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BIODEGRADATION (BOD/COD) TEST SUBSTANCE Identity:A mixturecontainingperfluorooctanesulfonatmea;y also be referredtoas PFOS, FC-95, or as a component of FC-185F. (1Octanesulfoniaccid)(CAS # 2795-39-3) Remarks: The 3M productionlotnumber was 1-2303. The testsample is FC-185F, cc 817-19. Currentinformationindicatesitisa mixtureof4% PFOS, 36% diethyleneglycolbutylether,29.29% water,14% ethyleneglycol, 8% Sultonefoamer,8.35% sodium octylsulfate0,.3% sodium laurylsulfate, and 0.06% tolyltriazole. The followingsummary applies to a mixture with incompletely charactedzed concentrations of impuilties.Data may not accurately reflectthe biodegradabilityof the fluorochemical component of the test sample. METHOD: Method: Not noted. Type: Aerobic GLP: No Year completed: 1982 Contacttime: 20 days Inoculum: Not given. RESULTS Chemical Oxygen Demand (COD): 1,200,000mg/kg 1,200,000mg/kg (replicate) BiochemicalOxygen Demand (BOD): 5-Day: 1O-Day: 20-Day: 250,000 mg/L 990,000 mg/L 1,200,000 mg/L CONCLUSIONS No conclusionsgiven. Subminer: 3M Company, EnvironmentalLaboratory,P.O. Box 33331, St. Paul,Minnesota,55133 DATA QUALITY Reliability:Klimischranking= 4. Values are from a summary sheet onlyraw data notfound. Study lacksdescriptioannd recordsofthe method followed.The inoculumwas not propedy charactedzed. There isno characterizatioonfthe testsubstance puritya,nalyticamleasurement ofthe testconcentrationsa,nd confirmationofthe amount offluorochemical components inthe solution. REFERENCES This study was conducted by the 3M EnvironmentalLaboratory,St.Paul, Minnesota,Lab Request number 7544, 1982. OTHER Last changed: 6/26/00 05/30/2000 ENVIRONMENTAL LABORATORY 1 ARCHIVED FINAL REPORT LAB REQUEST NO. 7544 CONTRACT LAB(S): REQUESTOR NAME: EAR EXP COMP DATE: 01/18/1982 DEPARTMENT: 0535 DATE COMPLETED: 02/24/1982 PROJECT NO: 9972210100 PROJECT LEAD: SA BEACH DATE RECEIVED: 12/17/1981 PHONE NO: 651-778-7452 DESC: FC-185F (CC817-19) LOT 1-2303 3M FAX NO: 651-778-6176 -------------------------------------------------------------------------------- SAMPLE DATE CODE DESCRIPTION RESULT MDL or (95% C.I.) -------------------------------------------------------------------------------- 1 96-HR-LC50 BOD-05 BOD-10 BOD-20 COD SLUDGE-TOX 2 COD 1-2303 FC-185F FISH ACUTE TEST BOD-05 BOD-10 BOD-20 COD SLUDGE TOXICITY - 96 HOUR COMPLETE 250000 MG/L 990000 MG/L 1200000 MG/L 1200000 MG/KG SEE ATTACHED REPORT DUP #1 ------------ COD 1200000 MG/KG