1259
DLFAC N/A
0.67 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 3.33 1.00 1.00 1.00 1.00 2.00
STL Chicago
Page 2
44
STL Chicago
Total Suspended / Total Volatile Solids (ITSS / IVSS
L a b N it B a tch #
/ 7#
Circle Method Used: A. TSS - E 160,2; SM 2540D D. VSS-E 160,4; SM 2540E E, Drinking Water
Calculations: TSS
mg/L = ( A - B ) / C x 1,000,000
mg/L = [gross(g) - tara(g)j / vol(ml) x 1,000,000
Calculations: VSS mg/L= (A- D ) / Cx 1,000,000
Paga # i
Boo
0C 3
7~
A P*tri Olah * DryRiu* W t (fl)
B -P v tn Dish T ar* Wt. (fl) C Sampl* Voluma (ml) D "P a th D ish+R aiidu* altar ignition (g)
