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226-7764,
Air Sampling Fluorochemical Report
[
DuPont Washington Works -- Air Sampling Program Round 7
Exygen Research Report No. L0001444
TeEsctyignegnLRaebsoeraartchory
3058 Research Drive
I
State College, PA 16801
|
[7 meoeeeeeerr----rom---- semesters
i
Requester
|1
Michael D Aucoin
URS Corporation
Barley Mill Plaza
-
Building 27 Room 1260
[
Lancaster Pike and Rt 141
`Wilmington, DE 19805
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ALL DATA CONTAINED IN THIS REPORT WAS GENERATED BY EXYGEN RESEARCH
|
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Summary
r Seven solid media samples were received by Centre Analytical Laboratories, Inc. (dba Exygen Research) (Exygen) from DuPont Corporation. The media represent samples of air collected on
[~ OVS tubes. Please see Table 1 for a completed listing of samples received and field air volumes
i collected. Sample WWK-A-AMS3-E7 had sampler problems during collection. No results are
reported for this sample.
`The samples were analyzed for Perfluorooctanoic Acid (C8 Acid) using liquid chromatography
~~ / mass spectrometry (LCMS). The method employed is entitled "Method of Analysis for the
|_ EDextyegremninRaetsieoanrcohf, PFeerbfrluuaorryoo1c7t,an2o0i0c3)A.cid (PFOA) in OVS Airtubes by LCMS" (James Miller
The OVS tubes were separated into three fractions for specific fluorochemical analysis. r Fraction A consisted of the filter, backing material and plastic ring. Fraction B contained the
first bed of XAD resin and the PUF backing. Fraction C contained the second bed of XAD
resin and PUF backing. Fractions A and B were extracted with 1 mL of methanol. Fraction C |" was not analyzed but saved for possible future analysis. Perfluorodecanoic Acid (C10 Acid)
was added as a surrogate spike to each fraction prior to extraction.
|" Instrument operating conditions can be found at the beginning of each analytical run. Raw instrument data is given in Appendix A. Chain-of-custody information can be found in
| Appendix B.
5
ALLDATA CONTAIINNTEHIDS REPORT WAS GENERATED BY EXYGEN RESEARCH
Pagel?
600269
| Results Summary
|
Air Volume
Sampled (L)
r
AJA--AS,8
WKANISIE7
T1aas6 138
r
ASE (Tota) ----
.
WAKsAAUeSSA78
11445500
|
WWKAAMS2.E7C
1490
AAS Tot)
7
|
wKhAaASEE7T8A
[
WAASUBUSSEA ET7o0a)
--------
|-
-- AAS 78 AEG
11553%0 15%
AUST To) --
1
|
wKARASASESA8
AAU E70
|
WA ISO (Tow)
CC
--
8 Acid
(mg/m3)
<c0.000000807 T0N0A03
<00.000000307 T0N0A03 <Z0o000000088 NA 500072 <<0c.0000000077 NA 0.000 <Zo0.0000000088 NA 00001
NA -- Not Analyzed.B fraction was below the quantitation limit, therefore the backup fraction does not require analysis.
| 1. "<"is defined as not detected at or above the reported level.
I 2. Sample results have not been corrected for blank results or control spike recoveries.
| Frasier Fs De 3. Please note the following descriptions of the OVS sample tube fractions:
|-
A5 F[rrtsEmxtroaectads oan
c [2nd sot boads extract (not anaiyzec)
ALL DATA CONTAINEDIN THIS REPORT WAS GENERATED BY EXYGEN RESEARCH
|
Page Sof?
600270
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600271
Surrogates
[ASurcruomgoagtaetsepsipkiekreec(oCv1e0riAecsiaer)ewgaisveandidnedth1e0faollllOowViSngbtaeblse.toTghievreeaarfienanlocsoentccernittrearitaiofnorosfu5r0ro0gpatpebsipniktehe extract. [rowers `Advisory ranges are 75-125%.
I" I mmm oo So -
opb)
ppb)
W WKA AAMRK SUFSBTLEKTEA? B 550000
533503
1708
|
WWKK AARRSS2EE7T A
550000
360734
17251
[7] . mWWKKaAAnARUUmSSH2eEE77s8A
5520000
o531812
157062
WWWIKAAAAMUSSSSEE7T4B
550000
5a97
1819
I WHARUSSE7A
500
WHKAAUSSET
500
5a6763
17153
[
CCoonntirrll SSppkkoo A8
550000
35473
6991
* Surrogate recovery outside of advisory range.
ALL DATA CONTAINED IN THIS REPORT WAS GENERATED BY EXYGEN RESEARCH
|
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600272
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Gn0273
~ Example Calculation
For sample WWK-A-AMS2-E7 A C8 Acid,
= [426 ng/mlof C8 Acidx (imi) x (1 ug/ 1000 ng) x (1 mg/ 1000 ug)] / (1490 Lyx (1 m3 /
.
1000 L)]
= 00003mg /m3
-- Signatures l
I
>X
Paul Connally, LOMS Team Loader
2)2s/o Tato
oo 17
SL
|
nM. Flaherty,Vice President
Date
OterLan Members CotingoDaa
James Miller
ALLDATA CONTAINED IN THIS REPORT WAS GENERATED BY EXYGEN RESEARCH
|
Page Tol?
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600274
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ANALYTICAL DATA REVIEW SHEET
I
LC/MS
I
Tames 10. Md\o,
ple. ne
|
Analyst
Sighature/Date
3i
_
John in Foley
adm lS shoe
|
Reviewed by
ignature/Date
|
-
|
|
0070
GO0R7?
Seen: G\HRCHEII\GERU2E1N30G5E.A ro Sense abies
Da mmm om boa Ca PUNE mmmmmm, mmmmoon loean
Lo Bun mma ome oe |
14 vial 15 10001444-4
FC8-10 1 Sample
| lo Vials I00luity Reo 1 Sample
~ pumy mews, me ose
- S3BmuM)Ii mmBmmammm Say mim
|
Calibration Part:
Umm: [- duimE
mum Bmiimmm
mmmwmoaooloonaon mm ob
ma 1 rmee)po
ie we gmeenee emness
Hi mim mf ; " | cuss 12/18/03 4:36:36 Bi smitior ROT tes
oamnm ae
G01
Page 1of 1
GNO278
|
LC/MS SYSTEM AND OPERATING CONDITIONS
-
I
Client: Dupont.
EXYGEN STUDY: _ L0001444
i
|
Instrument: Hewlett-Packard 1100 LC/MSD (LC/MS 5)
-
API-ES Interface - Negative SIM mode
|
Nitrogen: 10 L/min at 300C
Fragmentor: Variable; Vcap: 3500V
|
Computer:
Hewlett-Packard Kayak workstation
I Software:
Microsoft Windows NT 4.0
Agilent ChemStation Version A.08.03
i
HPLC Equipment: HP G1322A Solvent Degasser
!yi
HP G1311A Quaternary Pump
HP G1313A Autosampler
|
HHPP GG11934166AA MCoSlDumn Thermostat
|
HPLC Column: Thermo Hypersil-Keystone Betasil C18, 30 x 2.0 mm x 3um
Column Temp.: 35C
|=
Mobile Phase (A): 2mM Ammonium acetate in OmniSolv Water
b
Mobile Phase (8): HPLC grade Methanol
-
Time 0.0
%A 70
%380
|
6.0
10
90
I"
1010..00
T1o0p
ST90OP
i
TPootsatlTriumnet=im4em=in1.4 min.
|
Flow Rate:
0.3 mL/min
I-
Injected Volume: 5 uL
||
I~
Peters
Il
Ore
00279
v
-
Ions monitored: [
|
Analyte
C8 Acid (PFOA) 10 Surrogate
369 lon (m/z) 49
Extraction Date: December 18, 2003
Analyst:
|
r
James R. Millerysl toy
E30x3y8geRnesReesaeracrhclDrive, State College, PA 16801 Phone: (814) 272-1039, FAX: (814) 231-1580
-
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[ mection Date : 12/18 5:3/1:042P3M
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[__ Esameple Niame:STD 750 ppb
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Data file :C:\HICHEN\1\DNTA\Chemstor\11666074\AS06E8\FCO000.08D
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o
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-
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Fri, 15. Dec. 2003
u0z3
02:12:28 pm
rage 1 of 1
Gn0295
_ seme samesioooiat2es
|" sample Info:
1
`
[7 Injection pate : 12/18/03 7:17:45 pw
Seq Line:
1u
+ ses e[nTeRoof poTscienR s cnshoO niss acT tos TSSF
|
pa
ro
--0
-
Mw
[1] =
A[| hi. [|o=n [| =
I
Ir
.2500
T
compro mor.
|
Toee s e ||
|
es 3 snes -
-
i
Iose
Tai Endof Report tir
res 10 ue 2005 openosm 0029 eres
0002296
| bSaatmapleFiIlnfo:SCH \HRCCHhesEsorN\EL\6649L9\R\GHGBHO\FRCLOTROLA2.D 1
|| mFInejregcitiienonleveate :a12n/18e/03 7:32:54 BM hnSeq eeLine
"31:2
a unas} Eo bSieswero szians 0
Lo anatysis of porivors casbomyiic acids.
[ w em
re
[| =
[= ro
-
Mow
|
"MSD 468,EIC=468.7:469.7(CHEMSTORN| a 1666499A464B40FCO000TZD) APNegT,S-IM,EFraSg:V,ar |
| |] sen
[7] | on
I
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compound hens
7
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o
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|
|
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of report <ee
Pri, 5.19. vec. . 202003 02:15:06 "pm 00350 "Pa1gofe1
cnon9?
[ _ Sample Nase:10001444-2
3
Data file .C:\APCHEN\I\DATA\Chemstor\11665575\AS7008\C000013.0
"InoSjdxeecrotopimeoernnatcoDrat|e :| 1dImoio2iolt/esr187/:408:303 Pu Ditation i
SnTeqneLeivnee. :
sw1i3{
|"
~
sAeoqd.iysmiesehvoeathod
Last Changed
++|:
Cr1:e3\o/-1H150P0.C00HEN\1\NE10T251H85O063D5.S7
pm
I coms avtaass o sneer sassy seta.
|
ST ICTCTHEN TOR STRSTRFCIOTS0 APES, SWF Ve
=
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sional
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aloe To
wn 363, Eic-368 7369.7
8.193 159294 MSD 469, EXC-468.7:469.7
CT
Tendof Reporc tee
| 2C00414
Fri, 19. Dec. 2003 02:16:01 pm
rage 1 of 1
600298
__ Sample Name:L000144d4-4
|" sample Info:
1
! Data file :C:\HPCHEM\1\DATA\Chemstor\11666652\A469248\FC000014.D
"IAnTcnjqsetceOtupimeoernnattDoarte ;|: PJ1CmOi2DlAl/Le4r188/:003:313 BM
"svIeinqja.lLiNvnooe..
1
i
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|= piiation HE
vel.
sul
|
-
Aacnaa.lysmiesthMoedthod Last Changed
|rcC1o:2-\/H1t9P0/C.0A3mEM\L\METHODS\10211:8506:35.71
pm
| coms antanin of pesto cars seta.
[]- wom W3E 50EC-T 368TE CREMSTORT T6320 [TIOT RPNogE,SW.SFag:Var
| reo
|] ao
12000
[7] wom
ao
| - 8000.
[.| 200=000o 7 i 3 81C510S2ur-ai |
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[| ==
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ro |
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| 830acSiuarrogac 433209..133
87.138520 213557589671
|
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Dwsldl 436699,, BEixcCe-d3e6s8..77i:d36693..77
N [
| ecooars
+++ EndofReport i+
Fri, 19. Dec. 2003 02:16:59 pm 0032 Page 1 of 1
00299
sample Kane :10001444-5
[sample Info:
1
! Data file :C:\HPCHEM\1\DATA\Chemstor\11666728\A471424\FC000015.D
| eelIongjmeecpteeimoanrreDrate :fE12/e1A8/03 8:18:29 PM
[ E rfeqo, voee rbo + CsGeenec-- t0 ---- ee | corns amar of pesttuoee cosmic acta.
|- RT
FSom erqReLaie nle
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[| 1e50o00
||
wow
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2500.
|
[ convent sme ws xx. ween
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re
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hepa TT rot, 19. Dee, 20 02.2838 L0337age 1 of 1
600300
[_ SSatmpele i Name:L00014dd-7
1
Data file :C:\HECHEM\I\DATA\Chemstor\11666788\M73600\FC0000.16D
= || STIenojsaetGcrotueimmoeanntteDrate : C1m2iO/l1Al8e/Lr03 8:33:39 ox
VSeqaLirne
mj. No.
|-- spiolnutivonos iraso
ml vel.
[ ALnaasltysCihsanMgeetdhod :: C1:2/\1H9P/C0H3EM\1\METHODS0\11:25168:05173 pm
Le/mS analysis of perfluoro carboxylic acids.
-
FSO 85, EC-38873697 CHEGSNSSSSAATIRTIIFCOO0r00RTSe0) APES.
10000
| 14000
|] om 000
63
sul1 io, SW,Fig Vr
| 000
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1+565789AATIRISFCORONEETTT ) AAPNoT oE,SWE ,SFrag," Var: 8.198- G10 Surat
25000
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[1] wo
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87135685
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216s6c5e044d | MMSSDDl1 436639,, EEIICC-e436688..77::436639..77
i1, ecooata
TTR End of Report +e
B
Fri, 19. Dec. 2003 02:21:12 pm 0034 Page 1 of 1
650003300:1
SSoammapilee NTaatmee!:10003444-8
:
Data file :C:\HPCHEN\1\D1A1T66A85\6CAAh7e59m04s\FtC0o00r01\7 0
| Injection Date : 12/18/03 8:48:49 PM
| Adcrkiompeernattor |: dmoiololaetrs
vSieaqlLiNNone.e
:
i
117s:
J thee i
oven: sw
| nRBeadqsi,tyawCtehstahMoneagtheodd}| rCSc:as)\-iH1507R.0C8wHEN\1\ET15H210O81D035S.7\ pm
| Less analysis of perfluoro carboxylic acids.
-7 ow ST,EOS TT RESTOR GSS ATS GI73R88OcaRncPS.
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-
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|
=
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|
|
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|
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sigma
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| 10 Surrogat 382.30
81183 172062 MSDL 469, EIC-468.7:469.7
|| scoosa
Epp Fri, 19. bec. 2003 02:22:11 pm
vage 1 of 1
0302
sampleName:0001484-1
I Sample Info:
Data file. +C:\HPChCamsHtorE11N666\971IMTE\ORODNRERIOOTELSI,D
1
[mLpeirtooend. Ts 1 iun ve ae
ts ree oe FH: REA. sul
[[7 siPer,rEseermRmonated |+ sm esso E a 21000.
LCrHS analysts of pertiuers casbosylic acids.
| TR BRE E TaAnTa EE To WF
Mw
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|
7=
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2000
|
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|
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=
7
1
wr. sen
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rn
:
| conse
Prt, 15. Dec. 2003 02:23:06 pm
rage 1 of 1
660303
psaample Heme:u000L444-14
:
Data file {C\HICHEN\I\ONTA\Chonstor\L66E976\ABOL2BNECDO00L9.D
+ PThniigeecitoinoznebeate LfATNeyD STE | Be HH
TFmaeEe. HE
m? sul
I"
IE
Bsexi. oecrowsate
p +| BseaTvsoE n TSHIS
om
[7 Lens maton of peceiore caspase sete
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TR 38835 CENTOSESRFCOTOTE PE No S. WF i
! wo |
=
|
|-
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160
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|
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|
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| 10 Surrogat 462.39
8.209 206471 MSDY 469, BIC-469.7:469.7
| nao Repent 1H | cecccccsssssssssssssssssssssssssssessmsssssscssssssssassassssssssssssassss
| etonse
Fri, 19. bec. 2003 02:24:30 pn
Page 1 0f 1
600304
=e
:
! pata file :C:\HPCHEM\1\DATA\Chemstor\11667053\A482368\FC000020.D
[" Injection pate : 12/18/03 9:33:1B9M
| Acq operator : jmiller
Seq Li:ne 20
vial No. :
4
A he | Semis gino.
[7 worms oT atso pT esters commTas Rese.EE STE
[
Tanna
r
a
[
I
[r| oSmrd embmerontsesea ri
r
|
| 10000
|
=r- h,000:
I
I
z
I
cont tno wot) am arn
sonnt
1 Ep ccccscmcssscssssssssssssssscssssssssssssssssasssnassassanannnnnnann
|{ ecooara
Fri, 19. Dec. 2003
02:25:02 pm
vlog Page 1 of 1
5 G00305
~ fsaamlplee Name:sotvent blank
:
' Data file :C:\HPCHEM\1\DATA\Chemstor\11667132\A484608\FC000021.D
B IdnjoecmtimoneDate he : 12/18/03 9:49:32 PM
CSeq oLine :
21?
[E se eg wos rn R r| eO ason L roo A w2100es n
I ses castrate of paxciuo caspesyisc sods.
I
TT EET
ores
LI || =
[| =wo |= [| =
w
[ow
EE wo
2
|
I.----
min
| | 190.
|
|
[] = Mp
I
70.
{
I hk
compos sme worms nr, vem
sioner
TT
|
I
|[=
+++ End ofReport +++
Fri 19. bec. 2003 02:25:36 pm u039Page 1 of 1
600306
rosasmple tame:100014te-16
.
fBI oeisespue iz| ley fmBiEEe: pata file :C:\HPCHEM\1\DATA\Chemstor\11667167\A487104\FC000022.D Ld721
I . nERogi,olwlesSBteepeess s|: SenEsnircvmnonnogesss.
[| orns smatve of pesttueee casbomtic avid.
r
TT ES Tr
-
-
Ml -
| ow
I--
[1]J =
|
| ow
[lw
- r2 n wa a mo6 Tra a--n --8 ---- m
|
Ir] seo
So
[7] oo
|
|
r soo1
|
|
~
;
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;
3
[ comma woe worms xx. nee
J
[GIo ehognar o38% EE I E a
Se
i -- Soke 19. ton. Tn sriznenums ulsu sage 1ot 1
000307
=Samplk e Hame:10001484-17
\
Sate file oC: \HPCHEN\LDN11T66ATICSIAhASaSInSAs\FEtONoOOrTS\.D
I[ rlroidsemepeteaTMmearre |fTjoaitm eee Teme TweeT22
sh i
vl sul
{acTBaieyvaotrrmoeeatho!d |+ rESeanVrrioAsmL METHODS 1I 21003.
[7 ems anatyass of pestiuoro caspemse acs.
r
I a>:,
r=
Mw
[ow
r= |[F o| w A T RSTO AYESSATFE EEN Fi politi
[|
|
I T0000
|
5000
|
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1
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1
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pr
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|| seonase
Te Pet, 19. Doc. 2000 02:20:p50m 0041 rage 1of 1
650305
[Sao mple S Name:L0001444-19
1
Data file :C:\HPCHEN\1\DATA\Chemstor\11667330\A491712\FC0000.24D
= hTIncnsgjteeOcoptmieeornnattoDrate |:: P1mCiOl20l4eL/r4 1810/:304:357 PM
vSieaqlLiNon.e : Inj. No.
- pilucion ir
mi vel. :
| Acnqa.lysmiesthMoedthod : Cr:c\aH-ElC0H.EmM\I\METHODS\121803.u
~~ Last Changed 12/19/03
01:56:57 pn
2a 2 sul1
I|. = T563
| Toes
73597 (CRENSTORT GFTTER veer cn BlES, SW FgVar
Fl o= -
> ag
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|
|=
lw I
1 83, IGA7z4697 (CHEWSTO 1687S00ISTTV7 2F0GHAoPI0ES0:2og4,SV,Fi Var
0000]1
8187-10Surogate
[I --- !|
15000
|
| | oo
I 500
|
| I.
i
I
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| 8"30acStuarrogar 0s0s0.ss
781a87 1265902781 SmsDDl 346699,, B5I1CC--436688..77::436699..77
[ ecooara
I I of apenas
las
Fri, 19. Dec. 2003 02:30:32 pm
Page 1 of 1
650309
[~ SSaammppllee NIanfmoe::L0001444-20
1
| bata rite c:\monm1\DATA\Chenstor' 11667385\A453760\FC000025.D
[InAjceqcOtipoenraDtaoter::1jm2ill/er181/0:500:307 BM SvieaqlLiNon.e
Ta24s
~. DInislturtuimoennt fiPC00L4
Inj. No.
1
ml vel. :
sul
[sec novos + res0.0
~~ ALansatlysCihsanMgeetdhod :: C1:2\/H1P9/C0H3EM\1\METHODS\10211:85063:5.71 pm
[ers anayass o oeseruono casos acs
r
SOT 69, E1C-7(C3HE6MST8OR.TI7663738883537
Fog, SIV,Frag Var
[ =|
I -20
= 180 |
I 160
- | .
WSO 469, E1Cw48812453.7 (CHEMSTORY14667365RAGSe SUFGO0r 0025 0 a A ereP seNos geE ,SnW.SFrie anr, :Vuar
8183 010Surogat
|
| 1750
15000:
|
|] eo
|
10000
|
| 7500
0
I] =
o
[-coos mows wo3 m nz I
| a810AScuirdrogat 30.7020.65
50..108030
ween
1o67914
|
5
sa5 na
MMSSDDLI 436699,, EEIICC=-346688..77::346699..77
|
| ecooars
+++ EndofReporrrt
TT
Fri, 19. Dec. 2003
02:31:06 pm
0043
Page 1 of 1
600310
[aSammple Name:STD 500 pot
'
Data file. -C:\HPCHEE\I\ORTAChanator I1GE7635\MSSHUBNFCOOOUES D
SeImloenedmgoirrmienenrporee:
2mA /l8e0 0
SBpaanthe
Ld%S1
[7 . B dEelg,vawonty nooaes |+- S sSeNnsELo emoneniPenIs.S
|" ces amstyaie of pertiuore cashomyise acide.
|- ET
Tae on ee
|[|=
I~
|
[ i --
1
Io. [ EORS ROSE PTE oS
[| =
so [1] ee
| | 10000-
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| corpoms ome wr wm ven
ot
[a 80 SienR a 215.35 i The eHnuem weemnivesh, Emaesedse. oToans
a reer
ree
| -- Tet the oo TR OBA 044 nage 2 08 1
650311
[sam mple n Name:solvent blank
:
Data file iC: \HPCHENAt4or\16O674N93T\AA497\98C4\FhC0e000m27s.5
fP Tnieyc= tiobn bate
iE ie
HIRE ET
Sinem Hs
e e Sei l l me
su43
[7 preeq, Wemaemeog.eOd seCnteon
HS on
[7 sens amavis of pertiuoro caromiic acids
r BRSTCTBT ATONCETE PTS Fo, SF
-
[lo
fl o= "
I"
180.
170
| | 180
r
BRE2 ETO 4ATTAFA6TE TESFo SiFo ir in
_
204
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80
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wom
1
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1
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wme l w=ool 3i63, Emiceeie eiee
1 orp cammssmmssssssssssscsssssssssssssssssssssssssssssssssssssssssszsssssssssss
|| scoouna
ie Fei, 19, boc. 201 02:31:26 po uo04s rage 1 ot 1
690312
Esasptk e nase: 50 oo
:
Sata file Co\HICHEI\1\DNEMChesstor\LLGGTSAG\ASOOEEA\FCOADO28.D
~ hIseicmteiemomnmasecs |+ eiiaiients erm sHfB irhneosasd?i
[ EAE disLWac-- noa | EGxSEubdEitinsweioos 2H10S03.T
| ses anatyass of pertiuoro casboryiic acids.
[[r- e cm
Co
srocrasse ees
[7] w0= i
|
[1]
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[ow
w
[| =
| r EE 8 CTr O TERIA AoPrEeS 8S ;
2x00]
8.174. C10Surogate
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--
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|| ecooais
SETe
Fri, 19. Dec. 2003
0046
02:32:39 pm
Page 1 of 1
600313
[* SSaammppllee NIanfmoe::STD 100 ppb
1
Data file :C:\HPCHEN\1\DATA\Chemstor\11667644\AS02400\FC000029.D
|" hIIonngsjterOcutpmieeonnrtaDattoer::2Cm102i/0l14l81e/4r03 11:5BY0:4Svme7iiqa.lLNNiono.e o:::
2921
Dilution ii
wil vel. :
ES
| AAncaqlysMiesthMoedthod :: CF:co\-H1E0C.HnEM\1\METHODS\1218013
[mest Changed: 13/15/03
01:56:57 py
| 1c/S analysis of perfluoro carboxylic acids.
r
HST53, ECH388723897 CHETGNSSARSSCETADIFOCO0R002T90)
i
]
728-08
APIS: Ko, SW.FirVor
[1 w
[| owa
ro1000 |i
[| =
Il o HsISrD 469,EEC4E85469T.7 C(CHENSTORYHS1657638SOTI0OFCO:RDTE0A APNoFgi,SEW.FSs,Var
1
8178- o10
[7] wm
NE
|
|
| 100
|
[--commsol roo r3r nr. i es 3 siian
| 8"10acsuirdrogac 8884..1419
87.137386 3465969635 mSoDbLi 436639,, EEIICC--346688..77::436699..77
|
end ofReportt+ |
Fass etn osm mm uu4y meres
ponte
Sample Name:STD 250 ppb
I" Sample Info:
Data file iC: \HPCHEN\1\ON1T16A67\68C1\hASe04m57s6\tFCo00r00\30.D
1
[rTeoE mvaaorrT| sJemoiiitear RE
wnaitenee
s:
I -- Siucion if
ve
sul
rAEdiyeis Wethod | CLX\RERCHEN\L\HERHODS\S1218e03.4 om
10S analysis of perfiver camorylic acids.
I - . TE E5748 ESTO ESTH SCF OTSe]es PYESNa SW Fr
--
Il oma|
Fl
a0
od
2
4
8
min
[7] =! 2187 610Surg | -
NIST45, EIC=4637469 (CHEMSTOR 63789 AGOISTFG000300] PINE og.SS IM,F, rag:Var 1
|=
wom
7
rm
I" .
T
T
7
-
topouna_ soount (g/m) KT. Area
stnat
|ErSion 350.33 To s m eine wMesRt sSe, sEiomnsRI7n36n0d7
-
reer
sommes
00414
Pri, 15. Dec. 2003 02:33:31 pm 0048 Page 1 of 1
10315
E garple e Name:STD 300 po
2
Data file iC:\HICHEN\L\DATA\Chemstor\11667759\ASOBSO8\FCO000T>1
[oe ph [7
SPIbnjioeRcpotieolniDeatee
: 12/19/03
iEC
12:21:11 AM SefH rqrelLn ainde :
su3li!1
[[roogEvatmeotSethod || rCL5 eoSnoabETHiODS\NL2100L0. on
LOTS aratyat of pectin cawaAe wikis,
n ST u_--
07 Aves Far
hy
[] om
I] | woo
| | | me
[7 a7a
I FO SA SSTNRPTNo:ESWWS,AF:a Var
|
arin
[|
: on]
|e
ro.
[~somos mows wo1rms ar. 1 wees
rr
3 Taser
| 10 Surrogat 527.34
8.188 234376
|
Jz
wenn ae, menses Tae
MSDL 469, BIC-468.7:469.7
|" coouza
+++ End ofReport +++
TTT
Eri, 15. Dec. 2003 02:33:56 pm G049 2age 1 ot 1
600316
[seSammiplse Nmaimee!:STD 750 ppb
1
Data file :C:\HPCHEM\I\DATA\Chemstor\11667808\AS08526\FC0000.32D
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