Document zbzJVw52rrnOZXoQRO9MjgBL6
w JT *' ' ^ 32(
CODE RC-14-A
- %.3y1982 ' L2J3
7"b a t e . >
7'To t 7
3666* <. e s t w g t >
D. V.
PROCESSES
APPROVED BY
( )RC--14-A (I) EWk 12/17/81
COMTYP JOB NAME: 32RC014AMI
TYPED BY: JMH
EQUIP I KENT I
J !
NAME: *WATCHUNO* RED B
| USE I N-CODE |"ACCT
j LBS I
| LBS
-----------I------ !------------------ ---------- _------- :--- ------------------------------------------------- i -----------\ :----'----------- j -------
j J NOTE: DO NOT START IF PRESS WILL NOT BE
|
j
|
I } AVAILABLE WITHIN 3 HRS AFTER MAKING..MAKING]
I i SUPV TO REVIEW WITH P.R. .SUPV 6 RECORD:
j
I. I PRESS WILL BEa READY: __________ M___ _/______ |
!
i P.R. SUPV,,JlJL START MAKING_i_L,,_M_____ /
_J
. || ||
| | *j |
I I MAKING SUPV__T_<SL_,,
I|
|.
ii
i
f i NOTE: RUN 15* WATER INTO V-964. PUMP WATER |
S | *,
i |
! i FROM V-964 THRU DISTRIBUTOR. IF WATER DOES j
i
I
j | NOT COME OUT.OF ALL DISTRIBUTOR HOLES WITH 1
i
j`
I i FULL FORCE. NOTIFY SUPERVISOR'.
! |'
l'-
PREP i
RECORD:
BATCHES SINCE SPARKLER LAST
D. AFTER 4 BATCHES, CLEAN, DRESS
SPARKLER & PRE-COAT WITH 13* FILTER AID
OjpAW FOR SI 4 2-CHL0R0-4-AMIN0T0LUENE-5
ULFOyiC ACID
I N FOR S35 3-HYDR0XY-2-NAPH THO'I CT A
INSTALL DV & CV RECORDER & CONTROLLER CHART
NOTg,,:_NQTIFY PRESS ROOM BEFORE ROPING OFF
RfA UNDER V 9.22
CLOSE OVERFLOW OUTLET VALVE FOR DISTRIBUTOR
LINE AT REAR OF VAT
i .1 777-A i 746-C
l/ls-d
921 RUN 1*3" < 130G3 WATER INTO V-921 & HEAT TO .
16-166 DEG F
`
ADD IN 2-3 MIN (DRESINATE X) ,
136 330-A | 13
T STIR 5 MIN & RECORD; PH^t(3L(9.5-16.3) "STIR 26 MIN OR LONGER TO DISSOLVE FOR S46
wav 4 1982|
N 37*' < 762G) WATER INTO V-922
GH IN V-926 SODIUM HYDROXIDE & RUN IN
TIC SOLUTI ON)
M //?_ ,
X
7-D 226
TURN ON AGITATOR & STEAM & DUMP IN FROM SI
740-C 1 157
2-CHL0R0-
l ot .
*1 0.0X
4-AMINOTOLUENE
5-SULFONIC .
ACID
UMP IN (ACTIVATED CARBON) MP IN DICALITE, FILTER AID
25 11 3-A 25 16 777-A 10
HEAT TO 212-214 DEG F REICC IRD : HT.
DEG F
tc __ DEG F
"OWTs.
RECORD7 xj y y iin ( ) IF NECESSARY AD. TO 4-BY
?ODIUM HYDROXIDE
ASSUME >0%
7-D
LOT*
OQMTfP JOB NAME - 32-RC014AM'I PAGE 02
DATE PRINTED V27/82
EQUIP MENT
PAGE 02 OF 03 CG 32 CODE RC-i4~A
.I USE ! N-CODE I ACCT
<13 I LBS |
t LBS
------- I--- I -----------------
922 |flT I STIR 3 MIN AT 212-214 DEG F THEN SHUT OFF !
!
3 I I STEAM,. WATCH FOAM, RECORD: SPARKLER
|i
CONT 1 L^-PPESSURE _>_,,PSI, IF NOT ZERO NOTIFY SUPVRI
|
UPr| CIRCULATE 15 MIN OR LONGER THRU SPARKLER | I I UNTIL SOL 1 N IS CLEAR, MAINTAIN^!.L90-195 F|
| j
I I FOR S20. RECORJL START.A v4V 4 F\ IS. LU n Ij^j, a ( nn I ,,, tjf '"r-rtr I I TOTAL --' ` ^ '
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*`
I I HT ._ZJf.D:EG F, REC./M^EG F
MISC 4
cv 5
1 MEASURfl^wratUNI'TS IN V-928 FOR S3 (HYDROCHLORIC ACID) M,,_^,,, bhPjL__ %
?UN 6" (669G) WATER INTO \'~S$P^
I WHEN SI 7 COMPLETE , PUMP IN V-922 THRU I SPARKLER, MAINTAIN V-922 AT 190-195 F. I RECORD: START^&HC^f-TOTAL MIN.jfvL__
m>\
TO" (2400G) WATER INTO V-90^-
DUiJg^eALCIUM HYDROXIDE IN AND STIR
)OTH SLURRY
''
WEIGH' SODIUM HYDROXIDE IN V-926
RUN IN A STIR FOR S39
I TO I
'' . I ,$zto& I I
550 _
I i
i i
"WEIGH IN PT FOR S32 (SODIUM NITRITlp^^, I
922/CV 8
QMPLETE, STOP' PUMP 5. INSERT V-922 J
I
RUN IN 10* (209G) WATER 6 HEAT TO 190-195 FI
CIRCULATE 15 MIN THRU SPARKLER PUMP V-922 I
THRU SPARKLER INTO CV
*I
23-D 1 557
542-D ' 7~D
550 199
i >' 725-A i 368
r14G) WATER & HEAT TO 190-195 F |
JLATE 15 MIN THRU SPARKLER
(
BUMP V-922 THRU SPARKLER INTO CV
[
sIHEN MT BLOW OUT SPARKLER INTO CV
I
JUR IN (IGEPAL CG-630)
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[63 I
TO 165-170 DEG F
!I
RUN IN N-28-D HYDROCHLORIC ACID FROM Si 8 IN I.
I
r2~is min
i y& j
m I AD^UTO 45" (4266G) AT 32-38 DEG F USING.ICE 132X330
I COR^:
STICK.JO____ * .
P ].
S| RUN IN,N-725-A SODIUM NITRITE FROM S23 AFAPI
I
(5-10 MIN) & RINSE IN PT STIR 20.MIN AT 32-38 DEG F MAINTAINING
I j
I J
I +CR, +KIL RECORD: CR.^I^( + ) KI_7___I<+) I .1
i NOTE: (1) IF CR~,KI~ ADD 20# "AS IS*
T1
{ INCREMENTS HYDROCHLORIC ACID- ASSUME 32% !.._____ I
I RECORD: CR._
(+)
+) I I
j (2) IF CR+, KI- ADD 20# "AS IS" INCREMENTS I
I
i SODIUM NITRITE
ASSUME 33%
l____ _1
I RECORD: CR< + > KI..< + )
I' I
979 -B 57-A
28-D 725-A
'63 m*&
: :h%
DUP050060966
LOT- .
COMTYP JOB NAME
14AMI PAGE 3
DATE PRINTED: 7/27/82-
e urn 'ME^T
03 OF 03 CG 32 CODE RC-14-A
* (I)
IN BARIUM SULFATE MP IN FROM S3 & STIR 10 MIN
HYDROXY-2- /N4ftfki N-/-c
)PHTHQTCj 0l C3 W CtTfifZjj.
.rL0T`
I USE | LBS
N-CODE i ACCT I LBS
-------- -I------- -
470 65-A ! 470
! ' /-Ci -1 055 S5
JwKflft I
56 1 ADD FORMAIWAINING 32-38 DEG F THRU S40 f 6 RECORD VOL,,_,______
!|fX330J
57-A
1
931 10
90% 11
RU#37" (363G) WATER INTO V-931 6 ADJ TO |
0-110 DEG F
i
! ADD 6 STIR 20 MIN OR LOGGER TO DISSOLVE FOR!
S44 (STRONTIUM NITRATE)
`
1
ADD AMMONIUM CHLORIDE TO V--903L.
i
712 i 246-B,EI 712 i* I
228 I 165-A ' | 228
CV WITH V-90^AGITATOR ON, IMMEDIATELY COUPLE
12 V--90% THRU UNDERSURFACE DISTRIBUTOR INTO CV
(54-60) MIN. MAINTAIN CV AT 32-38 DEG F.
NOJE : OPEN VALVE TURN. RECORD : ART^,,J>^_, TOTAL MIN_j^fe?_
&r \ sStT:IR. 15 MIN 6 RCRD BASE_X_< +)' DIAZOJSL(
h l ____ (10.0-10.5)
'
IF. rH. IS BELUWJO.O ADJ TO. PH 10.0-10,5 6 RECORD: PHjSskZt SODIUM HYDROXIDE
ASSUME-502 HR 3_ HRS.. HYDROCHLORIC ACID ASSUME 322
7-D 28-D
V-931 INTO CV FROM S38
RCRD PH_&< 10.0-10,5) , IF PH IS BELOW 10.0
SODIUM HYDROXIDE
ASSUME 50%
ADJ TO PH 10.0-10.5 &. RECORD F'l-l/^X. /
. 7-D
'DROCHLORIC ACID .
ASSUME 322
.STEAM EJECT V-921 FROM S8 INTO CV
28-D
iIGH IN DRUM 6 POUR IN (OCTANOL) HfAT T(/1 93-1 95 DEG F JN^70-75 MIN RECORD
25
,588-A
25
IT^j k __DEG F, REC_7A_-_DEG F
STIR 15 MIN AT 193-^195 DEG F. RECORD: * START_JZrMlgjm
g^L^FLOOD TO 180-190 (+/-18;0O0G)
i
\%y^\ RECORD:
5-iO.O) IF BELOW 9.5,
I~
ADJ^FOT PH 9.5-10.0 RECORD PH^^ASSUME 502
PH IS ABOVE 10.0, DO NOT'' ADJUST
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7-D iJ^L
1 STOP AGITATOR
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i
I, WHEN INSTRUCTED BY PROCESSING HALFWAY THRU \
PRESSING DUMP IN 6 STIR 5 MIN STOP AGITATOR]
AND RESUME PRESSING.
J
10
588-A
10
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DUP050060967
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