Document zbkRJe9Q2o0ozbdMR8ZdOL3w0
LL/iL/iSl
< DATE )
< LOT >
4448* LBS. < EST WT )
PROCESSES < ) YE-721-D <M>
APPROVED BY: FWP 11/08/82
^/^boMTYP JOB NAME: 01YE721DMM
BI.tN.DED BACK: CG 01
-------
^--TPQtttmSJ
EQUIP MENT
NAME: MOLYBDATE RED
1*f>0lrAIN FOR S-12 2/4M3BTAIN FOR S-34 3 M/OBJAIN FOR S-38 4^tO0BIAIN FOR S-40 5ATJJJEffAIN FOR S-44 6iH^uBTAIN FOR S-47
USE LBS
68 600 120 195 350
61
| | ACCT |\ N--CODE ! LBS
1I 108-A ! |1 4-A |
3-A |
32-D | 3-A I
711-BD 1
68 600
120
195 350
61
WEIGH IN: OPTR
I_
OPTR
,,% 3f$o_ MK T-____ , .. JL
I--
I WEIGH IN; OPTR UkL,,-, .MK 4E& J33&3L%
OPTR ____ , MK
T-,,_, ______%
10-D 423-D
| 1509 I
| 243
10* <500 G> WATER INTO V-358 ?UN V-359 INTO V-351 6 PUMP IN V-351
ADJ TO 55* <2600 G> `IFT IN N-108-A FROM S 1
fR 5 MIN 6 RECORD: PH^2/JT?9 10*0) ADJ TO PH 9.8-9.9 & RECORD: PH
ASSUME 50%
ASSUME 66%
RUN INTO V-354 FROM BADGER METER. 0PTR_//21___ , MKh2.____, Shi
IMP FROM V-351 TO V-358 FLUSH V-351 t, PUMPING LINES WITH 10O0G
WTER INTO V-358 ADJ^KO 74 * <353& G> AT>^69*F
iCDRD: VOLVM.* 6 jUfL-*F STIR 5 MIN^ Je CORD: PHM.<' .2-7.4) &
G/ML /:J@S2. < 1.055-1.058) NOTE IF G/ML OUT OF LIMITS FILL OUT CHECK
LIST 6 ATTACH. TAKE 1 QT SAMPLE.
RUN 20* <996 C) WATER INTO V~G?j?_
STORAGE TANK TO PUMP, fROM.
CIRCLE ONEb 402 410 411 420 424^425}
SUPV:
STORAGE TANK MUST CONTAIN AT LEAST 1900
GAL : 402=39.*.--.410=20* , 411=38*, 420=20*,
424=20 * C425=25T *STORAGE m^rTTTOT HAVE STIRRED AT LEAST
20 MIN SINCE LAST ADDITION OR ADJUSTMENT
wSTGRAGE TANK MUST BE ISOLATED UNTIL ALL
DUMPING FOR THIS BATCH IS COMPLETE /W*
SET METER FOR 300 G & PUMP TO SV
j
LOT: EQUIP MENT |
sv~
5 CONTI
1
COMTYP JOB NAME: 01YE721DMM PAGE 02
BATE PRINTED:11Z08/82
USE I N- ACCT LBS CODE LBS
AT APPROX 100 G WHILE CONTINUING TO PUMP, CHECK PH 4. DENSITY. RECORD BELOW. IP NOT IN RANGE STOP PUMPING & SEE SUPV.
* <3.2-3.7)
DENSITY: J3.171_ G/ML <1.270-1.328) IP S-23 OK A WHEN S-22 COMPLETE, RECORD
DENSITY JbaJ2*&/ML ON TRAPPED SAMPLE !0M END OF S-'Za PUMPING.
USING DENSITY FROM S-24, FIND METER SETTING FOR
SECOND PUMPING IN TABLE BELOW. NOTE: TABLE ACCOUNTS FOR 3O0 G ALREADY PUMPED IN S-22. CIRCLE DENSITY 6 SETTING IN TABLE BELOW.
**# TABLE **
1 G/ML 1 1.270 1 1.271 1 1.272
1 1.273
f 1.274 1 1.275 1 1.276 1 1.277 1 1.278 1 1.279 1 1.280 1 1.281
1 1.282
1 1.283 1 1.284 1 1.285
1 1.286 1 1.287 1 1.288
1 1.289 1 1.290
SETTING i G/ML 1259 1 1 .291 1253 1 1 .292 1248 1 1 .293 1242 1 1 .294
1236 1 1 .295 1231 1 1 .296
1225 1 1 .297 1219 1 1 .298 1214 I 1 .299 1208 1 1 .300 1203 1 1 .301 1198 I 1 .302 1193 1 1 .303
1187 1 1 .304 1182 1 1 .305 1177 1 1 .306
1171 1 1 .307 1166 1 1 .308 1161 1 1 .309 1155 I 1 .310
1151 1 1 .311
SETTING 1146 1141 1136
1131
1126 1121 1116
1112 1107 1 103 1098 1094
1089
1084 1080
1076 1070 1066
1061
1057 1053
1 G/ML 1 1.312 1 1.313 I 1.314 1 1.315 1 >416
1 1.318 1 1.319 ! 1.320 1 1.321 1 1.322 1 1.323 ! 1.324 1 1.325 1 1.326 1 1.327 1 1.328 1 1.329 1 1.330 1 1.331 1 1.332
"s e t t in g 1
1049 1 1045 1 1040 1 1036 1
b
1023 7 1
1019 1 1015 1 101 1 1006 1003
999 1 995 1 991 1 987 1 983 1 979 1 975 1 971 967 1
1 1 1 1
1
1
1 1 1 1 1 1 1 1
1 1 1 1
1 1
1 l 1
SET METER & PUMP/d^^G (RECORD FROM TABLE)
I FLUSH LINE WITH WATER INTO SV FOR APPROXIMATELY 130 SECONDS
I I
I
34TADJ LEAD NITRATE TO 3244 G I 247) AT 67-69*F
HUtW 66.5*
I 41-D I
CORD:
___ *F & ICE CONSUMED C330S/BLOCK) 330X__| 57-A
STIR 5 MIN 6 RECORD PH: lk-2.. <2.2-3.7) ***# USE TITRIMETER TO ADJUST N-41-D PH **#*
I !
IF NECESSARY ADJ T.0 PH 3.0-3.1
ASSUME 66% ______ I 33-D
I 6 RECORD PH: 4,LL-
ASSUME 50% -JJxz. I 7-D
i^NOTE: DILUTE N-7-D 10:1 WITH WATER BEFORE ADDING
30| RECORD: JbJJrJ G/ML <1.12S-1.129) IF OUT OF SPEC
I
L^FILL OUT CHECK LIST & ATTACH.
34T STIR AT 67-69KF FOR S-33. TAKE 1 QT SAMPLE.
4094
::x:
DUP050059744
LOT _________ COMTYP JOB NAME: EQUIP MEN'r I
01YE721DMM^ PAGE 3 .{'sk.
DATE PRINTED:11/08/82 USE | N- | USE LBS | CODE | LBS
i\T~
5 CONT
OBTAIN 1 QT SAMPLES OF S-19 & S-31 SOLUTIONS & TITRATE TWICE
NOTIFY SUPV IF ML N-10-D IS NOT IN RANGE
9.5-9*9 OR IF THE TWO TITRATIONS DIFFER BY
MORE THAN 0*10 ML N-10-D (IF YES, FLUSH ALL
EQUIPMENT & REPEAT TITRATIONS). DO NOT
PROCEED IF N-10-D TITRATION IS OUT OF RANGE
ADJUST V-358 FOR A TITRATION PH OF J00 T0"'fT?01
I
FROMIWEJNAL PH &
IN-LINE TITRAT^(|^p ML N-10-D
RECORD /
Z/2T1
33-d | _ 7-D | A
I
sv
6
34#|^^p*J^HUNEDNE'R"SS-U3R2F'A"TClEfRDAIfSI0T.NR"IJ0lUKT7O""RSSTRIlNi<TEO""v-S:V358IN^fH,4R4U-4~6B0MfHIN"
RECORD : START
TOTAL MIN__M_&___
NOTE: STRIKE TIME UPrWHEN 1/2 VAT BOTTOM SHOWS
A BUBBLES APPEAR IN SIGHT GLASSES IMMEDIATELY DUMP IN N-4-A FROM S 2 & SET TIMER
FOR 15 MINUTES
DURING S 34, WASH IN V-358 .
&A STIR 2 MSN & RECORD PH_J_'_i__ < 1.7-1.8)
I PBXS,_J|l L._<MUST BE + )
37-1"STIR TOTAL OF 15 MIN FROM S-34 G
A RECORD: TEMP,,n^_F <67-73#F>
38**Vi>UMP N-3-A FROM S-3
I
3rs> STIR 3 MIN
I
40^1 POUR IN N-32-D FROM S-4
I
4.K1 STIR 2 MIN
I
m f# RUN IN LIQUID ALUM USING BADGER METER 43/4^ STIR 3 MIN & FLUSH ALUM LINE WITH WATER
604 115-D| 302 I
a4 j - DUMP IN N-3 FROM S-5
I
4jr I STIR 4 MIN FOR S-49
1
RUN IN HYDROCHLORIC ACID USING WEIGHT & FLOW. *
390 I CONTROL PANEL
MK _jL_,
S&JL 28-D | 90
7 L*--'
MK _____ _ ______%
AST\ DURING S-45 SIFT N-711-B FROM S-6 INTO V-390
28-D |____ * I
i^HdlTH AGITATOR ON IN 1-2 MIN
>I
4J^rSTIR 1-2 MIN TO MILKY SOLUTION
SV 4-'T"w HEN S-45 COMPLETE, IMMEDIATELY RUN IN N-711-B 0 I SOLUTION GRADUALLY OVER 5 MIN PERIOD INTO SV
j WATCH FOAM!!! IF FOAMING IS EXCESSIVE, STOP
Jt' UNTIL FOAM SUBSIDES.
5^,1 DUMP IN BLANC FIXE N 5-1 | WHEN SCHEDULED, DUMP IN BLEND BACK LISTED ON
| TOP OF PAGE 1
A RECORD : CODE
LOT
___ *
\5%A' STIR 20 |SS I RECORD:
PMHIN__S---/(-i < 5 * 8-6 * 0 >
| IF NECESSARY, ADJ TO PH 5*8-6*
ASSUME 50%
& RECORD : PH-______KTl-
ASSUME 66%
FLOOD TO 153* <7298 G) G STOP AGITATOR
275
128-Ai 275 I
I
I I I 7-D I<__ k_. 33-D |___
I
, 'T>RT
TMfc S&wHe Td l $6 rtS/lf
DUP050059745