Document zoZ0o7XJavGv7mOq4JEwVaZGB

A ------ ::: mMssNeOmsiTmEsBeisOnoOnKsssdeOrNmr~ePeLneEnoTen~OntmeNreIoNrdSooeTerr~rtUtoCo~OrnN5... o Ad pASLEezd roptnere edsde1 eeroesrdpLrneeerd bermtr te er fm dre CONFIDENTIAL - SUBJECT TO A PROTECTIVE ORDER ENTERED IN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00000011 EExxhhiibbiitt 22660033 State of Minnesota v. 3M Co., Court File No. 27-CV-10-28862 3M MN04758351 `CHCEOONNNNFFEIIDPDEIENNNTCTIIAOALU-LN- TSSUYUBBDJJIEESCCTTTRITTCOOT AACOPPURRROOTT,TEECNCOTT.IIVV2EE7-OOCVRR-DD1EE0-RR28EE8NN5TT2EERREEDD IINN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00000022 I3MM_MMNNo04477S588335522 `CHCEOONNNNFFEIIDPDEIENNNTCTIIAOALU-LN- TSSUYUBBDJJIEESCCTTTRITTCOOT AACOPPURRROOTT,TEECNCOTT.IIVV2EE7-OOCVRR-DD1EE0-RR28EE8NN5TT2EERREEDD IINN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00000033 I3MM_MMNN0044775588336533 ON: oT WASISSUED TO: | ove __Zniinitstn|orTo!raodansdovsdy oview oh 036"A recinicaLNOTEBOOK NUMBER asd Laboratory - ~ d 0 4 "m7 23 -- "TTHHIISS NNOOTTEEBBOOOKOIIKSS TTOO BBEE UUSSEEDD AASS:: ((CChheecckk tthhee aapppprroopprriiaattee bbooxx)) J pe -- A TECHNICAL NOTEBOOK FOR THE ABOVE NAMED INDIVIDUAL, OR N A TECHNICAL NOTEBOOK FOR THE ABOVE NAMED INDIVIDUAL, OR [] A LOG BOOK FOR Name and location of equipment FORNOTEBOOK | THE WORKIN THIS BOOKCOVERSTHE PERIOD THE WORK IN THIS BOOK COVERS THE PERIOD (CCFEEONNRTTEENRROUUTSESEEBOOOONNKLLYY FROM TO FROM TO Rhone P! RPREECCEEDDIINNGG NOTEBOOK NUMBER RE SSUUCCCCEEEEDDIINNGG NOTEBOOK NUMBER SIGNATUREAND INITIALS OF NOTEBOOKASSIGNEEAND ALL WITNESSES: To RE AULA: (py LANG YOURFULL LEGAL SGNATORE, AND SIGNATURE AND INITIALS OF NOTEBOOK ASSIGNEE AND ALL WITNESSES: NOTE #1: (Print) YOUR NAME, (Sign) USING YOUR FULL LEGAL SIGNATURE, AND SRORPtcp UNRURIONAELSRSUAEDARSASLOG BOOK. BACHPERSON SIGN (do notprint) YOUR INITIALS. Nt CNR APPEBEAL RMSA RECORD This BOOK. NOTE #2: IF THIS NOTEBOOK WAS ISSUED AS A LOG BOOK, EACH PERSON WHOSE SIGNATURE APPEARS BELOW MAY RECORD IN THIS BOOK. loPaC iAnoer , e OlaFiAaQ ntiesSu o e lacglR~EDBACoTgEDe Lis ASemon Print Full N~e, (Clearly) -- Print F~ Name, (Clearly) (nA Same Fu~ Legal Si~ture Fu~ Legal Si~ature REDACTED las INtials ~it~ls Emplo~eNo. REEDOARCCTTEDE ~mpioyee ~o, mney Alles men Prim Full Name, (Clearly) Full Legal Signature Initials Employee No. P"Prriimnt FFuullll NNaammee,, ((CClleeaarrllyy)) - FFuullllLLeeggalSSiiggnnaattuurree: InIintiitaialsls na Gey Prim Full Name, (Clearly) Ge Prim Full Name, (Clearly) lise Full Legal Signature Men Full Legal Signature Initials Initials FOR SUPERVISOR ONLY: FTI AOAMRMASACUCQPQUEUARAIVINNISTTOEERDD OWWINITLTYHH."TTHHEE CCOONNTTEENNTTSS OOFF TTHHIISS NNOOTTEEBBOOOOKK.. E`Emmppllooyyeeee NNoo.. Emme Employee No. Employee No. PrPirninetPFlulll NNaammee,, (Cary) (Clearly) Ful Leg Signature Full Legal Signature EBmupplooyeeee NNoo.. Date Date CONFIDENTIAL. SUBJECT T0 APROTEGTIE ORDER ENTEREDIN CHHEOENNNNNFEEIDPPEIINNNTCCIAOOLUUN-NTSTUYYBDDJIIESSCTTTRRIITCCOTT ACOPURROT,TENCOT.IV2E7-OCVR-D1E0-R28E8N6T2ERED COURT, NO. 27-CV-10-28862 IN 22660033..00000044 see S3MM HMiNno0a47758354 P"'UTUhRiRsPTiOeOcShSnEEiOcaOFlVNToTtHheEEboNoNOkOTiTEEoBnBlOOoOOanKKto you by 3M. I is egal record of yo11u11da77ly22te35ch4n4ical wrk. The `mmTSmmaeahaatcninttusmtnerneTreeersesrdrcicicwnhnoonwhnwnihecchcienaiecrlcrnnhhNnoiiyytonnoogtg1uuehkbyykeouooeseoueueprkpr. ihtwwshosoiorsrnkrkr.e.eloccIIaoonnnrrddggtmeeomnanyaeeyoyrrauaddl,,ebetytttehhre3eemMrmmim.nooieIrrtneeititesssiiannaadffdoeloeerqrqgmumuaaaalatctcriiyeoyocnanasosttrhheedevvoiibbddfeeeeytntntotecceureer.r.iidnnTTaaahhicliciyossoutunnerrocottothtoeenffbbiflcooaaoowwlkkwinnsstohthhrhookeeuu.llldedTegghbabaleeel secured when not in use. LUNUSsSeEEtOOiOsFTFnToTHtEHeEbEoBoNkOaOTsEaOBciOarOKy K-- Uresfeertheniscenobtoeobkoofkoaisnafodrimaaryti-o-n aay~oplualhcceavteoe rgteoarcteohcoerrrddeyydoo.uuUrrseefefffootrrtttsso aaenncddoiirnndtteearrlaliccyttoiiouonrnssr---e-seaaanrdcanhassyaynodouurtroeocwwhnnnipcpeaerlrsswooonnaralkl arssesuufscceehhrmebaanlsscieeiidsdb,eeoaapsos,r,koddfcoaeatrtsaasinfsffrotroerommpmsayytaiooonuundrrymeeooxdxuipphfeeiarrcviiammeteiegnonatnttsshs,,eursileleulddus.stiUtaratsptierioooindntusstcotooirffeocnnn,oeerwwhdoldadeleelsvvyiiooconuesrst,,reemmseeercachrhiacanhniuicascanealddl ,taaennrceddhfneeeirllceeeacnclttcrwreoosonntriikcoc "mrraeeusllssaaetttmeebddbelwwimoeoasrr,dkkpeaarncnohddcreiionsnnsflfouosrgtrmeimpcaaatstiloiayonn,doaannmsttohthdheeeifwffiiicorrasrtttiossnaailssleeudsosaanenedn.diffniiepelddroeedvvuaaclltuuiaoattnii,oonnnoooftferrseessouunlltmiinnaggtennreieawwlsppurrosodeduduc,ctsrts.e.feAArllelneecnietrsrieteoss must be made chronologically, as the work is done. c"TaThlhebernnatooittoeenbb,oooaokkndmmuaasyey.bbee usda used as aa lloogg bbooookk ttoo mmoonniittoorrththe aaccttiivviittyy ooff eeqquuiippmmeenntt iinnccluhdiinngg mmaaiinntteennaannccee,, calibration, and use. I WYWRouRIaITrTeIItNNheGGaSSuTTtYYLLhoEEfothris notebook; so, te writin style shoud fit your work eds. When you ecogize {at you have a new ida, write it down in deta an have t ithessed immediately See DESCRIBING You are the author of this notebook; so, the writing style should fit your work needs. When you recognize that you have a new idea, write it down in detail and have it witnessed immediately (See DESCRIBING | oo`YorrYrOiOi"nUnUnvvReReeennNNdttiEiEyooWonnWuoorIIccDtDcceEEuumrAArprrbeeeebrddleaoloootwvvwu)eer.)rre. ttHHdiimoaomtweweae..evoEEvenvervrRe,e,n3ndd3iccissrrpcyycrpoopotvvtigeieccrrriianneemoosst"tewwesshsh,h,eeoaannwswwffyrooorirrieutterxttxeaeacnanmtmpiiinnvlpilettethh,y,iissS"aSnnnaoaodmmtateebb---oo-ooulhkksuuennssicchlhhh.ooawawtAtlhh11soo1:ow:w3,300ttohh-uee-rddTTiidesusacecsyosoddvvmeaaearyryyyy" lbobieernfe"fibinlleleleteeddwdwweiyeitotnhhutrommptaeainmncsyypuuentshsreeeanfftuuuollr,t,eebbduubatttoaddioiosskjjnooRiitnons3tteh3eddop,,rweeovvgtceehrnnatmtssh:;" s0soah,,occwinhhnaaytnnohggguoeerugattehocotppti.iivccissFtyiaannnaanddld/oo,rarfrwweoyourorsukkeafddruiielrr.eoeccAttiliovsooannc,ssabytboyiyoudndr,rrdaeaawawyviimnengaogyaf falaiobbnrsseeeybnnoeccuteerw,,tessieiimccnekki,t,oonoprriwacwnsoyoirnrikkntihtnieegrnonvoganonlteaabbnneooottotwhhkeeeetrronppsrrahoodojjaeewcccettthnffteoorcnarahotappeneebrgroiieoookiddn:ootefhfntomtiumergie,hs,t.mmFaaikkneealaalynn, entry if you entry othat are on to that efftoeacccoutnt vacation, leave of effect to account for your time in any interval between adjacent notebook entries. nECEConnOOtmtReeRorrRrRiieEnnEffCtoCohrrTaTmmnIaIatOoOtiinooNNennSSiiinnnttootdthrheaewnnnottoerbootuogkhaeashyebyoonuuoiaoobrbaomtiaanitkinitio,tn. .IitFeicosxcaaecmcpeptpleteedd,leegYgaaoll upprrarecactioccredtttoosiommmaceaktkeeheiccnoogrtrrraeecclttiio3onnwssrwwoiinttghh se"`nwsTcewohhhctimeitilieeooosinnrYyneaoooguultlfheiiaaannrirnffeeonoorermmmnmaieaaaskklttiiimiinonnpoenggondirssaarwtnanwraworneeontnnnntgttg1hrr,y,yroddsiiurnrnhagoawYyhwootbauuhtlrbreholaonnitcncookfykttoeoeaarbubmrrooooaoaouutkeknin,o,ddnntJjt.ohuhstesFettoniirdndnfrfreoaxaowrawmlmreaaagpstailssloeiain,nsnatgeigaflnnneoeysddoenliuia)nnreadeteigrcattohigohrnonroodngauualsggolohhlnminceieeot tnttaahchhnniernrddaoogluucctggoofhnhhnoatttrttiihhmnniseeuaubewteb,oi.lrocooI1cknfnk3.,ga. AnAibTbtoee;hnatieaobnhbtlsshleteeienetrrtagooadarl,dedervetvlmtiriarnainnieeekitvvaaeisgegteeiiihttmieseepacatosohhisarraltyrytae.snscIfotctfammateonneentltseeirhmmnyoetnerwosysintytyishtoofhafruuooetsfuuyinynnnododddutttethoahobereobbeoeeiinknneefoporrftrarroomog(rninenameetoyaaoioouutlnusseig(ossaoaorrnolremmdisodeeetenetthaisime)emrvw)eewasittlrasseyteaareicrnc,e,thgnuddataotoellolnrnyyioconcctotgoonggrrfcoorreoeebbacrcaaltmtcciaaankknntfttoddiooroymyccnooooauurortrirnwwoeeicnicilltn.tl iScctheh;rcriootnninsoootlnelosoaoggdific,caanmllyssaeekqqepauutgeehenne.ccceeaoanrnrddercreteffeeenrrtbrbyaaccokknttoothttehheeneoerrtreroobnnoeeoookuupssaeegnnettryy.o.uAAlalsrsoe,,bobetehsesuurrwreeistoeoppellnaactceeeriaannlgienienttfhorhromuragthoiouununnouugnsseheidnd sections of any page. ODDnEeSEmCoRSrIBuICNseGoRYfYtOiOIsUUnRRBotNNeEEIboWWoIkNIDiDEGEinAAprovidinag datfor an invention.Forexample, if at some later time: ylcHoOiilonnunaueereiiiftnminynyyddaaoojnttouuhhdrrraautanntcsooyycettouoeeorububafrooctddooyhii.kkisssccwIwnuunhhsoscessetheiinnodobnyyneoooowwtuuikhlitlateaihhssshtt""ianSelSeraaptftmtnroo"o"ovff,f(i(,dyssPpeioenlaeueagcrcWWeaeuRRdtntIoacoIdTTthdeaIeIayNfoN'yosnGGraddataSSinetTsTebciYYbnuLevsLelEseoEin,wlo,tinaaotobbhnwooe.ivvtFlteheihon))e"renhh,G,eaaanaxssnmadlfdm"eddwwp(rlrttreioeit,tfeeaaiefnryyaeooiitnnunucsvvrrioenennmnnegetteiwwibooalndniac,d,etkeeddaar0rrawtwaiwiwtmit'hthehaea page with you cryptic ote. clarity and accuracy. Include the page with your cryptic note). heart of your luncheon discussion with "Sam" (referencing back to the [INESSING "oNTW NTnohho,tIeetTbeeppubbeNteoorrEoonsskokSootssnSnsIsswwNhohioimotGtuennuleoeddssnsbbseiieennwwwggoyiryiotktonuiunernresngnsoseootsdnteeeabatbsdshooeossookoskooaeennmnnteaatprsrsriipepeossojosesssschhsitobobwuluieilddtaabbfhfetteeeyssrroooueemmonnteetrrooiitnenehesseewaawshrruheeopoemmUruavandiddensee,o,rrpspdrtoraeenffemeedrrasaanrwwbbahllhgayysaetwwtrisyittortohheuuiissannparoreooennnnwsweeoibroewdlkreeekileisGnn:kgfg.. p`ayaoyannnoogddu,ued rrbdahuacaactttestinivvoeetiiatahttt ceciseehhoswsmp.op.araTTegdgohehse.nee,.ewwI"fwiSihttothanneremekepspsianssaggugmmeneosucnisssthttffhsausulieiltlglgsonon1aff:dimhda3isesat0atoopa,--r,rhothtehhjTeeeeurcewffwtusiuwlidtlltianlnnteynheasa"smystmsoheeisuesaowcocrrroniintrothriitoteaibralssolssurircpabbteyyiotrnotvhghrietestbohwhowaoarbtootrdoorddardasrmrtsta`"aahahreneatsaanasgodtdbibteeaarenhineneraddgenntstnuuytpaannookkddguneeeewnsnrri.s.sbettlIIoeotfoottfhddhto"ee"or JhuplaunavngcceehhwhdwiaestisthhtchSrSeabawmemd,o,rbabdunust,ett"thwhSaaiattdmyeyoao-u,u-wwlrutohrnoetcwtheeiaataton1ne1ots:t3es0ttio-osy-cyooToruuurrerosssbdeeoalfyrl,taf"otbtibheneeaghawtteilltuunhnnecceshhshwwiaistiscthhoSraSranaommubnoadarteatrt11is11nt::ga33n00nodoointnntghTToauoteefysstdodahuayyew. ieyIdfneoytaotusou dhdeaesvsccerriidbbeeedsd.c.riRRbeeemmdeemmabbenerer,w, tthihdeeewwai,ittnntheessess date st witness is date is the legal (ormboration) daleof a corroborating he/she has an legal (corroboration) date of a document. understanding document. of the ideas `CHCEOONNNNFFEIIDPDEIENNNTCTIIAOALUL-N- TSSUYUBBDJJIEESCCTTTRITTCOOT AACOPPURRROOTT,TEECNCOTT,IIVV2EE7-OOCVRR-DD1EE0-RR28EE8NN6TT2EERREEDD IN IN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00000055 M_MNoaTS8385 3M MN04758355 IIIFNwITiNtIeAsLsI eSsVVSuSs.Te. FFtUUheILLiLLnStSAiIIaGGlsNNLiAAnsTTiUUcSaRRdEEoftheir fll name, the frst ime they 117234 witness work n your nochook coIthhfveeewyyrimmtnoueufsstststhesessiigngunonsteaaenntbhddoeoppikrrr.iiinnnIttfitttiwhahielesitirniffneuuslsltllesanndsaaimmogneef ttaahhnneiddirriinffnulsslleelrtntnattahmhmeeeeiir,iinitnwhniiietttiiafnaillersssstsooinntinmtghh,eeetaahppe1ppyrrSoowtpplrirtininaaetctseecseliiwsnnaoesrsrykootinnno tthyhhaoeevueiirnnhssniieoddteemebffSrroooionnnktt caonvdeprroifnththeenirotneabmoeoks.nIdf wiintnaelsseosnstihgen itnhseiidrefuflrlonntamcoeveirn,wsiitnnceesssionmge, istiigsnsattiullrensecaersesdairfyfitcoulhta0vertahde.m sign ASA aunTpdpTpoArrT itCnitHntghMT deiEorcNnuaTmA OmeOnFetFaSsnC SUsdUhPoiPnuPiPltH OdiOaRlbRseTToaIM ntINNttahGGcehDE eDidnOOspiCedCrUeN UmfMaM rnoEenEnNT tNtcTlToySvS0er,nsoitnecbeosookmpeagseisgnianturseisngalree difficult layer usi to ng read. perma nent nSdSdsiiooouggtuupnnebbpeeblloddeoer-otooiksrsnriigdmindneaetdiddiytoiacattlabualeepepmddeemeooaaanrnrndtsddegglsldduh0uaaeeottueeilinlddnodnssbbbguuyyeccahhsttahht4atheeaowcwaashuauaeteytyhhdodolrtpooro..ceeeruRRnmnmesesefauufnenrertrereeesentntnthhalccayareelettt(otteoh0haneeooioyytttnhhceceeeabarrdnnonnosspououketpptrpppbbmaooaeergnrtertreiiesennnmtmiggnlooyvddva.eooesdccdi,uun. mmgEEelaeeancnctlhhtassyaaenntlortosatutccsaahhittnmmtagaeeccnpnhhteteerdmdmmuu(tsao0stntettbbhhneeeet notebook may be made so long.as those documents are retained permanently. iaiCCnrnoofefmomopnrrmpuomutaatte0teiirroobnnddeicicssouokknenesttttadttaeieissnnaseemmddsaaoouyynnbbbstthheeieuaadtdtttiisaasscckfkohheeteetttddeertetssoocuuoppnnrppoodooitirerentbtgbssoodhhooaaakklnndpypdwaawrrggiereeitssstettesesssnnoociihllnonofafnnoogcgrrmtmaaaissattvthiihoioeenniaaernueucttctohhhoreoordrdrneeorrddeiecttiiaabniionntotshshkee.dannudooputtleepibblcoiocoaoaktkt.ee. Dccioosppkyyetaainnedds Diskettes are not to be used as substitutes for recording daily research activities in the notebook. EpEuaatccehhr ddaiinssdkkeestttoteefitsiswat0orebbeeuslldaa.bbeellTeenddawwdiditiththissouunf,fffiicccaiiceenhnttdiiinnsffkooertrmtmeaattmiiuoosnntttoobeiiddeseningtiinffeyydtitassnccdoonndtateetnnettdssbiinynccllbuuoddtiihnnggthttehheeauttytyhppoeerooaffndccowoimlm.- pneneneusvstseserluuoasspniiendnggbseohhiifinstsgwooaprrreehhremeurarsnelleedengg.taaIlllnyssaiisgdgendncaaiutttriuouerrndee,;1eppallhcachceeeddndiosiiiknncebatatoeosseekmaalplueeasddgt,,eb.lleaabbseeillgeenddedeennavvneeldloopdpeae,t,ediiddebennyttiibffyoyitinhnggthcceoomnaetunettnhstos,r, with the and wit- with the envelope being permanently secured to the notebook page. N`NOWOhTeTEnEBaBOnOoOOeKKboCoCOkOMwMPilLPlLEnEoTTIlIoOOngNNerbeuscd und is only partially completed the page following the las cary W bsshhoooohuukellsnddsaiihnnnoddouiitlcceadabttbeoeeo""sknnioogwnffieluudlrrtnahhoneedrrlodeenanntgttrereiidreebsbs"y"e wtwuhisiettehhsdutthahpneeedrrreeivsaaissoosonnnolnrybbeehpiiaennrggtniasssltitladeytedecd.fo.rmBBoopnotlctehhotveppedaarrrttahnialeoltllpiyynaggaannetddhfaoftfululhlloellywyoicrcnsooghmmeptphlileesettlaeeacddsqtuaenninoontttireey-.- raebehddeaovvtoewwuekimist((tehchcsdllheettohtaahuroeerllltydycch))ooebnnppetTrtreeesiincnnintghtttsesnneoddieocfdfttahhatlteehhniieNedrrondnnntoaoaaettmtmbeeeedobeb,o,oobkoossykiikCg,tg,hennnhteeehtaddsaeturtaap,htnnheddBereuviiinninnsloiioodtttiribieaanboollgeoneoddo2tkth2kthhe3hh-eiaaBnsisiSsnni.bbssd0iieeed3deeee.fnnrofIfpprrnrorottoonnhcptpteeoeccrvrnoolleovyvyrteereener.xbx.oeoetUUciocnnunkugtuutesietsdhdee,ab,ddteaahnnnnioeoddntcoettrbrhbheoaasottohtouekakarsllnsilsesswwdahhicinototqunnusuleeladsdesissnb,ebetsees- rheetruernSehdotuoldthbeeTneochsniigcnaalnuNroesteobroodkatCeeinntseird,eBhueildfirngo2c2o3v-eBrS-03. If the notebook is being returned unused, there should be no signatures or date inside the front cover. RaAAanencddnniooairtttedbiibssoKonenooeeekkpcceeemmrssa,sasyaayArrlyybbleeffnorrooeerrittayycaioiobnnuoueerorddkoosffnnoogmgrrououuisippntngg1tbo0ewwooorornnrekek.t.yyAeuAeafamfrreteerffr0dooolollynlnoooeewuwriyiynneeNggaaorrcctooyyemmoobpuuoploelmmektutiuisRoostenntcrrsoseeoorttudullrrKoonnennegtgthhpaaeeessrnnyybooooettueufebobrroroeeeoommkkayaititoonnouiyynntooruuhtahrnreesNNessoroaa,ttmmeeerbbeeootfjoiooorkbkbe oRbbooryyrreyctttteohehhrrreemedmaNiNiKndnooaaietfttteseeeepbbueooyycroooo.hukkuArrlRRleeceenmmoccoppooptlyrerlooddbiyyosKKmmoneeeekeenecspnpetetmsersrww,u,aisirotottyhhnnbeeoe33rcMcMrooe.y.tppouyyPPurrrnrooiieoofcdrrtotfhhntttootoeiyrrnnneoeooututittueurnerbmgbnNiooiwonnooogtgkkrekbmaam.oannaoAyoyoklitcbbeRerebebemoocmmaoooaikkardvddtteeeoKoyww,tethiheiteetphhceTTortteehphcbceeyhehnfanamoippicarcppeayarrllyoobvovNNeauaoollrttotereoeafqbbfnutooteshhoofseeekktrel,lCCdabebreofneonrttoritaearem-er-r r1ttttoho0ehercbbyoTeTerheedrrecceeehahdtntduniuriiicmnncfaeeaslydlduoNNcuttohoorottattneehhocbbeetoooTeTpooebyekkcochoiCChsnkenien.nicnectactcaerloelr.p.sNNysToTaiohthrntiyeiegssbbfoccooofoooorppkknyyyooCCtummeeeranbancytoyeoo,rnbbk.teeiBBpnrreaeueecgcttiaeanaausiuginsnsewieeesddooonbrbfofkyyttt.hhyyAaeeooultuuhthehiirgfofgnoorhhrarilltyzyuuievppssdeeelt0nenyosxs,ittcitaeteeiinnvpcvoteeyypeenwnyaaaahrrttmessnurrraaaeeeyftteoroebrefrfeqtwwturhhheeheeiqsictuciinehhnedffsoitotiberrmmmydmeeaafytrtiioiiottooumiinnrss TreeccohnrdiecadlinDiyreocutrorn,oLteabbooork,orcoypHyeinagd oofrnPoatteebntooCkoupnasegle.s is not authorized except where requested by your Technical Director, Laboratory Head or Patent Counsel. `CHCEOONNNNFFEIIDPDEIENNNTCTIIAOALUL-N- TSSYUUBBDJJIEESCCTTTRITTCOOT AACOPPURRROOTT,TEECNCOTT,IIVV2EE7-OOCVRR-DD1EE0-RR28EE8NN6TT2EERREEDD IN IN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00000066 W_NNoa7s8356 3M MN04758356 s~o,n,.o.r..m.e,crn..oooice = DO NOT REPRODUCE TTAABBLLEE OOFF i CONTTEENNTTSS T 147210 1 PROJECT NO. SUBJECT PAGE NO. 1 BE E e ET e REESE = Fr 1] H SEEsEEeEeSmSSaERnaAcEhEsiEnteeCs=RscSanCBciRaEesEeRnsRiE istaioE nEssl: FH HHH HEH 0 NANEEEEEE HHH HH Ban Bo : HEH nh. i Lo EEEERE HHH SEES HHH HH HHH H : TT EEE cas est ie E --H [TI ~H H } Ee an [e= Sleas | S1aEsEsmE--ESEEESmH SEpEENamNaS=ESRNSNHEHRrSoEBeEN + En 3 EE [| =m Ee e ee - TT Ee ee + | Ea 1] C | ima eset =i eT HEH Hl 1H EN H - Hl Emm NEE HH EES ours sa COHNFE IDEN NTS IALN - SS UBJE ECR T TE O ARPRE OTECTIA VE ORDER ER NTERED IN - HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 3M MN04758357 2603.0007 wens... TABLE OF CONTENTS 11723% 3M RESTRICTED DONOTREPRODUCE TABLE OF CONTENTS 1 SUBJECT PAGENO. 2 HS H SF HEE EHE E EH EHR EH EHHE H HHH EET HHH ~o ENEENEEEEREEE HEH HL at wT 5 | Had [T1111 |11 TTT E LBoe EN EseSRSSHNIENANNRE ~ 20 3 HH [TT] as Et SiEREaERnn _ H [TTT H HHH HHH SH He ~0HHH SEEEEEEEEEEN H 1 g LL] 1 EE EE ETHH g5 EE CEE rr rrr EH EE TT HH HA EH EEEEH HH : [] rE I 1. I HH ee CONFIDENTIAL - SUBJECT TO A PROTECTIVE ORDER ENTERED IN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00000088 sons 3M MN04758358 CETT ETE o~,n,=o.,~rsm.-.e.cm~-aoonc: DO NOT REPRODUCE TTAABBLLEE OOFF CCOONNTTEENNTTSS 1 PROJECTNO. SUBJECT CT HE 11 3 EEEEEEE EE ESSHSSanSSHICHIC 5 THeH EEeE HENNEEEE BS [] Ee eee 10 a ESSE caESEEEEd m 15 F BR eE aeTcamREaSt Za [1] FE r E _ 2 HEH l~ 25 SEREREE H AHH EEE E H E ER H E ~0 H HT e H TH H ~5 HHHAHAHAHAHA TT HEHEHE HH HH RT ~o mE [ITT I CONFIDENTIAL - SUBJECT TO A PROTECTIVE ORDER ENTERED IN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00000099 susnorisss 3M MN04758359 w=,,r,,,,e~ss~-m,,,ce,-oroer TABLE OF COONNTTENNTTS 117234 DO NOT REPRODUCE i TTT FH pone $ 1 PROJECTNO. SUBJECT - HAE HHH I TT gE5 i ~ HHH EE +H HE e se i HSaEs fEn10 En HPHEH Eee HHT TH 1] [| HH EH HHH 1 HH 1 sEoEE SSHSSSRISSEENAET ET 3111] Fo~ ~o FH H HH HTH [111 1 LL Eon ed go] [| He ITT E E Lb EE E eH C,25 p oo HeeHEH lTh 30 TTh1ABN[1i]EeadiseeasI]EEaEy EE H He 35 EAESEeances cscsERR EE EEEEEEREN Emms 1 40 Bes Cr IT | EREENN HH A `CCOONNFFIIDDEENNTTIIAALL -- SSUUBBJJEECCTT TTOO AA PPRROOTTEECCTTIIVVEE OORRDDEERR EENNTTEERREEDD IINN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00001100 33MM_MMNNO044775588336600 is 3M RESTRICTED OO.OTREPROOUCE GG LL OO SS SS AA RRYY roNO. 1172308 H HH HEE r EE HH REE rT eee rr HHH TTT] 0 [TT TTT HHH H EE1E ] T H Tea E eeH 1 F BSeeasameH EEH =mH aEH Nh EH RRRESnEEE==agsss=[s] ee ET HT] 11 SHE HH E E 2 a h A aSea aRaH E EnE a EH RaA HHH HHH FE EaE 1 HEHE HE 1 IEEE EEEE HHH I Shee HH Fe HHH I ee CONFIDENTIAL - SUBJECT TO A PROTECTIVE ORDER ENTERED IN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00001111 sma 3M MN04758361 - aT 1 PROJECT NO. TE Ca Obj :cti~e: 3M RESTRICTED -- DO NOT REPRODUCE SUBJECT: NOTEBOOK NO. ~ ~ PAGE ~ 6 5"1c1 HEe r eee He TM H EAo TIT g SeEe on a a [2a] | ~ ~o L E E HH ~25 H SL30 ara BT ~ ' jh Con HH EE h f ST n WITNESS'S FULI~ NAME orINITIALS +RLE EE Ea T it 5 DATE: (READ AND UNDERSTOOD) CONFIDENTIAL - SUBJECT TO A PROTECTIVE ORDER ENTERED IN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 2603.0012 3M MN04758362 sunestRTED ~ coorREPRODUCE oe . 11 PPRROOJJEECCTTNNOO.. T EECEIT NEEEET TrIr FF EH EH EEEA EE Ob'ecti',e: 3M RESTRICTED -- DO NOT REPRODUCE nNoOtTeEBsoOoOkKnNoO.. SSUUBBJJEECCTT:: LL PAGE '1~ '4~ 77 22 3~/4~ 77 DDAATTEE:: 5/j2%) 5 Re]ererce: F/ C] T T P A E s lHi eris Se dea A HERE. il Hl TPH tig abo Te wa a1 : lO Copbpf 1ea ld l7an [ I S al V |ooh [pdoAe adAY|TR T]P SW Iz H a TB a a1 AFarTtH]I Tal Re zgd| [TTCTHe TT oo rm]E bo T FH a] E E | [de esl ed HH INN al TLSeriH] Gor|] i)3 0 fs] d22t 7Jot]m|o|s 7et] A dk12P4Y F 5 EED 3T|| yu ol T eAa]pI lkigahO e [= SebinEEEY RE A ST Tr pe pia HHH | H rd E EE ahd TT cara] dH Pa EEEEEEENEE EEEEE E EEEE EEE E EHH TEEET] |aumionsru Navecrs is4Chinas vate: 5/22/98 AUTHOR'S FULL NAME or INITIALS DATE: WWITINESTS'SFNFUULIE~LL NNSAAMMESE oorr'INISTIALINSTIALS. Cr (READ AND UNDERSTOOD) DDAATTE:E_: Be ET Soa 0. un nes `CCOONNFFIIDDEENNTTIIAALL -- SSUUBBJJEECCTT TTOO AA PPRROOTTEECCTTIIVVEE OORRDDEERR EENNTTEERREEDD IINN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00001133 33MM_MMNN0044775588336633 Mresmer-coRONE 3M RESTRICTED -- DO NOT REPRODUCE 1 33h oe PAGE ! 1 pomern0. 1 PROJECT NO. | he )bjtcti ~: fi at Eft 1]5 ~eflrenle: ] sSuUmBEJEcCTT:: [] OTE OO --- ! 8 = DATE: Sluis i. 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OT Z rI 1] / L: EI H CO a5 ~ HC[HE PTnT-- EHAE -- H ;IFOH TAE R HA E E EE E IA1 AUTHOR'S FULL NAME or INITIALS ---- Toon ps WITNESS'S FUIiL NAME or INITIALS (READ AND UNDERSTOOD) DATE: DATE: BEEN COAT SITES Soe R05 cu Tosser `CCOONNFFIIDDEENNTTIIAALL -- SSUUBBJJEECCTT TTOO AA PPRROOTTEECCTTIIVVEE OORRDDEERR EENNTTEERREEDD IINN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00001155 33MM_MMNN0044775588336655 fp1 PROJECT NO. 33MM RREESSTTRRIICCTTEEDD ----DDOONNOOTTRREEPPRROODDUUCCEE 1, PAGE ! wormsooce. 11723" 10 NOTEBOOKNO. suger: ote:_s/ay fas SUBJECT: DATE: I AI on EySNA TL Te iz [TT [1] LH TH [IIMethod| Quthopment || EEEEEE [] [] EHH ei et oy Heer HH 1] drach k 34 HH I AHHH] I] [I [] CI ed Jelp| TefalboarRd Bel+ltd gel) Tra] HHH | EEN HH I 2 EEEEmEEEEEEEE & Mado | [TTT TTT] [1] = [TT rrrrr Bah a on | z . Toth [Gl Cro J N Bol[LHI dee pbe ul HHH EeTT | n 1 [] E nahih Haka eoy n 8 HHH HH eda Gobind || | | - CT] TT Siddad dmg 11] HEbi 1I bl LTT] 2 1S el | Lotmal ating HHH Rap 18[ecotd pel " wilshoblh|gacnlasmide] P95 9 CQPO LTT [] EEE pls hlCe H ral ERE b |& Eick d sith |Mepi Hp STE eh a --NYNNYNDAH [|Teoh Jfbmet] | [TLL TIT Fe Sa ba De i sft H] [Tr Cr er . 1 amorsruLLNavEorrvmas Of A Qi pee Slaula i AUTHOR'S FULL NAME or lNITIALS ~-1~ A- ~J~ DATE: Cr . I WITWNEISST 'S FNULE L NSAMSE oSr INFITIUALL S LNAMEorINITIADLADATSTEE:: (READ AND UNDERSTOOD) Be ET Soa 0. un nes `CCOONNFFIIDDEENNTTIIAALL -- SSUUBBJJEECCTT TTOO AA PPRROOTTEECCTTIIVVEE OORRDDEERR EENNTTEERREEDD IINN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00001166 33MM_MMNN0044775588336666 i 1 PROJECTNO. PROJECT NO. rT mons notesookno. 3M RESTRICTED -- DO NOT REPRODUCE NOTEBOOK NO. suBgECT: _ SUBJECT: cePAGE 1177m22am344 5/1121135 DATE: S/27/% FReE dHnHa HEHEHE HT 5 rt Bobs Hr LHEim eee r HH L 1 E san gyHcdlic)BiD ka er s pl feE t T Sp ae rh, z] LR ig ET Heradhtd oHST ] =Hi El aA aiTTgee aE Fr HE L[hig opHe HChl pr ff [ve f pH a HF EHmL eSmpEeee hn hal 3 pH pee HH 1 Te apc Rai rn Ae ye FR ee 35 C PIr AT Te m]onTE TME EESE EERA LI rsp AvUtTnHoOrR'sSFFUULLLLNNAAMMBEoorr IvNTITiIaALLsS WITNESS'S FUI~L NAME or INITIALS nAOman pDaArTeE:: shalsa DATE: (READ AND UNDERSTOOD) ERR SAT CONFIDENTIAL - SUBJECT TO A PROTECTIVE ORDER ENTERED IN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00001177 sumer: 3M MN04758367 E TT\ Tomen pTte y n naE bseper pE amHm ws: sf RB - 1 PROJECTNO. woreso4o4k7n2o3.4 12 `33MMRREESSTTRRIICCTTEEDD ---- DDOONNOOTT RREEPPRROODDUUCCEE PAPAGGEE. t NOTEBOOK NO. ~ ~ ~ ~ ~ ~" 12 SUBJECT: DATE: ~ HHH TH i g . 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Re Hn EEE HERES )bj :ti~ Ee 5 {el :en 3M RESTRICTED -- DO NOT REPRODUCE NOTEBOOK NO.~ ~ "/ ~ 5 ~" SUBJECT: DATE: PAGE 14 L Ee [ Dabur bebesck == | Cha ck e| Midicoo 0 eli _ | TE lO Flor I] NACET 15 er NIEE1S HLEo NEEr RE ba so 2O Bostce TRL. Es A~ LPT P THT [1] : mT 25 E FOE REfnEaeEriTn Ch Lge aff ori _hobhing onl Lor hele] CEa5 ESel al be ATT AUTHOR'S FULL NAME or INITIALS ~ ~. ~ ~.~n~. DATE: WITNESS'S FU~L NAME or INITIALS (READ AND UNDERSTOOD) DATE: CONFIDENTIAL - SUBJECT TO A PROTECTIVE ORDER ENTERED IN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 2603.0020 3M MN04758370 J S sawn ----2--es PROJECTNO. 3M RESTRICTED -- DO NOT REPRODUCE NOTEBOOK Nq ~ 7 2 ~ ~" SUBJECT: DATE: PAGE 15 4 ET Tr rrrrr EEE EE I HE LEE [TTT H 1 Clas|se[Chick brmala | TTTTTTTTTTT] CEE Te HT HEE 1 8 EE ANNAN | efacfod | TCR [TTF LoTI CTT mg (sid || [1] SFSNP MMMM | 1111 Fe HH |EEREmmaRmDTnE LIT rrr ETT BH gH FH rrrrr TTT B EEREREeeTe ree nt HY EE NNN HimsT eshemT ar HEH HH H [ ~- Tbrrr ! HH HEN EENN NEE E = aE EE I] HE pe mons HEP eH PH ee I Te Ll [1 [1 mHoRSFULLNAMEceria Sf ACn owe Llaslaa AUTHOR'S FULL NAME or INITIALS DATE: WITNESSFULL NAMEorINTTALS ee---- WiTNESS'S FULL NAME or INITIALS DATE: (READ AND UNDERSTOOD) ee CONFIDENTIAL - SUBJECT TO A PROTECTIVE ORDER ENTERED IN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00002211 suman 3M MN04758371 3M RESTRICTED -- DO NOT REPRODUCE PAGE S55 EET wt 1,PROJECTNO. Thee] 1 aia mn 15iHeH" HE Hl HH |o e jaan: ur HH TH H SUBJECT: CTL TH a) Sa NOTEBOOK NO. 16 DATE: mmm | gubsemun A L HE nT ee HE -- tau LL Z,, + Fr agaR te B3 lk SHHE Jerhr HAh pr 25 TF r se iiHEEik Eh HH 0 * a PF aaaaal HH I EE i Hifr i eT 5 r renin AUTHOR'S FULL NAME or INITIALS = WITNESS'S FULL NAME or INITIALS SE FH DATE: DATE: (READ AND UNDERSTOOD) CONFIDENTIAL - SUBJECT TO A PROTECTIVE ORDER ENTERED IN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 2603.0022 3M MN04758372 J -- 3M RESTRICTED -- DO NOT REPRODUCE oePAGE ECP fe REE NNoOtTeEsBoOoOkKNNoO.. '1~ ~47? 223~4L 1177 TT 11 FPRROOJJEECCTTNNOO.. TT SUSBUJBEJECCTT:: DDAATTEE::3oifas I Impet Ob ~cti,'e: C CC H H EE EH TT] T[ Hafoird 41 dFA ply ||EC C FO HAE IA aR ] l or op tid SEabeod bbeed d ad l PTTm r Thsvp ]e nds EEEEEC E T| TI TolrH leh b I CA B2e dLitel] ] gstpChTela TIL co [gd BEomhmon ET5 Re Fa E r E EEE A= ENNEE teT SHEE o ANEEa Na ERLSETREEEEEEEEERERAE Beg ana pahs alaa] L | epssLEE ERE E BT H CF FEAEENEEF NEEREEEr ESEANES AE ] C CT res d oro CA mePT e T FH = Her HHHe HH HH C Co HHHH EL E s TH H1 H = I E Er ET HT FT T eP e r CT HTFTT HBE armors ossOnA Clr owe told AUTHOR'S FULL NAME or lNITIALS (~;k ~ ~- DATE: TR IWWITINETSNS'ES FSUSLSL'NFAUMLELorNINAIMTIEALOSr--INTTIALS (READ AND UNDERSTOOD) DADTAETE:: EE `CCOONNFFIIDDEENNTTIIAALL -- SSUUBBJJEECCTT TTOO AA PPRROOTTEECCTTIIVVEE OORRDDEERR EENNTTEERREEDD IINN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00002233 33MM_MMNN0044775588337733 1 PROTO. I PROJECTNO. _ suc: CN owe: gag 33MM RREESSTTRRIICCTTEEDD ----DDOONNOOTTRREEPPRROODDUUCCEE PAPAGGEE. - N.OOTTEEBBOOOOKKN.OO.. ~4'~7'123-3,'~ ~ 1188 SUBJECT: --DATE: ~ ETE EE Feb fat ada HE ff mibELpe e flme e Elee T n 0HH: Eh tr frre eo L r Z pTTtoe aEn 0 25 pe OH Eee kL 30 I PAE mi FAA HT 1 Hi 35 SH mors rou avg entra shGn AUTHOR'S FULL NAME or INITIALS ~i ~,, ~r pe Hof DATE: [WWIITTNNEESSS'SSFFUULLLLN~AAMMEE oorrINNIITTIAALLSS eran (READ AND UNDERSTOOD) PDAATTE: -------------------- ee CONFIDENTIAL - SUBJECT TO A PROTECTIVE ORDER ENTERED IN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00002244 soon 3M MN04758374 Hr ee + some. Iii]l PROJECTNO. --_ 7234 Slain 33MMRREESSTTRRIICCTTEEDD ----DDOONNOOTT NorEsook RREEPPRROODDUUCCEE 0. 2, 19PPAAGGEE .19 II Fh Corba L LRk H H . LLo H 117I HHH HHH HHHAH diet $36 ~ u [E:y =y PY [17ee || is.C0 bie] 38 Gandy hoz Hp tes dd 3 ] Hyd Ea & 7 El[Sr = TTS [I fe Trxy Tr rT rrr rT I E 0 e ee ma [Er rrrrr errrrr rrr 11 [BulTTTTTTTIETTT al IT] [1 [ 3 1] E 2 d 5 EE HEH : EEE Ig8a HTTTTTTT T 5 OT TTTI A A LH A 3A I RP PH aH H Hy I 0 1 1 PTT] 1I LLLI i 13 1 Heesr wt TTT eS TTT PTPTE A LEE TTTTTA ETT ! T EE T TTTT LlsTT T=" = TA LwoS mnowsrT o asgeemais dee Clonee Ta ToTr TFET Foalsa WITNESS FULLNAME INITIALS AUTHOR'S FULL NAME or INITIALS WITNESS'S FUI~L NAME or INITIALS WRoeETod On, are: DATE: - (READ AND UNDERSTOOD) [1 Hl ;1 HENNEPIN COUNTY DISTRICT COURT, NO 27.01-10.28862 (CCOONNFFIIDDEENNTTIIAALL -- SSUUBBJJEECCTT TTOO AA PPRROOTTEECCTTIIVVEE OORRDDEERR EENNTTEERREEDD IINN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00002255 33MM_MMNN0044775588337755 wer sors 3M RESTRICTED -- DO NOT REPRODUCE PAGE 1 PROJECTNO. IT] SUBJECT: .OTE.OOK 2O TITDATE: n l i eT aEEE HEEre HEL a [| EERE E FsEt A Aaaoen Fo Aseken oe otLd HET i Fence : SF SEB BHHeeEEpe he Ee H m ee mH130 FEE H EEE HH LE EEE T H HHH HH HTH 35 CH ee TT I messsoanns Tinn AConeia pos, ali ~,UTHOR'S FULLNAME orINITIALS W(ITNWESSI'S FT IJLLN NAMEE oS r INIS TIALSS FULLNAMEoCDDAI ATTEEN :: ITIALS (READ AND UNDERSTOOD) ERA SE LT Se CONFIDENTIAL - SUBJECT TO A PROTECTIVE ORDER ENTERED IN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00002266 sone 3M MN04758376 1 moreno TTTTTT] 1 PROJECTNO. He -- Ob I~cti,'e: ET TE 0RESTRICTED--DoNoTREPRODUCE pace 3M RESTRICTED sumer: -- DO NOT REPNRoOOrTDeUEsCOEoo0x"7254, PAGE 32121 SUBJECT: HHH [TITTTI IT TTT 1s |meter|e|n|k|e|: ror Ir 5 Ret ~re~ :e: rrrrrrrr rrrrrrrr rd rr THE HH EHS 1 HHH le TTT 10 TTT ITTI HEESE HHH H s SH HE Ho E 2 FT EEE Zo [TT ] I5 .'~ 15 ] EEN I ETT TrTrey Fee E_~ e2o HH HHH I] BH HEEHHHHHH HHH Eee ST gal ([TTTTTTTTTT] HENNE HH AH Cee HHH H HHH [TTT HHH [a TTTTTT 30 HHH HH [1 LITT HoH EEE EEE BRR SEEeRnAnsEEERRRRREERRRREEEE [1] [| He HHH TT HEH HH [1 II EE EEe RRSREeansEee 1 1 HHH TTT Ir TT rad wrorsro avons AnA Chien pee AUTHOR'S FULL NAME or INITIALS DATE: WTSSRUE L RO EN D STOON n EwN m TAS WITNESS'S FUI~L NAME or INITIALS (READ AND UNDERSTOOD) DATE: EERE [TTT TENNER COUNTY DISTRICT COURT. NO. 27-0110.2882 `CCOONNFFIIDDEENNTTIIAALL -- SSUUBBJJEECCTT TTOO AA PPRROOTTEECCTTIIVVEE OORRDDEERR EENNTTEERREEDD IINN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00002277 33MM_MMNN0044775588337777 1 PROJECTNO. 3M RESTRICTED -- DO NOT REPRODUCE SUBJECT: NOTEBOOK N~. ~ ~ ~" "~ ~' DATE: PAGE 22 HEH HoE ElEE T ae mn 1 I] HH Hl HT mE HE [IT B E FB rFe SE -RHEeE h e e oH E] e eh e eH E e e SHHa E EeEA HE Hn I AUTHOR'S FULL NAME or INITIALS WITNESS'S FULL NAME or INITIALS CONFIDENTIAL - SUBJECT TO A PROTECTIVE ORDER ENTERED IN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 2603.0028 3M MN04758378 SMRESTRICTED -- DONOTREPRODUCE pace 1, PROECTNO. 3M RESTRICTED -- DO NOT REPRODUCE sumer: noresookno 1172o3ar4: NOTEBOOK NO. '~ '~ ? 2 ~ l,~. 23PAGE 23 TITT 1 PROJECTNO. TTT TTTT SUBJECT: HHH DATE:FHA CZ )bjl .~cti' ~: HHH HH 1 1 He HH FH [TT JRE 7 HEREEEN I HAH ~eft ;rer :e: HHH HH HHH HHH [TT] HH HAH H [11] CHEER [1] ERNE EEE TT] 10 HHH er rrrrrr rrrrrTr rrer H[A ]H H HH H HEH HR HE 1 H Lb [] HHH [11] eH HHH HE ee] Zo [CITTETE | Eg1H ] H HH H H b H ebe |] HH[1 aN LE 1 2] HHH LLLP slLH [TT HHH EHH |e 20 CTHHH Ler EHH HHH 2] 9 |fgas25| T1i] HHH [TTT HHH [1] Hee EHERHEH HHH [LITT Fee HH HAH HH H HHH [1] CT Ee SSSmmiEan [la | HHH H H 30 HH HH HHH I EE HH Lr | -H HHH HHH EH errr rT Heb la]TH PITT H35 HH ] HAH rrrrrr I] HHH I] HHH EEAEUTFULLHNAMOEocRirSs EOeEEAEChNEENEEEwEwN [1 [] ~.UTI-IOR'S FULL NAME or INITIALS __ DATE: mn WITNESS'S FU~L NAME or INITIALS ED ORTO00) (READ AND I_rNDERSTOOD) DATE: HCCOEONNNFNFIEIDDPEEINNNTTCIIAAOLLU N-- STSUUYBBDJJIEESCCTTTRITTCOOT AA C OPPURRROOTT.TEECNCOTT.IIVV2EE7-OOCURR-DD1EE0-RR29EE0NN8TT2EERREEDD IN IN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00002299 W_MNo4788579 3M MN04758379 1 PROJECTNO. H ea aT[eoPTr Tr|P eT T eTT E I TTTT TI]TTEe EEECe EEIEFTa1 1 PROJECTNO. woresooAxTnoHa 24 `SMRESTRICTED --DONOTREPRODUCE. 3M RESTRICTED -- DO NOT REPRODUCE al PPAAGGEE | SSUUBBgJEECCTT:: vse: NOTEBOOK NO,~ ~ q ~,.,~ [~. DATE: y2a4 a CE bkhpf E s eR o aetHL mER J i pp ndeai 1TE 82. ] EEL TTa ar TT d EEEEE EEREF ErERT tEL : il"Lobel oroeo 1 ob 0bd ZT HEH Iam dim i rat HT |2g ly |alia F9 E A dpb [PTC PY SP IT {Fhka hod | PT I B RL aoti TP Loelth i JMa fel AREER fHee]aJ]affTe r Arm u TLM aks TT Sah EHEEeEtEE FT1 Ra nS Tet Fel Pree 4SER: Ce HH a] fifo | ob H om la] eT] rT 2 FE Ep } EN 0 rgd ot LH AUAUTTHHOORRS'SFFUULLLL NAMEor NAME or INITIALS INITIALS A Che oxe_ la er FLA TNS ee ETEe Home . WITNESS'S FULL NAME or INITIALS DATE: (READ AND UNDERSTOOD) TE CONFIDENTIAL - SUBJECT TO A PROTECTIVE ORDER ENTERED IN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00003300 worms 3M MN04758380 rH ee eereH suRESTRGTED -- DONOTREPRODUCE cePAGE no.OrTeEs~oOoOkKn.d4. 1~l 7? 223,~ &t, 2255 CT rr TI 1 PROJECTNO. 1 PROJECTNO. SUSBUJBEJECCTT:: ODANTEE:: 24/78 Tjese EEEEEEEEE HH TT per||FACT |cheg| chil EERE | T 0 H GEL AbCE T|rTbenbe C sppai|c|pCnoad) |C | 111] T CT r daJi T nd bd | |TTI I CeFl H odoI f0 f I I [ C IE rEh FidIeT | 1Il TF Zxl11 T kb | hPoyr|b GE +lCnbrn I 2 2 Soh (Sle |TI TT] I g Thal cond 0 TO [NO TT 0T 0 TET | olETanalT{C PT C Le I TET 1dT GV T di T owksLt | Brefbieirepre]on] |4|LU bode]11111] E Tg] E Toi TE n dNoEfuchEidale] he otic| | Cy[| |rr I a rrr [I 1 J TT eee I EERE EEE 3O HT H A H TTH T TH e I] Cer LT TI 3 A 35 eTrT [rd [morsrurosaveanamais_ oe 4Close SCaOla EE Emma Td C EEEEENEO EEEE ow 3/2209 DATE: W|ITWNEISS'STFFUUNLLLLENNAASMMEESoorr 'INITSIALINSITIALS ETE DATE (READ AND UNDERSTOOD) COBNFEIDEENNTICAOLASTUBJSEICTTETSO ASPoROeTECR0T5IVEcOuRDTEoRssEeNTrERED IN CONFIDENTIAL - SUBJECT TO A PROTECTIVE ORDER ENTERED IN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00003311 aw_wosesst 3M MN04758381 _ 1 PROJECT NO. asta oversees we 1 3M RESTRICTED -- DO NOT REnPoRrODeUsCoE okoy 7.3 NOTEBOOK N~O.~ I ~" ~'~DATE:L' amen 1m 22a SUBJECT: PAGE 26 26 Cre Ob ~cti~ ~: HE +H ' HH HH eet HH I ad alyoma] 5 Ret~ren:e: ~)V EEEEN HT H TTT]H I H HH I] -H E Sr L LL HET Harp Mn hTokba3 linf nie I HE H n rata eLsitPeH +H Bree Hr 5 Tr Bh [ETI ges: w |[11] Fest ne L HHH [ZulT13) Qepon || | |||] I] Hl - I [11 5 PLE Hr tT BE]Sp Ep bo |adis] [133|| [Q~s25] | TTT] HHHL I] [] i TT Fert [1] | 30 ot | ps HHH Ha] Hr] I] pFirei rorit] REAa. H er EEE REESE CT 0h [1 AUFTULLHNAMOEorRNTTISALS AUTHOR'S FULL NAME se 4 Clenta owe #)w ---- w(ITW NESIS'STFUN LI~E NAMSE S or INSITIF ALU S LLNAMEorINITDDAI ATTEEA ::LS (READ AND UNDERSTOOD) H- SE SA ru CONFIDENTIAL - SUBJECT TO A PROTECTIVE ORDER ENTERED IN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00003322 sme 3M MN04758382 rere omer ar noresoox7n9o1qs 27 3M RESTRICTED -- DO NOT REPRODUCE NOTEBOOK NO. PAGE 27 1 PROJECT NO. SUBJECT: ET TL TTT ma Th Oh ~ctfie: He HHH eH : see: 5 Ret ~rer. :e: |"i~ #n.[nelly de~ ~a"l | PPP ~ ~ t~ e H CIT [111] DATE: HHH Bl IEPrEr re rE I 10 FP lee] ot bolt cli to | pe 4 HHH m B moe 2 12 Z| | CE 1 HHH 1] HH CTT] HAH HH Hl A= EEE Eh SR se EH EENEEENAnes: TT S | 1 [ol eld mtb ho tog |[Tednala HH HHH Pe Es ] 1 [1 B HEH re 30 I SSSSaRe a lela bh I 1 HH Ie] HH CT | TZ rr EEEEERE boolppduck || 35 ~ HHH [] EEE HHeH e |AUTFUH LLNO AMER orI' NITIS ALS (Xi dion frescos ER -- AWUITTHNOERS'SS,.SFFUULLLLNNAAMMEEoor rININITITIAIALLSS DATE: DATE:, 22/92 (READ AND UNDERSTOOD) pp CONFIDENTIAL - SUBJECT TO A PROTECTIVE ORDER ENTERED IN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00003333 sors 3M MN04758383 E ogee. E amen T rormonctd ee 1 PROJECTNO. Obj :cti~ e: AMRESTRICTED --DONOTREPRODUCE 4372" moe ` 3M RESTRICTED -- DO NOT REPRODUCE ~'~ j~" PAGE NOTEBOOK N~,, '~ ~ 28 SUBJECT: DATE: CETti 5 Ref~=ren:e: ~GT m~-;n,, 8 EEREHE EEEu same HH FHo I[4R 2 1 [E| EMh pbe]rSheet|C _|] E| i] HELE EEEmEER H [rioT t gage ksgAenand+ EEEEEE TToT Fore =g2]irEaeeSalEE Pt ali Tn]ek HEEa TaTs]hHr reLrTeR Er FE a THTH m EE | 8f fe H ed 0 ens he DEeSia > sanHE EF HT Ee E EE {ig Fal] Esk FET oH dd fu m i H7 HTIT FE E EHH E HT ee HHaE eerFTETTT = ITH]mi 35 ee HHH TE AUTHORSFULLNAMEceNTs OF A Clanton AUTHOR'S FULL NAME or INITIALS oes WWIITTNNEESSSS'SFFUULLLLNNAAMNEE ooer INNIITTIAALLSS eee oe DATE: (READ AND UNDERSTOOD) ERR SAT CONFIDENTIAL - SUBJECT TO A PROTECTIVE ORDER ENTERED IN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 2660033..00003344 sono 3M MN04758384 dTL L oaweco T erC fer yC T Se oLT ETE=r sEEmEL EeNEH IEEFTETERE TRErEeFEmatRTE 11 pOECTNO. PROJECTNO. 3M RESTRICTED -- DO NOT REPRODUCE NoTesoo4k7N2o34 NOTEBOOKNO.! ~ ? 2 ~ 4. suBECT: DATE: SUBJECT: DATE: 29PAGE 29 ~8/5//3q9~ Pde EL HHH [aTa8lTT] Hea fe aboil a ep elyiTeadPaT LE bbbT |a iokeoeFicdtlyadb enatlbt Loe H Prob pte FH eT he Ba rll dt {find ml EEE EEE Ado SdaedJoy Tl |] E zlA BL HHe H T EERE E 2 ThGe lefdo]d pBLL]l |Lad adA adpb A T g ||l RAT CL e LL T shR eedae epoereT sbo e E BT STR TT HrE e EEE EEE EE HHH 8 AEE EHEE T E EREEEEEEa8E M Er =e r TT 8 oT] CE J E a TE H HHE H HE HI] r EEE For SPEa ENNEEND EEEEEo ERERRI]EH RREEET J HC eH eee r ee AAUTHUOR'T SFFUUH LLLLNNO AAMMEER oorrII' NNIITTIIS AALLSS __ (fan [mess WITNESS'S FULl. NAME or INITIALS A Lean DDAATTEE:: __ 2105/4 TR eT DATE: -- (READ AND UNDERSTOOD) INn EAT `CCOONNFFIIDDEENNTTIIAALL -- SSUUBBJJEECCTT TTOO AA PPRROOTTEECCTTIIVVEE OORRDDEERR EENNTTEERREEDD IINN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00003355 33MM_MMNN0044775588338855 `I3MMRREESSTTRRIICCTTEEDD --DO -- DONNOOTT RREEPPRROODDUUCCEE ge PAGE | 11 PPRROOJJEECCTTNNOO.. Ee mn Obj cti~ e: | SUSBUJBEJECCTT:: Ny o NOTEBOOy K NO~ ,~ 1'~ '~ ~ ~ 8J300#/% DATE: ~ )~/~3 1I I i HH CEE es NMS \ Ea EShandauAERan wT re [LolTTTH Liki 1d d uighe | elie Godt bro Hr FT ELh T e Be meEee [BulT feteae | [|[TTTTT Ipbole|a" [std I Eb HHH 1 Et bh battnt Lo Eben opi alLine| [Ea [Towel | TFTT EHH g [L EdRH Cod]y be TTer dT EIT | i [QF[9CIEdbln of] los Posh leads[|[| 3 oh onde Js | 1[TGaT do fod, s00ly BT al Pits T Le[s]bflfL] ! dy ar] ieas ] es Jugs? 17 ET Bh [T] . 0 [Rda d] d elbale|Hel high dod H HH Lite ranged for] Oe and 1 E HeeLE : 1] ledod[TTT] Ee BamTEnE TT HE HH HE moses ursavgcenvirass AUTHOR S FULLNAME or INITIALS WITNESS'S FULL'NAME or INITIALS (4iCslo EER Cd ve Shale DATE: iw ; DATE: (READ AND UNDERSTOOD) ERA SE LT Se CONFIDENTIAL - SUBJECT TO A PROTECTIVE ORDER ENTERED IN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00003366 sons 3M MN04758386 1 ocr. 1 PRO~ECTNO. emer oonrmonee i. suger: ote. 3/0v/9p 3M RESTRICTED -- DO NOT REPRN.OOToDEU~tCOEOe~s~qo~ 1!o'7?k22n3~g4~ 31 SUBJECT: DATE: I] CIT II TT ITTI TT CT [Cfowetes|TU [TTCCTTCT] Pe HT EE pm HT x) Hhordoenide|With {5 Mellon |Yehsad Perdhile Adid| {Lie r eRe e B [113)Qhdahoctachic] Condihont| inraroke [Viale t JendPupha Gor[1h Gollingd | | | TTT | ck Godse orbsad | |||| - [1 8TT ERE Fa te HE me! ded Ruma] | | LLTILTTTT] EHH BH BH PN TT Td wu g || TIN rrr rrrrr rr rrrg I NTT EH EN HHHHH 5 TT SSN HTT HET TH I Tr Ne 1] mn. [11] SHH H ISN I Es rrre HR FEE 3 HH HHH HH rr rrr PN C 1] HHH A HH E H H E EN [rman uaenemas or-- vrrv u xo aMger e ms as-- OlaA Clu AUTHOR'S FULL NAME or INITIALS WITNESS'S FULL NAME or INITIALS oe Yorn DATE: DATE: (READ AND UNDERSTOOD) ee CONFIDENTIAL - SUBJECT TO A PROTECTIVE ORDER ENTERED IN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00003377 son 3M MN04758387 3M .EST.~CTEO -- OO NOT .EP.OOUCE I we 1 PROJECTNO. |FHT ReErEh E rEE LE e H a Sica: 5 SUBJECT: NOTEBOOK NO~ ,~ ~ ~ ~ l~" 32 DATE: le 0 CFPgoocomBtLef TrnE Eoe RaR sa iiahA t gen FoRme TE Blimsheto Be Hh RT H eEw E e ETr ~ HE r EE eh ChE AUTHOR'S FULL NAME or INITIALS DATE: WITNESS'S FULL NAME or INITIALS (READ AND UNDERSTOOD) DATE: ERR SAT CONFIDENTIAL - SUBJECT TO A PROTECTIVE ORDER ENTERED IN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00003388 sons 3M MN04758388 nse cover nonie ee 3M RESTRICTED -- DO NOT REPRODUCE PAGE + prom. 1 PROJECTNO. semen SUBJECT: mEREE FL HEE T Hs HTH FE [] " 112884 NNOOTTEEBBOOOOKKNNOO.. ~ ~ ~D~}~ lV ni HH TTT gzfer 3333 ~/],~/S TT 117 o JEEEr RSeaReElyspRARanananaRaR anna" lcd Jc|Eberbvbonluidid desallis]andcbs] ||| | | HH 0 Hel agonyodlSley TT dfeer)d ep LLL FE rte EE rrr rr rrer rr rr rrer errr rd re rrrr rr GBe opte pL i agt J etse er datTT| a TTTLon Todd[RPT]Gilad, 1 eldsI altIndicteddpe] | [7[17] Error EM Es iy ol dip EE lg | Ce rer rer rr rrrrr BA rr rr rrrr rr rrrrrrrr rr rrrT E8r T rr E EE T= oH CT rT rr rr PLTTTT TTT PEA rrr rrrd CT bel N HTH HEL leh H Ho 1] [] eee TO TT rr Errr rrrr rTrrT TT Le THLE HHH I] HATE rT FH HE eeET ee TT TITTT TI TT LL [1 I] |ao FULH LNAMoEorrINITs IALS-- Lin A (fu ore Yplar kUTHOR S FULL NAME or INITIALS DATE: |WWITITNNEESSSS''SS FFUULLLI~NNAAMMEEoorrIINN]ITIAALSS ET (READ AND UNDERSTOOD) DDAATTEE:: TTT CONFIDENTIAL - SUBJECT TO A PROTECTIVE ORDER ENTERED IN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00003399 sma 3M MN04758389 [------ Le 1 mPoROmJeECnTo_ Hes FHF HEHE NO. 3M RESTRICTED -- DO NOT REwPoRrODeUsCoEoknog 4 12% 2PAGE Csmper T NOTET BOOK NO,~ '~ '1 3.b~a~ V3/29 DATE: J rr rT TT ll ea a FT TE Co a ICH kla dediBTdake|dalBom Blg k 284 {aobrcoi y lothur |Sisco. ) rT Mu RTT 10 ih ons ks Rebs o [yes pobrpad.at LT Ricker - {orp ni A er Bl ghd ar XeLEF]REEEE] gly 7 TE Oy : | Co er | E2 | [frao me 1 1 HH ) wee H LL ga 1 fl ew HH TTT &5 I TTIT] ] [1ml bi LTT 05] | 3a lefa Eb| Frac = lena] TET Bl Fre Gy Ean! | :I [Eo TT SH Ea " H I frche_hulpghg R| aorng]o|aolylbue FE H m 535 1 HEE S11J I | a TEE + | 3 LLL TTT TTT morsru aMpoeOresAiQruaas TE (WITNESSSFULLNAMEorINITIALS--________ (READ AND UNDERSTOOD) HHH owe Salis DATE: paDAtTEE:: Be ET Soa 0. un nes `CCOONNFFIIDDEENNTTIIAALL -- SSUUBBJJEECCTT TTOO AA PPRROOTTEECCTTIIVVEE OORRDDEERR EENNTTEERREEDD IINN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00004400 33MM_MMNN0044775588339900 [I ------ oe 3M RESTRICTED -- DO NOT REPRODUCE PAGE moreso somer NOTEBOOK|"17284 a3n5 e |0 ook | eth]d iA ]POLeod wmbbeh gre e 2 I IP 1 I || [H 1] H LE IT IN PPeerrcchhlloorriicc AAcciiddEExtxrtraaccttiioonn MMeetthhoodd T LHH crlO a E[BT1TlT1T]T] 2 MsAstme10emP ofmepceknrioie-- foemseispdmemeniategsmnrtoitoidem1ov0me%s)inmg.te a "lgHe7 !1 IE : 3 Goma Omission ps. ||| ~- 2o E [HEE8iTHHaHle S+ tsi emmastwamsotpeL nse hia kohHLHHiHaHkH ]] (~ 25 wos 8112/98 1. Homogenize 1.0 g of liver in 5.0 mL of methanol for 1 minute. 2. Add 1.0 mL of perchloric acid reagent (while vortexing). Perchloric acid reagent (recipe for 100 mL). 70.0 mL of acetone 200 10.0 20.0 mmmLLLooofff MMCiolinlllciiQ.QPwwaertacteherlroric acid (70%) 3. Centrifuge at 2,000 rpm for 10 minutes to spin down the precipitate. 4. Remove an aliquot of supernate. 5. Adjust pH (optional) 6. Analyze HHH 1 ml oH I o0 H] ate nb ph ad EEEpod EEha NEIERENPErRRE T HE HH HEH 1 morse saveOneb n Cnm n asp_as WITNESSFULLNAME orINITIALS AUTHOR'S FULL NAME | CI WITNESS'S FUL NAME or INITIALS (READ AND UNDERSTOOD) Date: DATE: 8a CONTDENTIL. SUBEJECTTTToO ATPREOTETGTVE ORoDeErRSENTTERED IN CONFIDENTIAL - SUBJECT TO A PROTECTIVE ORDER ENTERED IN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00004411 orzo 3M MN04758391 `SMRESTRICTED -- DONOT REPRODUCE 4733 es { TT 1 PROJECT NO. Obj ~ctb e: her HEH HE ee TT TT SUBJECT: . re .o~'~oo~ .~, ~ ~ ~ ~ 36 DATE: Fo 0 Hl EEE EE if T ra nECiHdEReE Ai eo I]ls Vainal be | HH prea H 10 IT EF 05pla ei ~15 TH [LIT 1 T op f Ee ae sasctiisfunit fr i HE BH He 2H HHH HHH 8 HE H Ce HH T I H g + epBrc LH EEE I iN ELH BERH NE is N Cr EiA smesiepped{Canninelneee= HA/ / 35 // ~_ ~ +7 E HH EE AH HFHTTTT F TT E T HTd [wrrorsFULNAME AUTHOR'S FULLNAME or INITIALS I -- ~ WITNESS'S FU~L NAME or INITIALS fie 4Clos owes alte DATE: (READ AND UNDERSTOOD) ET Sa CONFIDENTIAL - SUBJECT TO A PROTECTIVE ORDER ENTERED IN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00004422 mere: 3M MN04758392 3MRESTRICTED -- DONOTREPRODUCE Pace 3M RESTRICTED -- DO NOT REPNROoDUtCEesook7w2,.~o7,~:,,~s4-'~.~. 37PAGE 37 11, PPRROOJJEECCTTNNOO.. SUSBUJBEJECCTT:: DATE: 8/15/99 NOTEBOOK NO.~ ~ ?" DATE: [11 ot HHH HEHEHE HH~H Pl foOvbej~ectni~eer: |JTLTPP LLL HHH LTTrrrr err Pr TTPTT PCT [TsInetenrbe:|the|ufdale| olubi|L/ od Hells | ulusDBELd Akad leodeeltll dls He ieHe HH HHH HAH |T] hie Rods 4 Lb hiddenLLL LTT PLTTTTPP PT TT] TTT Rl a|| Tec Cond Frcs|e | Fish phe] n | Wh |ckeg]of Ae|_| TelTT TT TT Fobod oclba ddan | dike{adid|i]Helobhullgrogel | HHH ee EHH bile bd EL LITT Chl Bed] eT LrrTTad TTT LT PT LL TTTTT TTT PET TT 1 Geb 5 ob theliba plod Cob LLL LLL IIETT rrTT rirr [11 [TT] tg TTT PrP TT EP TT rT] Ey eE GoNNININNNEREER ea EL HHA HEHEHE HHHHH grrr] LLLP PEEP [1g TVA Td TTTTTTTTTT doddade bcddo| || [TET TTLposl meh] Lebod] Toddler|||[oleclodedds 0[TT] HE Hele EO HHH HHH gos] ||Lnllalor |[ HHH HHH BE Aging Aockes| std EEa he ae TrAE api] Er ID Hol + bdr doce [i Lod fon] 1 Hae Rael pp de dfa ! ITT LT TPPIT TT TT TTTT TT TT] LLLTTTT Tolmhzd TeToth bdid ae TTTTT TTT] ! HHH HH PEER [1 || A HE HE 35 bt 1 eee ee ee LITT JT AAUTHU OR'ST FFUULLLLHNNAAMMOEEorIRNITIS ALS (Tote A (lige, ee EE 1 C pate: 8/18/92 WITNESS'SFULLNAME orINITIALS WITNESS'S FULL NAME or INITIALS READ AND UNDERSTOOD) DATE: DATE: (READ 7hND UNDERSTOOD) HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 `CCOONNFFIIDDEENNTTIIAALL -- SSUUBBJEJCETCTTTOO AA PPRROOTTEECCTTIIVVEE OORRDDEERR EENNTTEERREEDD IINN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00004433 33MM_MMNN0044775588339933 en i `SMRESTRICTED --DONOTREPRODUCE 3M RESTRICTED -- DO NOT REPRODUCE ol PE : 38 NOTEBOOK NO. ~ ~ ~ ~'~:~ la" PAGE 1 PROJECTNO. Obj :cti~ e: I TT SUBJECT: rd SRE 5 Ref ~ren ze: ~J t(-T t ~g~,~, TTT MoH [1 EL HEN H Hl GbpeaarHH HH 10 DATE: EEE[TTY i EEE ERN| IT] ] HH I 22. H EHH Tr HH " [TTT Po IE HH H is NEEER [2 gan hb baa Hh TT I av odkdTl H [Delany obbeleld |alkihg! obit! 4 In! Bonsindge Beer Bre dada An Pr HT 3 oH 8 bre EE [Soar|| Alaa al R bot Gal J SEINE U1 Fading Hn HCRHRHERCCEEPSRestaasn HcHtl HEH HHH SE a HHH FH Hel 1 35 CA ~/ tH HH Hl H e HHe HE morsro aEaTins AUTHOR'S EULLNAME or INTTIALS ---- i WWITTTNNEESSSS'S FFUULLLLNNAAMMEEoorr IINNIITTIIAALLSS andChoe HT RES H [11] +1 owe Sly DADTAETE:: (READ AND UNDERSTOOD) ee CONFIDENTIAL - SUBJECT TO A PROTECTIVE ORDER ENTERED IN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00004444 soon 3M MN04758394 mere srs 1 once. PROJECTNO. - eESeiAE EEEREES HE HH HHTeEeRNE | Tslnrote soncr 1738 3M RESTRICTED -- DO NOT REPRODUCE NOTEBOOK NO. SUBJECT: HH H [LITT] TTEr PEopa ik a bs ooodtp1d hde Bikn| HER TE Me - Andes |Sehead I ; p Ce ee gifEasad fee tens g Foded | Ton | Bish neil to hip + Br rr fh ra ee HH IZ TT LT 18LL-H Gece 1 H B SE E EEE HH Ee CHEE e Te EE Th =m H[TT TT LS A] FIHEEE ImamaeIs HHTITTT] AHH HH A AeH ITT TTT TT ETT womensroesavearsmins Fond Co AUTHOR'S FULL NAME or INITIALS -- WITNESS'S FULL NAME or INITIALS TT TL oie 3 2L/ DATE: TTT (READ AND UNDERSTOOD) I CONFIDENTIAL - SUBJECT TO A PROTECTIVE ORDER ENTERED IN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00004455 susnorisss 3M MN04758395 `33MMRREESSTTRRIICCTTEEDD woresookno, ----DDOONNOOTTRREEPPRROODDUUCCEE. 447%"a P4R0E ! Me 1 1 FAA PPRROOJJEECCTTNNOO.. SUSBUJBEJECCTT:: AHHH ate: 9/3/48 NOTEBOOK NO. ~ ~ ~ ~'~" ~ ~'~ DATE: PAGE40 ]~$ | EEmEeeEeEE ANE r HH TTEE]N [<fee] oH 1 FAH r Hg T HE did H dt]E Cadhle doefbeb8o0daeel]TFpT db C eH TE Pp I dd Tae Jechielfn]||| CPsA hade B, on GRedL loalled atha d DeleBl QuuT l | lE n oT ] I I 0 adr u HHHHHH HHH 18 I i = I ET TP ON TH HHH HHH HAH E Tal T | C C P o 1 Err = A a HTT =] 18] EEEEEEE C 1] AN T La5E]ENEEEENENENENESD ERTETEE I TT]T EEE HHH HH| P EEE EEE rrrrrr C 3O8 P7 /T / E AEEE EEEaaauscuan EEEaaaaEs InENEE VE1 EE CEH EE EEEENE fF 3s5 Z E // = F e H eeeH rET H / pans [T HHI CC [ras fie h Cho oe afnlsp AUTHOR S FULL NAME or INITIALS DATE: ||WWIITTNNEESSS'SS'SFFUULI~LLNNAAMMEEoorrIINNIITTIIAALLSS [rrrme (READ AND UNDERSTOOD) DDAATTEE:-- BEEN COAT SITES Soe R05 cu Tosser `CCOONNFFIIDDEENNTTIIAALL -- SSUUBBJJEECCTT TTOO AA PPRROOTTEECCTTIIVVEE OORRDDEERR EENNTTEERREEDD IINN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00004466 33MM_MMNN0044775588339966 NTETTED CONROE oe noresookno, 117234 41 : 3M RESTRICTED -- DO NOT REPRODUCE NOTEBOOK NO. PAGE afmasdanatans I eke A 11, PPRROOJJEECCTTNNOO.. SUBJECT: 7DATE: 9, 9p ElT ee I] HE I EE EAA 7290 T ET A A. oP Sh Hr NERiEUSERREEN a0 i te pe igperi oepi peI n| IHHH IC EE EE wi Ae TR Eemr HH1H ] HIHH T Er C mlbT | pd Fd E 8 e 1 Etkbebt aTiltil, Tfeide |dlT a HT T Te] k 0 Zo,[1 Je Vid bf 8 Jo rgd Jota oAgAy olbp Lopaite || TE 2E H AAS r AE PrrR FE r EE SH Fo]HHH Te al T pe eeT erTT Fe EIR]ERESEEFNerDMT TT 1 a CE ee I] H TTE FE EEEE TT] Hl [rr aE wmvorsru NaMEcermns AUTHOR'S FULL.NAME or INITIALS m(eFinR gA CehoT rse ageor wesms WITNESS'S FULL NAME or INITIALS DATE: (READ AND UNDERSTOOD) EE Seer `CCOONNFFIIDDEENNTTIIAALL -- SSUUBBJJEECCTT TTOO AA PPRROOTTEECCTTIIVVEE OORRDDEERR EENNTTEERREEDD IINN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00004477 33MM_MMNN0044775588339977 sem sin _ 1 PROJECTNO. 3M RESTRICTED -- DO NOT REPRODUCE [~ woreaoonno 41122" NOTEBOOK NO. ~ ~ ~ t~,~ sumer I iT SUBJECT: DATE: 42PAGE M4e2al CeEE5 Rel.~rer ce: HH +H i a LH HT I] I IA i |H Fr Hee m. ipLt TT TTT EETfebbook |C cob gsodanct.S |eth In spurga e[6 | | | | [1 F F R EET Er E Eh aE area e I Ee Rataaaoriy gal [11] E 1 a{othk esaf TE I L 30 T oily rl EERE a HH AENFH=Lr I Eman iS EELLLTT I TT | SEE eLe eeETH HH35 EEEEEPCd ENEEEEN a. HH HHH HAT HH |AUTFUHLLNOAMERaeI'NITISALS CF Chi Cee AUTHOR'S FULL NAME or INITIALS vars: dloaltr WITNESS'S FUI~L NAME or INITIALS (READ AND UNDERSTOOD) DATE: I CONFIDENTIAL - SUBJECT TO A PROTECTIVE ORDER ENTERED IN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00004488 sumone 3M MN04758398 RESTRICTED --DONOT REPRODUCE Pace PAGE 3M RESTRICTED -- DO NOT REPRODUCE noresookno, 117234 43 1 prOECTNO suger. NOTEBOOK NO. ate: 9a4)3 PROJECT NO. SUBJECT: DATE: _] [TTT TTTTTTTTTTTITITT T L CS a gadis yl ky I Development future needs: ~.~f, lq-D~J, t5 05 (B2O) 1) C140 (9 GGrroouunnddwwataetre,r, dirinnkkiinnggvwatatee,r,rriivveerrwwataeter-- QQuuaannttitcataivtevtteoo ppppt lleevveellss 3 Spt gram wn ody " Contact: FACT Team - KJH Foodprodu: bres, ik. gas. pork 0 Tema lookin or PEOS, MeFOSE, EFOSE Food products: bread, milk, eggs, pork (ppt) - Tentatively looking for PFOS, MeFOSE, EtFOSE Con, BaTlAD&'eSAD ody * Contact: Battelle LAD & SAB 3Oda'~ j~ Je Etrrosee "4 T 35 (D Cnn eam ah Scimens opppb)EIFOSE.OH Contact:SedimentsFAcT(ppt/ppb)TeamEKtFIOHSE-OH- &metboltspossibly & metabolites possibly MeFOSE. MeFOSE, EIFOSE EtFOSE t0oddey - } Ir D(9)9 -To T-opsoe ( SStlhuuiddggsee.,mmmiicircroonbbsedddeegegrgraradadadtaifoionnooffEEtFFOOSSEE.-OOFH((pppbbi/ppppmm)) ++ FCI29 r(_2j~ "~ Contact: FACT Team - KJH CodagtMiinniehse,hs. ~0~Xird'~c,'i7~ tsoe rb king or FOSadmoses + fom cll eh Municipal sludge (ppblppt) looking for PFOS and metabolites - "~a (31a ~b~, ~-t-. Comat FACT Team.KH p AcddiTgousl FsOSi,PoREInS,c-e. 30d Contact: FACT Team - KJH Acid digestion - Total PFOS, PFHS, etc. Comet FACT Team.KH 3 Contact: FACT Team - KJI-I or indy.indy ooff Lrcr i~tdZ~, of "~/~-1" ns a+ ome OD gmmiedice mh een todey . in B 7) Expansion of LC oincludealertdetectors - LCMS 4LC-UlraviolevELvigahptSocarttaertinigMvSe T Expansion of LC to include alternate detectors - LC/MS & LC-Ultraviolet/Evaporative Light Scattering-MS Contact: FACT Team- MEE and SP Team- TLH ,~0 Tp MoMnoonooesseterr frroomm ffooooddaannddffooooddppaacckkaaggiinngg ((FFCC--880077)) ttiedittood##22 sods T - Conant FACT Team LAD 3 -- Contact: FACT Team - LAD X~ monn T L `CCCooannrtptaaeccttt:c:hBeBmatiatsetlrlyte --eWWKKlRR,l,TTLLeHH. ((WWililddlifelIntt'lanaanlaylyzziinngg)) ~~ T E kn erascene T Textile chemistry - all other chemistries not covered in #9 L Comat. BateWER.TLH (W1intlns) L XQ Paper roc chemiFCs.e) MroSE,ie. T Contact: Battelle - WKR, TLH (Wildlife Int'l analyzing) Paper product chemistry (FC-845) MeFOSE, etc. i. L Cone:Basle WR, TL (Wit 1 snl) Contact: Battelle - WKR, TLH (Wildlife Int'l analyzing) = = 15) Vepeion - ooking camtcssionin various pactom,s Vegetation - looking at translocation in various plants - corn, etc. = Conant.FACT Team: KOH Contact: FACT Team - KJH SST Newneew shhamaons tomPROSichemyise - 12) New chemistry - new alternatives to PFOS chemistry I Comet: VakFACTIOR HS) 125) Nowa sic in onto heey n 12 Contact: VoksiFACT?/KJH 12.5) New chemistry - toximty in relation to new chemistry in #12 r Comat, FaBanaWACTY Undeg we Contact: Fran/Battelle/FACT? ~- ~/) d&/~ ~4? r 13) Now Toxmethods -suporiog newmaces in cumefonusncie ai L 13) New Tox methods - supporung new matrices in current/future tox studies Ue 0 Jon Tocminic mens ody engoig Contact: Battelle/Voks/KJH Cos 19) NowFCF (FC Fale)methods nding effete. 14) New FCF (FC Facilities) methods including effluent, etc. rs 00 nrerecna Goda 4 Contact: CentretSPS 0 mn wl 2 tk sos od Tee (19 oviumnmenocso of sbidale och 2.3% Sechr 5 i Companies ous: Batelco), NoctvBieLtabeUrsn, Vok Or. Voss, Reseach ole ic NO, | Companies for outsourcing: Battelle (Ohio), Northwestern Bio Lab (Utah), Voks (Dr. Voyksner, Research Triangle Institute in NC), 1 ie Fon For i Oma Cote uid Blan 5c T Wildlife international, Fran (Fraunhofer Institute in Germany), Centre analytical - 3M Building 236, etc. AUFTULLHNAMOEo RINITSIALS fe 4 oe: lte AUTHOR'S FULL NAME Or INITIALS WITNESSSFURELADANLD UNNDERASTOOMD) EGpsCINTIMS WITNESS'S FULL NAME or INITIALS DATE: (READ AND UNDERSTOOD) `CHCEOONNNNFFEIIDPDEIENNNTTCIIAAOLLUN-- SSTUUYBBDJJIEESCCTTTRITTCOOT AACOPPURRROOTTT,EECNCOTT.IIVV2EE7-OOCRVR-DD1EE0RR-28EE8NN6TT2EERREEDD IN IN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 SM_MNO&758360 3M MN04758399 22660033..00004499 3 PROECTNO. IOTA T FlJRoemmE |do|E]E gR o aE s [MI aA ldi | TE T EIETER I PROJECTNO. 33MMRREESSTTRRIICCTTEEDD ----DDOONNOOTT RREEPPRROODDUUCCEE qk PPAAGGEE ! ~,~ ~ ~ woresookno. 417 44 NOTEBOOKNO. ~ ~ "~ 44 sumec: Lo oat: 9/4/53. SUBJECT: DATE: ~ gn)pepo HHH T EARE ESI Ibol bl Cnob | ||] uNii TEs ne MOmEer a aa r 1 a sade E een ene aa [gE abl rt - fg iSSgHaf sseeese EmsaEs HH I SHH HH an J Bob A HE HEH uHi JA mu | He HHHHH H Je eIe HH uil EEE EEHE H HEEIT A TTE THEEL |AUTaHOuR SFUFUULLTLLNNHAAMMEHEoorOr IINNRITTIAASLLSS (Fn A Clu oars lle EEE i WWITNI ESST 'S FUN LL E NAMS E orS INITS IALSFULLNAMEorDI DAATTEEN :: ITIALS (READ AND UNDERSTOOD) CONTA SURES OASTE onogan `CCOONNFFIIDDEENNTTIIAALL -- SSUUBBJJEECCTT TTOO AA PPRROOTTEECCTTIIVVEE OORRDDEERR EENNTTEERREEDD IINN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00005500 33MM_MMNN0044775588440000 re 3M RESTRICTED -- -- DO NOT REPRODUCE aePAGE NNoOrTeEsBoOoOkKNNnOo.. 11~ 1~ 77 22 3~ 4~ 4455 11 FRc, PROJECT NO. SaSUmBJeErCT.: DDAATTEE:: 9/1/94 mel HHH EH PEE HH EppEEn i Obj,~cti~~: I's[Rethrenk ar hey Lasts solr_xs] mee] kite, ide\(o|Goad Put] Gad) | | HHpLe A tn whe e eb e TT dlI Hat bo kl] clo dTa LLT] bChiT RiTEaPLig Ld IHEERRp ALrir SPs t E [2l ] pPt AbT eled C alll T HHH 1 LE gfol C ad ETEA EEbdET E1E ] E FH Pr We aplc|mdBh| efrdyT| 5f] BLLRte E E rs r Le H L H i|C Ly T H T Bae 8T~ T~5 T SoTbelT:|] HH HHT HI HT T TT] lint fad CE opie i. F HR h pTad t/ 1 HCiEld EEE e H e b peH dHa E EEE E A REYEWhI is bo {Absd Jo0 g]] lpalA aald I vss ou coors aut FULLhNAMoEarr iNis aLs AUTHOR'S FULL NAME or INITIALS WITNESS'S FUI~L NAME or INITIALS (VisAe SE Clones owe 9lieler DATE: --------,----, _ DATE: (READ AND UNDERSTOOD) Ce ET Soom 3 mero CONFIDENTIAL - SUBJECT TO A PROTECTIVE ORDER ENTERED IN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00005511 Sr3M nazseict MN04758401 -- pr TT Vm, nfs i PROJECTNO. 33MM RREESSTTRRIICCTTEEDD ----DDOONNOOTTRREEPPRROODDUUCCEE . PPAAGGEE ! 46 NOTEBOOK N~,~ ~ ~,,'~ ~ SUBJECT: DATE: Obj ~cti~ e: E HE H E CO5 C Ref.~ren :e: i r Chg " [] [2L THsheT l orld driv | Sol 5m mighedl | 53 adel, ra [T1 TT TRRe [al lop ep THAT H [LI shor!Sun faa! eaddala. oomlblel J duds& lodlods TT11 H ret eh ] TTT Ny [Zs] oll of [4kLh] BelferLLL HH SESE EH EEENEEEEEEEEL Ee Z 20 Ee P:B BH hoa ck o apldsddi aH Ll embdid 1 HHH 30 I tH . TTT HHH EE Ee He -H [T] HEH HHH HHH HH EEEAEHE HHH EE Ee wrsorsro avons OnAChoma pire. 3[0]85alnkg AUTHOR'S FULL NAME or INITIALS ADD RTOOD | WWITNI ESST 'S FUN LL NE AMES orIINNS IITTIIAAS LLSS FULLNAMEODDAr ABTE:: (READ AND UNDERSTOOD) ee CONFIDENTIAL - SUBJECT TO A PROTECTIVE ORDER ENTERED IN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00005522 sons: 3M MN04758402 3M RESTRICTED --DONOTREPRODUCE ---- pa 1, PROJECTNO. `SUBJECT: vate: 422/98 H He I L[T H T heFEr HT reE E t cee CC Ed T IT sTe 1g |_| Bm HH ET Bl LeLT I 31 H Ao hS etledd I a HHrH EE 1 pbs] HHH HH 1 YI HHH 1] Se HHH 1 [ITT HH I Ir ] SL HE [11] Ld LHL LIT [1] ] |Chalbu|g=teos fo shadGTpedi| |Solihelled [ola A 4 | [ HELL ea tina edu eet [TTT A AAUTHUOR T SFFUUH LLLLNNO AAMMEER oorrII' NNIITTIIS AALLSS ae A Clune A WITNESS'S FULL NAME or INITIALS DpaAtTeE:: 4 DAT E: [1] (READ AND UNDERSTOOD) ee CONFIDENTIAL - SUBJECT TO A PROTECTIVE ORDER ENTERED IN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00005533 sores 3M MN04758403 33MMRREESSTTRRIICCTTEEDD ----DDOONNOOTT worssookro, RREEPPRROODDUUCCEE 71" 48 PPAAGGEE t\ lade] | 1 pROECTNO 1 PROJECTNO. HT suger: SUBJECT: i NOTEBOOK NO. I] AY o0 e a)n/ey EE NCS ESSEFEAr Hn P F[eE lude pactJade, TL TEET T e HEh Y 1] Refap pr LTeT t gE k] [T reon lal) 0 LEE EE EET : oRt Aa E l db I age pal hep dT id r edraedTT Batol det Salo | CE gh tel alo ST LT TT hi Ti, nn BeOPeY TH I Fn TEs EE | 13 Rp od pie| orioeof | | J trlbrt]latedsi a || | | ST I [1T 11] 2 HHH AA 7 EER Ba e0ae SARE SRE Snananes HEE EH bad EHH ml Fab [Cl Repg E| H HENNE I EEHE TH 1 I 1 wrnorsrou xagoeiris-- OseAChora AUTHOR S FULL NAME or INITIALS pure: 3a |WWIITTNNEESSSS'SSFFUULLLLNI~AIAMMEEoorrIINNIITTIIAALLSS TETRIS (READ AND UNDERSTOOD) DDAATTEE:: Be ET Soa 0. un nes `CCOONNFFIIDDEENNTTIIAALL -- SSUUBBJJEECCTT TTOO AA PPRROOTTEECCTTIIVVEE OORRDDEERR EENNTTEERREEDD IINN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00005544 33MM_MMNN0044775588440044 SMRESTRICTED -- DONOTREPRODUCE Pace PAGE NoTEBOOKHNO. 3M RESTRICTED -- DO NOT REPRODUCE NOTEBOOK NO. 4499 1, PROJECT SUSBUJBEJECCTT:: 78k 9 fe 1 PROJECT NO. [T TTT TTT HHH IT . [ovate i Ob: ,~cti, ~: |TTTTTTTTT] I I [LITT] [1Ts Tetpeke: | FacET |EEHhE] H r H [r Pirrrrr rr[rITTTre 5 Ref,'.ren~:e: ~[~ ~ ~ ,~ Re [=R fan] hdd (pbs) | | I] H Cr 11 HH [T1011] [TTT] [1-Tafbid oki gl 4 cd rrr rd I fol |] fete Tl PA be help de LL [] AZAR ETH [TT Tok{rat tg fel H [TTT TT Lh [TT rrT rrrr LZI z HH Fide eg Prosmb|lalfoller|iod |Hcu|ndpeZboeddaelwodaltd||bia| | TT[TT Leth er] 1 + I sh RETEST i [= HE eeLH | HEREEEEE [eg TTT] df odfron [Bd le fog=[=fAodt Hoidel gl,|t || JE] H 1] CTrd EE 2 bfonchli]ce obed_if_LL_Seats| ps PebsA, Prodad., Ms io [Tr Cr g | [TTTTTI1 H [TTT TTT rd BTTloged held d |E plat pall DL LL 87 ok hf EAN TA STOTTTT cl Tillug dot Ble [TTT 1 TOT feb dF lima |6-Lt (cot do IT{flb e[eb lu Crrrrrr [] [CT Tecle[neds 1TTTTTT [IIT] Lo I A HHH AEA I] ooh beeps Gade |Tatled Whol doFlulachent H KARNSENERSEEENE Cr l 80 bol LLL LHL I pl by oa 1d JS TEI HHH [TT iol HHH He pod TT Fee EEEEEN H CITI Hi EE [sek FETell red [o ipo] | pspoh] dking] hell]orpaleads |||| Leb eT TTT [1 [TTT L iorsFLLNavi oe vias adCline oars Alb WAWUITTNHIOESRS'ST'SFFUULNLLI~NNAEAMMEESoor rINISNITITIAISALLSSFURLEADLANDNUNDAERSTMOODE) OpraIm NTIALS (READ AND UNDERSTOOD) HENNEPIN COUNTY DISTRICT COURT. NO. 27-C\-10.28862 `CCOONNFFIIDDEENNTTIIAALL -- SSUUBBJJEECCTT TTOO AA PPRROOTTEECCTTIIVVEE OORRDDEERR EENNTTEERREEDD IINN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00005555 33MM_MMNNO0044775588440055 -- PROJECTNO. TEE Ter MbObj.~ctke: i | SM RESTRICTED -- DONOTREPRODUCE gab mee noresookncytT 3M RESTRICTED -- DO NOT REPRODUCE Iv NOTEBOOK NO~ ~ ~' ~''~ anser I SUBJECT: DATE: 50PAGE 50 TTT TT HIER o r T ES EHHH 5 Ref.~ren:e: HBEERr S ENEESmLEuRHnE]E ann RR EEEEER EEEeEeNENEEH EEREENe NNEREIEEEe EEEARLETLUE EEENH RREEE EmRmRmEEEn ee Te g2SoaEmER e H Spr e e HT Hl LIRR BE HT "Hseh Lr a bpaaHT ifcateRunsaggrmmnnninananaaet 2Err rrH RLretTTLlpiHT Tl 2 Ee mnma EC EmEETmn TFT]AHH EmTEH FuIEssEE:ERE-H RRoEtNNNJ NZdS eRET EE2NL NE8SEST ESEAEEST EEEEH EnEEa auT FULLHNAMoE orRNTTiSALS AUTHOR'S FULL NAME or INITIALS ((~:C,9t. e4,4 7(D)in~ oDaAtTE:loiolf~t+~s/sr W WITNI ESST 'S FUN LL E NAMS E orS INITS IALSFULLNAMEOrDI DAATTEEN :: ITIALS -- (READ AND UNDERSTOOD) Seren sero Loree ross `CCOONNFFIIDDEENNTTIIAALL -- SSUUBBJJEECCTT TTOO AA PPRROOTTEECCTTIIVVEE OORRDDEERR EENNTTEERREEDD IINN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00005566 33MM_MMNN0044775588440066 Tat] 11 PPRROOEJCECTTNNOO.. unssTacrep-- bonorremonuce ce woreookngf 7234 51 3M RESTRICTED -- DO NOT REPRODUCE HHH TTT HH 1] SuSUBBEJCECTT:: .OT~SooK.I. 1 T 2 g ~+ DDAATTEE:: PAGE 51 1/7/30 {TL To FE L ty H IT ITTHE HT a edt+h bbb Alene dente ee 2 EE 00 10 H THS ST re r eT Ee Te | SEEERRA RRRREARASARRALRA a NEl E T ESe I- FT ~-- 20 SHARBAAcVa ESREHSPEACCEEE HhFT TR7 2 HHH AEEEH THHH C Hee HH EEEEEE THeB3O EEEEHEREEEPYR HC EHTT (AJ RE I F AA . H TCTpTH easT1 HHTT ST EE TI eTLEEe EE e ATTT swriorsFuLLNEAL (FaACave AUTHOR'S FULL NAME or INITIALS en WITNESS'S FULL NAME or INITIALS pore lolzfr DATE: DATE: (READ AND UNDERSTOOD) ET CONFIDENTIAL - SUBJECT TO A PROTECTIVE ORDER ENTERED IN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00005577 wma 3M MN04758407 o CHjw r T e T smn woreaook TphT,T1 ous: 1 PROJECTNO. 33MMRREESSTTRRIICCTTEEDD ----DDOONNOOTTRREEPPRROODDUUCCEE ask ~O [~ NOTEBOOK I~,~ ~ SUBJECT: DATE: oforag52PPAAGGEE 52 t@~ ldo a |iid Lr] PTttTe S nib e dl Ebeld CRITm T1T]] Pre Le se LE Ms TH CHE E ea oy SNpE]ni 10 HEE Te o s Tt aWm l e EESEmmEE HHH UNE. ET Hee 8 gal [ osL[I ele TdT id oid I gold TTT E Eae E Fer e TEEa ala Coeg TIrT e EE TT HgE| AS7d 0 tr rE 0 | eIr 3 H0E25 TE HHH t HH Hees EEe E = rr HHul 130 FE HEHHH Ese eH FHreeS rr ECeT r CEERCREre AEH erHeH 35 LT HL HE H TT PE E a EEE CET I [mruLo LNamr eaenrs iaLs-- Ole fb Qi AUTHOR'S FULL NAME or INITIALS TT vDuATeE:: lblisfas |WWIITTNNEESSSS''SSFFUULLLLNNAAMMEEoorrIINNIITTIIAALLSS-- TEE (READ AND UNDERSTOOD) DADTATEE:: CONTA SURES OASTE onogan `CCOONNFFIIDDEENNTTIIAALL -- SSUUBBJJEECCTT TTOO AA PPRROOTTEECCTTIIVVEE OORRDDEERR EENNTTEERREEDD IINN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00005588 33MM_MMNN0044775588440088 TM3M RESTRICTED -- DO NOT neo REPRODUCE .OTESOO~.O4 ~177 2235 ~ 83PAGE 53 T oweE TTTT 1 PROJECTNO. oT EF EEET WEEEN EE ERDAETE:H parH EER ia tor|oieT1T1T1 TTT Hl al AlesApinses ETE T a Te rere ephui Te ee rr re J fE o L HE - taHe EL EE gmsH 1E |SENSEr EENEH SESNT ESH EEES NST PJENNEEHEHEHREHEE 5IJESEEE EEEEEEENENo ESE a HEE EEEEN HEHE 1 FH Eee ENE EEMSASENN NEH EENNNEH EEENESEENEE BERRARNAREeRERARRRREEE HH HEHE FH HH CO35 A TEEELLT LL EEFE PTT mors Earns AUTHOR'S FULL NAME or INITIALS TF WITNESS'S FUI~L NAMREaor ITNITLIASLS U eA nepws pI2% DATE: er DDAATTEE:: (READ AND UNDERSTOOD) TTT CONFIDENTIAL - SUBJECT TO A PROTECTIVE ORDER ENTERED IN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00005599 mae 3M MN04758409 Hee + FroCTO PROJECTNO. 33MM RREESSTTRRIICCTTEEDD ----DDOONNOOTTRREEPPRROODDUUCCEE I PPAAGGEE - noregooxno, 4 25" 5454 FA sumeerH : MN o+n Hifsfas In SUBJECT: .OTEBOOK.O.~ ,~ '1 "LDSATE: IHTH ue| 06 PeabH o 1HTTT EEE NJ NE] R . HE oe ] L : T HHH HRLTTConchoCon|||Hele JT HHH ] FeHlHmm PS TT dhe LT|] ahd i; HHH 1 Golo i Ter doi TN B]E| TN op lb Lebo bec] osAtNn |EGoEtdhEE EE TE 5 : 1 + qd TET Tod wch | pofer| 0 Dugaek 4 making | by Lh bod iTo Mg LT I TT TT Cget LT] IBree I rr Fe re 2 TSee8 l Lali bal[oFod [Z8 H FET me oe fo ae] a ~ 25 feck] |] 1IEEE EEE J i TM IT SHF E O aiSssass THER 3O Per HEHEHE Cfhataedtl L iP nes lo |elke CI 35 C EENEA NEEE e EEe E EeEEe e EEEe EEE THORSFULLNAME Tis nA Clie oredr AUTHOR'S FULL NAME or INITIALS DATE: | TE WWITNI ESST 'S FIN ~LL E NAMS E orS INITS IALSFULLNAMEorDI ADATTEN E:: ITIALS (READ AND UNDERSTOOD) Be ET Soa 0. un nes `CCOONNFFIIDDEENNTTIIAALL -- SSUUBBJJEECCTT TTOO AA PPRROOTTEECCTTIIVVEE OORRDDEERR EENNTTEERREEDD IINN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00006600 33MIM_MMNN0044775588441100 some 1romero sumer: ou [ose 3M RESTRICTED -- DO NOT REPRODUCE PAGE n.oo'rrEeBsooookKn.oo.. '11 ~177 223~4h 5555 SUBJECT: T Eee SSRE SSASEEHE T E CTETT I H HH 1 Teepe mLeeETeH EE Lol [BD Dlbiad [Togo Diol ~ 5,0 LH H 1 i HES M heCiL e gre LE I e | ~~ L T TTe ! Fhes HHH [Za] Ed afect bimnd[kddsildlialcd bec ote] H | oTeE [eo I(I a Ta, 1o1d (2d Sn.HEHLi HH g Bana Sol ors JoTHE bd TH - IT 8 TTT alal Be |T 4deledug dhe Logon] TT Ee -- lw] --H Rei dil [114d i ae Li IPE | a LH THEE rks] 2 LH Shee HH HHH Hee I eo HEE EE LTPP PT BEEEEN RE |AAUUTTHHOORR''SSFFUULLLLNNAAMMEEoorr IINNIITTIIAALLSS Tin A Lis, DATE: ou GP WWIITTNNEESSSS'SFFUULLLLNNAAMEE oorlIINNITTIIAALLSS ray DATE: (READ AND UNDERSTOOD) I CONFIDENTIAL - SUBJECT TO A PROTECTIVE ORDER ENTERED IN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00006611 sumer 3M MN04758411 TR EE HAA HH + ocr smn ws falar 1 PROJECTNO. R C ETCTfE]eItTed |Sami H E EoegI E o|dl ELoA tE CBToEC.Te [6] e e IETTETEd Ob +~cti,'e: voresooknay 3 T% 56 33MMRREESSTTRRIICCTTEEDD ----DDOONNOOTTRREEPPRROODDUUCCEE ~at~ l[,~. PPAAGGEE. : NOTEBOOK NO~ '/~ '~ g" 0 56 SUBJECT: DATE: a Pbse T hhcE 1 paT d TT] IH 1] T I]BE10 RETAEtrG ppEdReaEl E EEnR e RAU T a L. fE ag ] [aPyhd TebT fd fT lnk[| METHI ~2Z1l5 oTaLL L&T 1 CET EE 1= g 116 Lost ob falLhT i lib L T rm slf TZEaTl[L 119]h esde fualna Tig I FEE 11 Ibeo 0 af ald Lil 0 daOdEe8i A fS53 ] 8 H CH T CPH T rE | gal CT EEEEEE ~8 25 Fre ee HH CT I Bs =H CEeEl ECEEEEE a= A TETTIN Be EEEEENE CaEN lPATSET E T HEH CT T TTF FE EE HEE rrr EEREASssaESBSANEREESEEREANEEE IN rC ereT eee wriorsruLLxavea iris AUTHOR'S FULL NAME or INITIALS Clin8 Qowe pate: ola ER WITNESSSFULLNAMEoDIATN E: ITIALS WITNESS'S FUI:L NAME or INITIALS DATE: (READ AND UNDERSTOOD) EE Seer `CCOONNFFIIDDEENNTTIIAALL -- SSUUBBJJEECCTT TTOO AA PPRROOTTEECCTTIIVVEE OORRDDEERR EENNTTEERREEDD IINN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00006622 I3MM_MMNN0044775588441122 -- suger: ini 1 PROJECTNO. pingnan RREEEREEES ] HH Obj .~cti~e: eee Ee H E r E 5 Ref ren:e: `33MM RREESSTTRRIICCTTEEDD ----DDOONNOOTTRREEPPRROODDUUCCEE. NOTEBOOK NO. SUBJECT: i PAGE 57 RRR, ah FE mai Sp T E HEh ERa Ea n Een eEe REE Flim mn ey eal 4bled, HT] | PTT B B So E o E t E e es HH HE SenssEie= Hl rT H Lal HT - HH T SS H EAE T E T 35 BammmmmEd Ee =AS-- AE-- Ao-- AUTHOR'S FULL NAME or INITIALS HEE DATE: WITNESS'S FULL NAME or INITIALS (READ AND UNDERSTOOD) DATE: ERR SAT CONFIDENTIAL - SUBJECT TO A PROTECTIVE ORDER ENTERED IN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00006633 sora: 3M MN04758413 FETT 1 PROJECT NO. `33MM RREESSTTRRIICCTTEEDD ----DDOONNOOTTRREEPPRROODDUUCCEE PPAAGGEE | 1 NorERooKNo. aandh l58y SUBJECT: ,o'rE~oo,~.o. ,~,~ '1 ~~ ~ 58 DATE: I I /q2 TSlr eOabt~ectei'~y e: docELLaFlSloEysT aauT EAseeT aisss=et H: H i-= ETEREa E BE ne ELA Bn fiai 3 | pie ldn oTT a hhTTT EE ER EN im P IV om N e EERE H He EEEEREr R BeeHE 30 He enee HH 35 A] AEE PHr HH AUTHOR'S FULLNAME or INITIALS P A O Hoti DATE: HH : WINTNEESSSS'S FUULLL A~AMEE oar IINN ITTAIALLSS roy DDAATTEE: (READ AND UNDERSTOOD) TE `CCOONNFFIIDDEENNTTIIAALL -- SSUUBBJJEECCTT TTOO AA PPRROOTTEECCTTIIVVEE OORRDDEERR EENNTTEERREEDD IINN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00006644 I3MM_MMNN0044775588441144 nesmcres conor ssonuce mae 3M RESTRICTED -- DO NOT REPRODUCE PAGE eH 11 PPRROOEJECCTTYNOO.. l Objl . SUSUBJBEJECCTT:: 117334 las NOTEBOOK NO, ~ ~ 7. 59, ~y Sa is bf Te Ts pm yoER = HEE REE Pri eae TH TTTTT lgiledunte.Sak] jr dT HEH ER ZT FE y A bo doa T pct JEIGL T ITT]T E 8 eE e EEEE ET od i utd | ET 1 TE K|NEhig.S]mth pEitLt ebb Ehof od| O] E E 8 TH h Hl La Hl feConn I ad il lol 1] B Sent rLe H ni EL I] bat LI eter ti THE TLET HH Er efitpcE{e GaTbi EyE RH ce He be T HmoH H ns unHnR s AUTHOR'S F~LNAMEorINITI~S A Hre ee TH T H Cr oeAlm om ile ~ 4 ~,~ DATE: WI~NESS'S ~L NAME or INITI~ a DATE: (RE~ ~D UNDERSTOOD) ee CONFIDENTIAL - SUBJECT TO A PROTECTIVE ORDER ENTERED IN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00006655 sora 3M MN04758415 no 1 PROJECT NO. ---- 3M RESTRICTED -- DO NOT REPRODUCE NOTEBOOK NO. samen reo. SUBJECT: LePAGE (33 80 DATE: Ha =H H BEH saE zamas T r ma T s HHH. [1sTrebor:|Singing beWd]Sc Erihortole] E04 add || || | ||| PEE HH TEE The + fee ee TM H 1 fash bebo pellball Bogda [TTT TT] i [TolTTTT Pla Bok butidlede] | | I LTT TT1] P EEE L H eof U ae mp] d sbi i bp HHH HHH HE] [BH] Badal nbn bl dla Lt HH Fe a )Bro|csobbaeunat.in] || NIN Er rrrrr rrrrrrrr TT Ig | 1 che [te] EE ans Err rrrrrr rr rrr [OTT TaalddEloulegl Wodabla oleTed eke] 11 LH Shellac) hen Fl seeks I Spade " 4 eh hadebbie] chin eghcsbbell TI ded[LCT ET HHH HHH HH HHH -H Hee ee CT ryPr rr rr TIT hel CTT Ee + FC EE Td HHH TTT HH 35 - HEE HHH Here - Oo,~,~c~.. eee eH i TTTTTTTodkelbal3 dod TeallToll ad ViedepdbTTTT1 [TT |av FULLmNAMo E cer iNrrs iars Oe 4 Cline rT AUTHOR'S FULL NAME or INITIALS WITNESS'S FUI~L NAME or INITIALS | ITNESS FULLNAMEor ((RREEAADDAANNDD UUNNDDEERRSSTTOOOODD)) DATE: DATE: SE SA ru CONFIDENTIAL - SUBJECT TO A PROTECTIVE ORDER ENTERED IN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00006666 amon 3M MN04758416 aM RESTRICTED --DONOT REPRODUCE Pace 3M RESTRICTED -- DO NOT REPRODUCE PAGE 1 PROECTNO. SUBECT: NNOOTTEEBBOOOOKKNNOO.. T~ E~ fn~ ~e~dbLy6611 ofa PROJECTNO. SUBJECT: Heeb HH HE TIT TTT TT [ome Obji :ctix e:TTT 0 HHH LTT rrr HHH [1s[nebreter|FACT [Mella| | | | | | [TT [17 [| HH bet edo sdspebgelebe LLLLAE [] 1 debi Be al TE i hi C [L TolcC haT d T T heET rbT bkoT st T fad, T T[PdF TWseleeda He lnk lL [iol 1 Toles ToolbileodeTeodeol| 1 Togsol[TTTTTTT [lod Jel| AH HEH Ese . [ITT i TTT 1 heli?Er duh Vclophee|| Hunde[SHEE] | [11 pd dd I 5: = CY I [[ EHR EAE EELE & Hepatol odor pool boca p Lidl tid LLL ETT LI] HEH H i, E TolDTSolbudblhd beclonfTcol fers[TTT11|| [LTT [EaTol adh] allied |Trakel Risto|phoska |pos [plod |oalilds| | 1 || EE LAhnmEEEE [i x=hula | gpl] DLL DELL LLL fe [IT CT ' T A TY [2 TT TReloade[Fh TerociatealMesh||| | bug |Mb;dll cle.[det]ails 2 he Fedde LLL DHL iii LD LL [ls| hd Heb ore [eH HHH , EHLLL 18TT 1 eT k bore | =o ||| HHH Bhd] dag CT TE ili [LTT edd Tad TTT Eadoot | | TobDliodtlade 8 6:00[4] Hobe Heel Bad| LEE ade Badal LL [Jw T] Dhl Jou2] 4 a NNMAMNMMMNMNMMY TTT Terr rr rr I] eH TT Qa bled bl delTUCITT TTT HeLLLLLL LLL SHE PEER EEE HHH [las]|| AalBa] bod) fecdas| ph h spl LLL CITT Beseba]oli? doled dk|TTTT SPT] 1 CCTT TPTTT TT abe | [LTT 1] J2 YR 9 TY 0 OE 9 AT 27 1 THORSFULLNAMEoriNTIALS Cfo it Clio pas lllalit WITNESSSFULLNAVE INTIS AUTHOR'S FULL NAME or INITIALS WITNESS'S FULL NAME or INITIALS ADKD CRDERSTOOD) pew DATE: DATE: (READ AND UNDERSTOOD) HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-26862 `CCOONNFFIIDDEENNTTIIAALL -- SSUUBBJEJCETCTTTOO AA PPRROOTTEECCTTIIVVEE OORRDDEERR EENNTTEERREEDD IINN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 33MM_MMNN0044775588441177 22660033..00006677 1 1 TJ PROJECTNO. PROJECT NO. EESMREESTRCTED -- DONGTREPRODUCE\ EENne __ woresooxnoy 4 7% 3M RESTRICTED -- DO NOT REPRODUCE |~, SuSmUEBJCEcCTT:: DATE: NOTEBOOK NOI~ ~ '~ ~ "~ DATE: 62PAGE 62 3s be eee m Obj.~cti~e: ~ F"E Tble ET e iTT TFH 1--+1 1IiECmH E T 5 Ref ren:e: ~,~ ~ ~ ~o LE eFe AT The E E dd L | TT wl] PTT dadEP I/ ' 1 aCl]ICrIt T ;IT I an EEE FEET EET E Bal| ulibal ne CE 2EEB |Tstr [1m1nApe i 1 Tl1TtTsPpT kI iI El Atonof 4curve 2 imcach mat. (Live, See)followingthe procedurechangesandwing enwmises. Before starting the validations test curves from 1 ppb - 1000 ppb will need to be prepared and analyzed to check the efficiency. 5 A total of 4 curves 2 in each matrix (Liver, Sera) following the procedure changes and using the new mixes. VVaalliiddaattiioonnss RRababbibti,t, RRaatt,, BBoovviinnee,,MMoonnkkeeyy Liver re -- 1. PFOS, PFOSA, PFOSAA, PFOSEA, M556, EtFOSE-OH 1pt A i Bd l. sen Sera 2. POAA, M570, MeFOSE-OH, PFHS 1. PROS,PROSA,PROSAAT, PRoOSTA,M556 BIFOSE OF 1. PFOS, PFOSA, PFOSAA, PFO~EA, M556, EtFOSE-OH 2. POAA, M570, MeFOSE-OH, PFHS H a -I 30 ~: AA.. MixMix 1 and 2 wwillill ccoonnttaaiinntthhee ccoonmpounds specified;nneewwmmixixeess may need t0obbee pprreeppaarreedd.. hon i te pe pats coer B. M570, PFHS(C6F13SO3), and monkey sera have not been received yet, please start with Mix 1 for the liver A ot validations after the results from the test curves are reviewed. ST Extraction procedure changes i in 1. MTBE will be used as the extraction solvent dispensed using the new dispensers. 2Ale cenvfoiannd befor removing sientut ample to an ACETONEIDRY IC bth 2. After centrifuging and before removing solvent put samples into an ACETONE/DRY ICE bath to ny freeze aqueous then pour off all 5 mL of MTBE. Need to test how long to keep in the bath. ny 3. Evaporate to dryness and reconstitute with 1.0 mL of MeOH. BAELAEE --H nN 4 a35 I TT 1 "TThheessee eexxttrraacctionaanndaannaallyyssiiss emeothosdswwililllbbeeggiivveennpneeww FFAACCTTnnummbnebresrs.. PPllesasse taallkk wwiitthhKKharoi orrGGrraantttoosaissgignnnnewwunmumbbeerrs.. ||_| Ll ] i L AUTHORSFULLNAMEceINTIAL OF dChine patte ol _ pl_ od DATE: ) AUTHOR'S FULL NAME or INITIALS (~-~ ,~ Cba~_- Cr WWITINETSS'NS FUELLS'NASMESorFINIUTIALLSLNAMEorINITIALDASTE: DATE. (READ AND UNDERSTOOD) rTM A `COCNOFINDEFNITIDALE--NSSUTUBBIJJEEACCLTT TTOO AA PPRROOTTEECCTTIIVVEE OORRDDEERR EENNTTEERREEDD IINN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00006688 33MIM_MMNN0044775588441188 ener soeronce - 3M RESTRICTED -- DO NOT REPRODUCE PAGE ee 11 pRojECTNO. PROJECTNO. Ok ~cti,'e: HH HEsumer: SUBJECT: HE NONTOTEEBBOOOOKKNNOO.. BEDh o6633ffs '~ ~ ~A~E~ ~ I~ [TTTTTT TA rr art EH TT i CC TTTe TT PT Pro HIHe HHH HHHH EC TIARAES BAA BARSSA RENA [asdasl LLL TT cabeldcdt Cail]ducal bodbagd| ||| | | |||| I] PCEEMEEEEREREsEREEEEEEEEEEE [EM FRE [1] II le TTTTTTPTT TT PIPTTPPT PPT EHEE HE oH EL 50 ded p alk iL fo[plehod Dedelopadedl| kd| 0 0 AA 1 1 E _g 25 HH // POE HH Er A HAH HH ET HH HH 1 11 HT [TTT A eH I C A E HE 5ee ssee HHH HEHE 1 [wmHoRSFULLNAMES AUTHOR'S FULLNAME or INITIALS [WTITENESSSS'SPFOULLLL NNAaMEror INTITIIASLS Of &Cres (READ AND UNDERSTOOD) pe DATE: DADTAETE:: salou ee CONFIDENTIAL - SUBJECT TO A PROTECTIVE ORDER ENTERED IN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00006699 sonst 3M MN04758419 nestor oonormermoovoe 437a%e l PROJECTNO. TT TT Te [1 Obj ;cti~ e: L Ia HHeifg]sssTaEnEtce aseassenH ] e C EEE 5 Ref,,,re[ :e: 3M RESTRICTED -- DO NOT REPRODUCE NNOOTTEEBBOOOOKKNNOO.. ~ '~ ~1 ~ ~'~ :PAGE 6644 SUBJECT: Pl DATE: - SENo10TirEeRreEtHAt pwuln]sitHnr HEdantmas [eee J:Ego L| EWI MTTrh TI HH I Ha eo fat di E8T] Hie a Led TLCTE TmmIaE H0N Fo Hine + EEdHhCmE Eer e EaPe TTrH TTHHHH Ha=I ~25 : BH HH EE HE IN E HH E eH AH 30 Foe] HH I HH THLE HCEET Te] T rF T r HNH E F H H 35 THe eh rH HS TH HE AvUrTiHoOrRs'Sr FULL NAMEu orINITIALSp Olde Mensa es pare _iofosles |rr -- e FER e WITNESS'S FUI~L NAME or INITIALS DATE: (READ AND UNDERSTOOD) CONTA SURES OASTE onogan `CCOONNFFIIDDEENNTTIIAALL -- SSUUBBJJEECCTT TTOO AA PPRROOTTEECCTTIIVVEE OORRDDEERR EENNTTEERREEDD IINN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00007700 33MM_MMNN0044775588442200 BE EEEEMEEEMEMsESEEEEEREEEEEEEE 1macro. 1 PROJECTNO. Ob ecti' 'e: J -------- nae noresooknot 17234 3M RESTRICTED -- DO NOT REPRODUCE NOTEBOOK NO~ ~ 7 ~, ~ ~" sumer: na SUBJECT: DATE: 65PAGE 65 ErHH HH Fld HHH SEH 5 ReJererce: EEEe EA Ee ARP e ETart C LH EE : Gp F PEL E E HE E 1 EH aLE dad 1 FT B | REEde uldduasurdueanamsEnH] ET . EAN A EHH e Me TT TTTLe TT ETEHte aet HT [E ETrofl buble f0 ol 4 beet aTTT] IF2~ L ob E Lod dd SHEEE kTE Eat,d Toda Body [TleT [1] AH T E edH "fd LTaelH de HHH R HPE T FTEAe Se P of[ OPa chad SOT T H bo[bfa-p|a|s1e1]] IC TTR ] HHEEEEF EEEERESC E : EEEEEF/ SEEEEEEEEEEEREES FEEEE THEe HHRert I A } i AAUUTTHHOORRS'SFFUULLLLNNAAVMEEeorvINIrTIAaLS Ce Urnas WITNESS'S FULL NAME or INITIALS bate 1/ox/o (READ AND UNDERSTOOD) Ce ET Soom 3 mero CONFIDENTIAL - SUBJECT TO A PROTECTIVE ORDER ENTERED IN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00007711 Sr3M norseszt MN04758421 i a soner owe: 120] i PROJECTNO. TI Hee C I E HIE ] HE EI EEI LFT E TT 5 Ref.~ren;e: WMRESTRCTED --DONOTREPRODUCE 1, PACE 3M RESTRICTED -- DO NOT REPnRoOrDeUsCoEoxno. 11723" 66 NOTEBOOKNO. SU~ECT: DATE: S E EPRNART mARREEE 1 TaIlT se e TT EEEEEEEN| lO Fe p; lore llcTel ts HH EEee Z ~ 15 g | Tehfa Lh --~ 20 FC EEEEEiEa=aEE HH E BoT baen Bod,eE onH ] op 5 duu ? % :41, Cr Baba dn 025 T I H 1] a I] T a b E foulh diEbmalEa EE BREE or LI Fr 300 | | ol L "| abe bl edo bbl Rb LH HH HN T c A Eman Bede saE Rnn ger CaFzaEsaaiane 35 ee moHrHs rHu xamE rinaHisE ed CoE mo pare lifer AUTHOR'S FULL NAME or INITIALS DATE: I WITNW ESSI 'S FT ULLN NAME E oS r INIS TIALS S FULLNAMEorDDAI ATTEEN :: ITIALS Sa(READ AND UNDERSTOOD) INn EAT `CCOONNFFIIDDEENNTTIIAALL -- SSUUBBJJEECCTT TTOO AA PPRROOTTEECCTTIIVVEE OORRDDEERR EENNTTEERREEDD IINN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00007722 33MIM_MMNN0044775588442222 SMRESTRICTED --DONOTREPRODUCE PPaAcGeE. 1 PROJECTNO. supEC: NoTesookno.f 7234 DATE: o1/066,/779 [T1111 I A IC. A AA II rrrrr rrr rr rrrr rrrrr idee LL LEE HEHEHE NN [rrr rrrrrrr I ul [of]Bd mad] + Th practhetlbt| lhlgbedsel LTTTTTTT JI 79 AA II A I Lp dilly LEE FlA ml gud oodLf pd hid] bbe [libido clad 0 1 MI I Crrrrrrrrrr rrr rrrrrrrrr rr rd HH EHH EE Heapiso LH Hg Heb beepJo dad pba] LLL ol ||| EHH HHH TTT ed TT ke TTT g [111] I 0TPPT DSEREYPOPE EE EE NYY -- 2 LE LbLlu uM,| MRL ag EL Lal HEH tsete Wad Ladd LTTTTT PEO] = I] Pr rrerrr rtrrrren rr rrrrrerr rrrrrrrrrr I 2b babehod Lob hl LLL EHH HH HEH rrr HE HAH |1] I A II I Qs [TTT ELTTT PP PP FE EE EHH - HH EE HR I HHHHHHHHH |[1 DIT Cerre rr CTTTTTEA TTTTd EE NEEERE EY HERE HEHEEHH He [TT] EEE 1 HEHE [rrr rr rrr rrrrrr rrrrrrr eH EHH EEE HE ar re rrrrr rrPLE Td [111 [ EHH EEE EEE IIT] [1 [TT rrr rrrrrr at wh FuLLNo aveorms viriats ie 4 (lianas are_eufeufis AUTHOR'S FULL NAME or INITIALS WITNESS'S FULLNAME or INITIALS WITNESS'S FULL NAME or INITIALS "READ ANDUNDERSTOOD) ome DATE: (READ AND UNDERSTOOD) `HCCEOONNNNFFEIIDPDIEENNNTTCIIAAOLLU-N- STSUUYBBDJJIEESCCTTTRTITCOOT AACOPPURRROOTTT,EECNCOTT.IIVV2EE7-OOCRVR-DD1EE0RR-2E8E8NN6TT2EERREEDD IINN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 33MM_MMNN0044775588442233 22660033..00007733 `3MRESTRICTED --DONOT REPRODUCE 1, PAGE - 3M RESTRICTED -- DO NOT REPnRoOrDeUsCoEokno. 44725" 68 | NOTEBOOK NO. TTTECTTTT muTmT 11 PPRROOJJEECCTTNNOO.. SUSBUJBEJECCTT:: vate: ALele,4m]n |FmElE eSe1aE HHAE ie e He TIT 7 CirprFeela Eee b or re To SleT]0n i TTT T Sp |ke mheT slope e ob 2d iIT Eg FEdE a e IAR e eoHHTT THT Eee o ymA dI FE Rb Bg=E T[|] TI Ee Fr3 ady BeDigehhe epre rle" TT aron ed el ee TT THe]Fela ald oid eli a Hd Lh rTaReTeeBeee ad REe oee e pEmEREE FH ptb| morse ode fodisd TH] Pe Fe AeG sPe re e pere pe en 1 Ls i 1 | Ch I CorerTTLT EERE 1 [ AUTHOa R'SFFUULLm LLNNAAMMEo EoorrIINNr TITiIAALLSS (Sf owe oun f -- IWWIITTNNEESSSS'SSFFUUI~LLLNNAAMMEEooerIINNIITTIIAALLSS (READ AND UNDERSTOOD) DDAATTEE:: Seren sero Loree ross `CCOONNFFIIDDEENNTTIIAALL -- SSUUBBJJEECCTT TTOO AA PPRROOTTEECCTTIIVVEE OORRDDEERR EENNTTEERREEDD IINN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00007744 33MM_MMNNO044775588442244 sr.noresookno. 3M RESTRICTED -- DO NOT REPRODUCE NOTEBOOK NO. PAGE 117234 6699 1 I0 Obj~ ~ctb .~: 0 _ DATE: tH ha EH a ESSEHASEEey HHH HHH EHH H as pl Lb LL LH ] HE La st '10 HH i Tr] EAdcaeEt F F H SEeeRiaL nfRuidpRsT inE sEnTalnEte huTneinte EEEE SNM NSM aE ] el TT rar Mal LLL TTT] Heed Et BH 00 ap BTR Hi t= i LULL ELH Aelopiint] mE Ce ETE Hea ei 30 H ptE t S HS e 35 HE msrsro agains-- OiAUn [ITT AUTHOR'S FULL NAME or INITIALS TTTTI TTITIT] oe _eluln DATE: mess rues: WITNESS'S FUI~L NAME or INITIALS DATE: mm------ (READ AND UNDERSTOOD) I CONFIDENTIAL - SUBJECT TO A PROTECTIVE ORDER ENTERED IN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00007755 sumer: 3M MN04758425 SMRESTRICTED --DONOTREPRODUCE p= PAGE LwoECTNO 3M RESTRICTED sumeer: -- DO NOT REPRn.OOoTDrEUBeCOsEOoKoNxOn.,o~ 4qt '7~2'~3Da~%re~: 02770O0/59 1 rT PROJECT NO. SUBJECT: DATE: I] EEEEEENEEEEEESEERY - - HE ERE ENE 1] EEEEE 1 ep i _ HH pb iy dat dod rode|| TFTTTT ah le El sul Lio Fah] acta [ello4 ells 1 1 [11 cole lheobltza=dmocfhedoicu.|sabit- okkd 9 H 1 Hel HE se H IR CH apse ape ITToa hed[LTT UE TP CE TTiad WhT a afb eH CEs] nu ope rts] H [ ZIE | 1 rrrr rr i galls | TT Tr rT rr g[Ns TT l Sere od A Fer esi HHH CIE fost| HHH TL I 0 Ewa |]piBelelo]c 6d acd] HENNEEEEEY (che to dil]wher.+] hae| comple[whe [cle||11] | | LL TUTTonlala Tall sb[LITTTTT TTT Errrrrrrrrrrer ma iSineanmaasRsmpRE | a Ce ee 1 Eee HH rr rrTTT EEE A e EH E LTT I Cr rr rrr rr er rr rerr CThad TTTTTT L Ho 5 | On Logs [mid odd palicbion ohh s| |] hnakoatbeded tTLTT TTT TTT OT rrTrrrrrrT rrrerrrrg HEH HHH HH EEE TTT TITTTTT] AUTFULHLNAOMERo I'NITISALS Chi A Clr ore: ol 20/59 AUTHOR S FULL NAME or INITIALS DATE: WWITNIESSN'S FOELL NSAMESor INSITIAFLS ULRELADANNDUNADERSMTOOED) orpDeIATwE:NTIALS i (READ AND UNDERSTOOD) H`CCEOONNNNFFEIIDPDEIENNNTTCIIAOALLUN-- STSUUYBBDJJIEESCCTTTRITTCOOT AAOUPPRRROO,TTEECNCOTT.IIVV2EE7-OOCVRR-DD1EE0.RR26EE8NN5TT2EERREEDD IN IN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00007766 M_MNOATSS42 3M MN04758426 11, PPRROOJEECCTTNNOO.. WRESTRICTED --DONOTREPRODUCE pace 3M RESTRICTED -- DO NOT REnPoROrDeUsCoEokno. 197234 71PAGE 71 SUBJECT: NOTEBOOK Ly SUBJECT: DATE: JI ICOIb2%ti~ e: HHH [TTTTTITTI] | CT rrr [rrr 5 Ref-~renze: ~fO.~ FY~,~a li~r:~ _~__,;r]~ ~t~I~ HER Eee H {Abds Toh | RlTrl, TThlShelafh Eh [1 HHH ee [Led Shea) idriok, Plaats, hick [td]| [TT Mobi Bl | TT Ler] Se lib tole |] TTT]mal] EE HHH 1 rrrrr rrr rrrrrrrrr [] Foo I H | rE H 2 LTTTTT] Le rrrerrrrr 8 | Telaader(057)| [LikeSuck,Ua | LEH H EI ER eT u~l 2o Batfll | HHH " HHH ole Ll [] 5H Te[ad|eidlLeick Cl piurd IphahobeClda] Lid, Sh] 13] Lige [idsal LL] [] gr fa ih 3 | Luprg Al 1g] 1 8 ABS zl(thd)| [Hees H izI H1 TT windsll ced] [11] [11 CTT HH tobe] HLH es+ | hoe| x3o | [pn| 1 EE HeHH [I] [11] [TTI rrr FR i LH oH REEE ih C TEe 5 [Cebus Koleribg |CHeslesot)| | | | | | ||ag | [| | [|[| |] TTT Datefra Gla TTT FI 03 nfl vad HHH J LE - Pros, Pros, [Prosah_n sag, (erfost. osbye) bie|n| ~ wmnorsFuLLNAMEceivimaLsCnA Skuemees -- nure:__lolot)o AUTHOR'S.FULL NAME or INITIALS BATE: !O !Ol!O3 WITNESSSFULLNAMEOrINTIALS WITNESS'S FULL NAME or INITIALS RAENDNDA RRSTD OOD) ose DATE: (READ AND UNDERSTOOD) HENNEPIN COUNTY DISTRICT COURT. NO. 27-CU-10-29082 (CCOONNFFIIDDEENNTTIIAALL -- SSUUBBJJEECCTT TTOO AA PPRROOTTEECCTTIIVVEE OORRDDEERR EENNTTEERREEDD IINN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00007777 33MM_MMNN0044775588442277 11 PPRROOJJEECCTTNNOO.. Er HE a 1 J )j :ti~ 5 ff en ,: i ~. RESi TR,CTa EO - Do NOT REP~ODUC~ SSUUBBJJEECCTT:: NOTEBOOK a1 er DATE: 22/41 I HEA 1 HH 1 HHT E p E Hf :EEME e r R E m E a e Ti [BT tok 1 C ( hei ldie| oka(lhl ase fal [1 25 La EH EE 3O H HHe eE ireee She H ee eE e \UTHOR'SFULLNAMEorINITIALS DATE: [ESS WITNESS'S LN FULL NAME NWS or INITIALS (READ AND UNDERSTOOD) DATE: ERR SAT CONFIDENTIAL - SUBJECT TO A PROTECTIVE ORDER ENTERED IN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00007788 sons 3M MN04758428 PT Le] mmm SMRESTRICTED --DONOTREPRODUCE pace PAGE veocso 3M RESTRICTED sumer -- DO NOT ~ REPNRNoOOtDTeEUsCBCoOEoOkKoNNoO..w1i1447e722334Jo77a33n 1 PROJECTNO. SUBJECT: JEL] H LLL I HT HHH CJ r Jos [r Te T1 rr EEE rr I MEH [] [1] [Tolustmds | TTTTTTTTPT I IPE T 1] 5 HHH kbEe To: Dale Bacon and Bill Reagen From: K. I-Iansen, L. Clemen, M. Ellefson HH ] [I [] |Tio]|| ] 10 [| HT TTT CI Fans 2 15 EH[EE11]0 {Ee 20 January 22, 1998 hemiaie BPeroopDeosseedd UitiiliaztaitioonnooffOOuuttssiiddeeRResesoouurrcceessttooSSuuppppoorrttTTooxx SSttuuddiieess:; rose Battelle: Argus 012 (placenta, fetus, liver) tsar Argus 013 (placenta, liver) `Argus01d Given Argus 014 (liver) Argus 015 (liver) ter aAlsdOtinipiroovgreens)s, ser vation complet paces lidion *liver validation in progress, sere validation complete, placenta/fetus validation =re ABS, Inc: Argus 015 (feces, urine) Argus 013 (urine) Argns 014 (milk curd) ps0 rik cary Argus 009 (mira etmt) Lonmin vse *will require 4 rat validations pad planned ER [1] 1 Zi og Gl bl [1] [11 HH HCHHH E[gR:1E1 5 25 [8H [[TTTT] [Fer Fratmhoffer: eit i Ton4e eio) ns *will require 4 validations FACEPACE: Arms em) Argus 014 (sere) Others, if appropriate | swt va ation.tt,cos voi *will require 1 validation (rot, cross into rabbit) 3O PE| [ **suggest negotiating a "per study" fee instead of complete use of the facility until competence is proven FACT Eipthafdevenleopeeitsehitsn amr se FACT: TOX030-6 Mo. PFOS in Monkey 4 * new, non-GLP projects InIn-v-ivtirtroossttuuddyy Telomer feeding study Method development mnniotic fluid and mammary tissue | ERO its napionfsng es snes fo a AAltlthhoouugghhmmoossttooffttheeststuuddiieessccuurrreently aawlaiitinngaaanlalsyisissaarre PPFFOOSS,,wweewwililll reqquueessttvvaalliiddaattiioonn foorraallll 35 EtFOSE analytes in anticipation of using these resources for future studies. 1 I [7 L HH [11]] ma + : TiHsAH1 HH H I HH sumorsrugoes (fim A.Shutnsen AUTHOR'S FULL NAME or INITIALS d;~. ~. ,~__1~ WINESSFULREVD MTNDERRSTaO00TNTpSes WITNESS'S FUI~L NAME or INITIALS (READ AND UNDERSTOOD) pDiArTeE: tolotJoa DATE: CCHOEONNNFNFEIIDPDEIENNNTTCIIAOALUL-N- TSSUYUBBDJJIEESCCTTTRITTCOTOAACOPPURRROOTTT.EECNCOTT.IIVV2EE7-OOCVRR-DDAEE0.RR2 6EE8NN6TT2EERREEDD IN IN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00007799 W_MNOATSOAZS 3M MN04758429 sm 3M RESTRICTED -- DO NOT REPRODUCE vo NOTEBOOK NO. 417207 00 74 EE PROJECTNO. SUBJECT: Ere Repncte:|||| HEREEN HAH A 7IIA HHH Ho AHH, TH He TE LPTrrred LTA TTT [] HAHAH HES AHHH eA VPATTP TTT Be HHH HAH SelTrrr | HHH rAr EH HH AREER Ee STA u THE le 11 INO A TT CESEARR{ENENrARERARAAE BHANRARCE Lrr rr r rrr rr rrr E rr TTL HH / ee ee] ] HE 30 / CEE / HHH ! / EE HHH HHH eee ! = [TTT 177] HE 35 /I __ HENNEERNE |] eee T ITT TT / PP TP PLPTT [11] [1] re AUTHOR'S EULL'NAME or INITIALS DATE: |WWIITTNNEESSSS''SSFFUOLLLLNNAAMMEEoorrIINNIITTIIAALLSS EH (READ AND UNDERSTOOD) DDAATTEE:: ee CONFIDENTIAL - SUBJECT TO A PROTECTIVE ORDER ENTERED IN HENNEPIN COUNTY DISTRICT COURT, NO. 27-CV-10-28862 22660033..00008800 soraso 3M MN04758430