Document zbQBYVno2kre610V3g8Komd13

VUo MjiMfi ADfchkmof Vfcto Owmical Compony Highway 25 ft* Otic* Bax 91 Ahontooiv MinWppi 39730 Phona (601) 3494111 LETTER OE CERTIFICATION Date: Customer: Athol Manufacturing P.O. Box 105 Butner, NC 27509 h VISIA Product: Sty Trailer No.: -gJj JET7 Attention: Tom Baucom, Mgr. Tech. Services Lot No.: Date of Shipment: j j ,, "2^-S- "T ^ Order No.: ifc? j.3 S'<3-J & 3 Moisture, % ABR-1A Bulk Density, gm/cc 8.410 Brabender Dry Time, mins 8.450 Particle Size, % on 8.300 40 Mesh 200 Mesh Pan Residual VCM, ppm 8.955 Inherent Viscosity 8.600 / $.0 0 ___ J<3 Not more than 8.5 PPM This material was produced to yield an inherent viscosity in the range of /OO to / Laboratory/Supervisor/Lead VAB.000120959b Customer PVC BULK TRAILER ANALYSIS Particle Size Distribution: Screen Analysis Mesh Size 40 Gross Wt Tare Net Wt % on Mesh 8 0 & P.DO Screen Analysis Mesh Size Gross Wt. Tare Net Wt % on Mesh 40 Min On Rotap shaker. 49 gins. Resin plus 1.0 gins. Carb 60 80 100 120 140 200 Glassy Pan Part. <-5~? L0 Min. On Rotap shaker L3A 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 t>,67 /3 Glassy Pan Part. Remarks Star 207A Revised 1/12/87 , - --- ......... - ------- --^-VAB.0001209591 isva vnvyvnarv AOMMMof Vifto Chwmcd Company Highway 25 Post Oroca Bax 91 Abtfd--n, Miniirippi 39730 Phono (601) 369-8111 LETTER OF CERTIFICATION Oats: // // 7 J> Customer: Athol Manufacturing P.0. Box 105 Butner, NC 27509 Trailer No.: Attention: Tom Baucom, Mgr. Tech. Services Lot No. : Date of Shipment: f// *70 Order No. Property Test Method Moisture, % AER-1A Bulk Density, gm/cc 8.410 Brabender Dry Time, mins 8.450 Pai'ticle Size, % on 8.300 40 Mesh 200 Mesh _ -5*'/____ j.Lt____ PPm 8.9 5 5 Not more than 8,5 PPM Inherent Viscosity 8.600 This material was produced to yield an inherent viscosity in the range of to 4JLijL- VAB.0001209592 X PVC BULK TRAILER ANALYSIS Date / /-~ t Customer ATh&.t Technician O.X U Product 6. MOIST r, 0$ FRONT 1 1 CON'T. l1^ 1 \(- I1 GEL 1 1 11. I Trailer Number. 7^- JIJ JT/ Time Order BULK DENSITY DRY TIME COLOR L= vise RVCM A= -//* I L= MIDDLE [ * 1 11 *> * 1. II I END 11 -1SM1 * B= Particle Size Distribution Screen Analysts Mesh Size 40 Gross Wt Tare Net Wt H on Mesh O'** 0* C7 ^ Screen Analysis Mesh Size Gross Wt. Tare Net Wt H on Mesh 40 Min On Rotap shaker. 49 9ms. Resin plus 1.0 gins. Csrb 60 100 120 140 200 2.n 43-1* IS. 12 4a 49.0 LLA ~I.Oiw LC3 4ul Min On Rotap shaker 49 gins. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pen Part. LA Glassy Pan Part. Remarks Star 207A Revised 1/12/87 "4 ,Tf i. VAB.0001209593 Vista Polyman A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730 Phone (601) 369-8111 LETTER OB' CERTIFICATION Dat% Customer: 30 90 Athol Manufacturing P.0. Box 105 Butrser, NC 27509 Product: vm Trailer No. : 7-2&0 Attention: Tom Baucom, Mgz*. Tech. Services Lot No.: Date of Shipment.: *30 Cki. 90 Order No. : %3/'3#&-3t,7 Pnopertx Test Method Analysis Moisture, >9 ABR-1A Bulk Density, gm/cc 8.410 Brabender Dry Time, mins 8.450 m Particle Size, % on 8.300 40 Mesh 200 Mesh Pan ___ JJL Residual VCM, ppm 8.95 .'5 Not more than 8.5 PPM Inherent Viscosity 8.600 This material was produced to yield an inherent viscosity in the range of__ /.fiD__ to A0Y___. upervisor/Lead VAB.00012095^ PVC BULK TRAILER ANALYSIS Date Customer Technician FRONT % cT i Product Silo \o<\0 i im\*m hi T- Z- <? Trailer Number. Time T)too Order MOIST CONT. Bottom 1 Top j Bottom 7.............. A.. 1w * '1 i A GEL I BULK DENSITY I M DRY TIME COLOR L == )9d-hl A - # f 2. vise 1I B= l. L * RVCM MIDDLE II END Particle Size Distribution: Screen Analysis Min On Rotap shaker. 49 Mesh Size 40 Gross Wt. Tare Net Wt. 0.00 % on Mesh Screen Analysis 60 80 100 .It JS.S3 .3 13.1 31.1 Min. On Rotap shaker 49 m Mesh Size Gross Wt. 40 60 80 100 Tare Net Wt. % on Mesh Remarks Star 207A Revised 1/12/87 >r ----------------- A- *w VAB.0001209595 Vmu rayvnvrv mwon or Vbto Qiwwicol Compony Highway 25 Pbct Offica Box 91 Abardawy Miiii-ippi 39730 Phone (601) 369-8111 LETTER OF CERTIFICATION Date: 6> Nay. 9o Customer: Athol Manufacturing P.0. Box 105 Butner, NC 27509 Product: Trailer No. T- VISIA Attention: Tom Baucom, Mgr. Tech. Services Lot No.: Date of Shipment: A/cv* Order No. : Y3/38f-3t Property Test Method Moisture, % AER-1A Bulk Density, gm/cc 8.410 Brabender Dry Time, mins 8.450 Particle Size, % on 8.300 Analysis . /J _ . S'// S'.G BvikB 4^IB 200 Mesh Residual VCM, ppm Inherent Viscosity 8.95*5 3.800 3.1 /./ Not Kt than 3.5 PPM This material was produced to yield an inherent viscosity in the range of ____ to __ /oV a tory rvisor/Lead VAB.0001205596 PVC BULK TRAILER ANALYSIS Date U'J, Customer Technician M4^rC Product Silo___ Trailer Number. Time 0930 Order FRONT 11 MOIST CONT. Bottom Top I Bottom j GEL !. .......... 1 1 11 1 1 ba joa$3 2. BULK DENSITY 1. ,r// 2, rr P" FT T DRY TIME l S%0 2. 1. COLOR /oot fo<t B = /// MIDDLE 1 1 * T 11 1* It -i ** * 1a rr 1. * I. vise RVCM END T ba 1 1^ * 1 1 mm a sb e Particle Size Distribution: Screen Analysts to Mesh Size 40 Grose Wt. Tare r Net Wt % on Mesh d.oo 0,L 0 Screen Analysts Mash Size Gross Wt. Tara Nat Wt % on Mesh 40 Min On Rotap shaker. 49 gms. Resin phis 1.0 gms. Carte 60 80 100 120 140 200 Glassy Ran Part. 2f./ //. 2i. (tSS Z3 j.i 22.C tl.l *,r S.7 Min. On Roteo shaker 49 oms. Resin olus 1.0 ams. Carte 60 80 100 120 140 200 . rj /,/ Glassy Pan Part. Remarks Star 207A Revised 1/12/87 Labor ry Supervisor/Lead i f Jk f VAB.00Q\1 2^597 Vista PMyiMfS ADWoncf VMo OwnhcoI Compcmy AbwdNit MMNtapi 39730 then* (601) 369-ill1 LETTER OE CERTIEICATION Date: 19' ~L? 0 Customer: Athol Manufacturing P.0. Box 105 Butner, NC 27509 Product: Trailer No.: 7"' Attention: Tom Baucom, Mgr. Tech. Service Date of Shipment: /G- r? o Lot No.: Order No Prggggty Moisture, % Bulk Density, gm/cc Teat MsShgd AER-1A 8.410 Analysis *y i -v Brabender Dry Time, mins 8.450 -2jZ Particle Sise, % on 40 Mesh 8.300 (a. t tf C 200 Mesh Pan y Residual VCM, ppm 8.955 Not more than 8.5 PPM Inherent Viscosity 8.600 This material was produced to yield an inherent viscosity in the range of / O O__ to / 9 q . Labor Lsor/Lead *> * VAB.00Q12vW5*98 \ ' 4 ^ * PVC BULK TRAILER ANALYSIS Date Customer Technkian^dJL FRONT Product MOIST Bottom I CONT. Bottom GEL I I I. Trailer Number_Z Tlmg o 4,3 O Order OA6 BULK DENSITY DRY TIME COLOR l #>'(,3 vise So <7 /./r RVCM (a W MIDDLE i. END s# 1*|i. i. i. L - 1 ^ |2. a 1 A- a B= Particle Size Distribution: Screen Analysis La Mesh Size Gross Wt. Tare Nat Wt % on Mash Screen Analysis 40 Mash Size Gross Wt. Tare Net Wt H on Mash 40 Min On Retap shaker. 48 gms. Resin plus 1.0 gins. Garb 100 120 140 200 Glassy Pan Part. 1.73 2Z.27 /3-0f 7Z LI 3.1 2LHA n.3 SA 4. Min. On Rotsp shaker 49 gms. Resin phis 1.0 gms. Carto 100 120 140 200 AW (.4 Glassy Pan Part. Remarks. Star 207A Revised 1 /12/S7 % VAB.0001209599 VbtoM)fiMn ADMaonaf WQ wWPHCul \*09lipyfiy Highway 25 Port Ofnc* Box 91 Ahwdmv Mwaappi 39730 Phoo* (601) 369-8111 LETTER OF CERTIFICATION Da t o;: fO -fCr1 r Customer: Athol Manufacturing P.0. Box 105 Butner, NC 27509 Trailer No. Attention: Tom Baucom. Mgr. Tech. oervice; Lot No. <r>? Date of Shipment: lQ~l(o Order No. : ^ Property Test Method Moisture, % AER-1A Eulk Density, gm/cc 8.410 Brabender Dry Time, mins 8.450 Particle Size, % on 8.300 40 Mesh 0. 06 200 Mesh Pan -A*- Residual VCM, ppm 8.955 Not more than 8.5 PFM Inherent Viscosity 8.600 This material was produced to yield an inherent viscosity in the range of 1.00 to / O . Laboratory Supervisor/Lead VAB.000120964b S flat- fO-/C'fO ________ Product^___________ __ Trailer Number Customer . AfioK Siln i 1 Time /fS * Technician_____ __________________________ _ Order No. f'2-%0 ? 4 Particle Size Distribution: ScrMn Analysis /O Mssh Size 40 Gross Wt. Tare ^ Net Wt. H on Mesh )t0Q 6.0 Screen Analysis Mesh Size Gross Wt Tare Net Wt H on Mesh 40 Min On Rotap shaker. 49 gem. Resin phis 1.0 gms. Carb 60 60 100 120 140 200 Pan Glassy Part. 30 2/,/r S' 2-. St, j.a ,, Lo r lfi K<3 JV. 7 /7.J____ +<7 3.7- /. Min. On Rotap shaker 49 gins. Resin plus 1.0 gms. Carb Pan 60 80 100 120 140 200 Glassy Part. Remarks Star 207A Revised 1/12/87 A 01209601 Vito Mftmn A Division of Tiiw vifSHBODi MNnpony Hfebwmr25 fort Often Bax 91 Abm6mn, Mhiiiiippi 39730 Phono (601) 369-3111 Dat: /# _ ^ Customer: Athol Manufacturing P.0. Box 105 Butner, NC 27509 Product: Trailer No.: Attention: Tom Baucom Mgr. Tech. Services Lot No.: of Shipment: j $ _ yfj -JG Order No.: Property Te5t Method Moisture, % ABR-1A Jt.7 Bulk Density, gm/cc 8.410 Brabender Dry Time, mins 8.450 y-9 Particle Size, % on 8.300 40 Mesh CO 200 Mesh an Residual VCM, ppm 8.955 Not more than 8.5 PPM Inherent Viscosity 8.600 This material was produced to yield an inherent viscosity in the range of l.&o to r VAB.00012096f * PVC BULK TRAILER ANALYSIS Customer SUo 30 - (, 7/ Technician AjT 4- /f, // Order No. J3/3 Trailer Number _ Time J03Q ~3& / Particle Size Distribution: Screen Analysis Mash Size 40 Gross Wt. Tara Net Wt. H on Mash ft 4? Co Screen Analysis Mesh Size Gross Wt. Tara Nat Wt. H on Mesh 40 Min On Rotap shaker. 49 gms. Resin |plus 1.0 gims. Carb 60 80 100 120 140 200 Glassy Pan Part. O '%<> A Min. -?/.-?? 4lX 31.2 tSH /{,. -*? f S. / o(? 2.( On Rotap shaker 49 gms. Resin plus 1.0 gms. Garb 60 80 100 120 140 200 a 4 Glassy Pan part. Remarks J Star 207A Revised 1/12/87 VAB.00012uA03 ip ir Visla Myman A Division of Vhla Chamicoi Company Highway 25 Post Ofhc* Bax 91 AbanJaan, Minmippi 39730 Phona (601) 369-8111 LJiTTER OB' CERTIFICAT X OISI Date: Customer: Sis' Se^i. 90 Athol Manufacturing P.0. Box 105 Butner, NC 27509 VBIA Product: jy/r Trailer No. : ~T-2.9/P Attention: Tom Baucom, Mgr. Tech. Services Lot No Date of Shipment: XS~ 90 Order No Property Moisture, % Bulk Density, gm/cc Test Method ABR-1A 8.410 Brabender Dry Time, mins 8.450 Particle Size, % on 8.300 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity 8.955 8.600 Not more than 8.5 PPM This material was produced to yield an inherent viscosity in the range of to __ ________ . VAB.000120^^04 A Date Customer Technician PVC BULK TRAILER ANALYSIS Product Silo___ Trailer Number Time Order No. Particle Size Distribution: Screen Analysis______ ^_______ Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb Mesh Size Gross Wt. Tare --/ Net Wt. % on Mesh Screen Analysis 40 O-Oo Q-& 60 80 100 120 140 200 o^3 o,S~ 15.4 7 lb'55 S/.9 33 i l/Ol <2 /. (s 3,si 7,0 Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Mesh Size Gross Wt. 40 60 80 100 120 140 200 Tare Net Wt. % on Mesh Glassy Pan Part. o.i7 o-9 Glassy Pan Part. Remarks Star 207A Revised 1/12/87 - VAB.QQ012096Q5 mo rovynwn ADMaonof Virto Owmiooi Company Mi uUyilrawaomv 25 MOne Box 91 Abadnn, Miwiaippi 39730 Phono (601) 369-8111 LETTER OB' CERTIFICATION Dat,:f- Z?"?0 Customer: Athol Manufacturing P.0. Box 105 Butner, NC 27509 Trailer No, ugio Attention: Tom Baucom, Mgr. Tech. Services Lot Mo.: Date of Shipment: ^-^3 -- Order No . : $3f 3 $8 Property Test Method i Vi ! Moisture, % ABR-1A Bulk Density, gm/cc 8.410 Brabender Dry Time, mins 8.450 - Vi Particle Sise, % on 8.300 40 Mesh ___ 0.0 200 Mesh Pan __A1_ Residual VCM, ppm Inherent Viscosity 8.955 8.600 Not more than 3.5 PPM This material was produced to yield an inherent the range of tc. _Lpj___ . Laboratory Supervisor/Lead m rT VAB.0001209^^ t Date 3~ PVC BULK TRAILER ANALYSIS iV . \- Particle Size Distribution: Scraan AnalysisWn On Rotap shaker. 4S gms. Resin phis 1.0 gms. Carta Mash Size Gross Wt. 40 __________ 60 80 100 120 140 200 __________ Tara NMwt. HmM __________ o.?o b>Hl lf.JY /STjS' fc Y"> 2.CZ J,U OQ O rl 3(r,~? 3!.*! I *?.f ~,X ^f< 2, Seraan Analysis Min. On Rotap ahaksr 40 gms. Rssin plus 1.0 gms. Carta Ql--y Pam Part. ________ ________ &L1/ _____ /-3 ____ Mash Slza Gross Wt. T-- Nat Wt. H on Mash 40 ____ __ Pan Bm4 100 120 140 200 Remarks \ i Star 207A Havisad 1/12/87 tfm* rnmasai <- 4-- h .t PM VataMynun A Division of Viria Chwnicoi Company Highway 25 Rost Office Box 91 Abardstn, Mississippi 39730 Phono (601) 369-8111 CERTIEX CATION Date: f fO Customer: Athol Manufacturing P.0. Box 105 Butner, NC 27509 Atxention: Tom Baucom. Mgr. Tech. Date of Shipment VEt\ Product : Trailer No.: y~0 &/ P s Lot No,: Order No.: $3S3 Prope Moisture, % Bulk Density, gm/cc Test Method ABR-1A 8.410 Analysis USL. Brabender Dry Time, mins 8.450 Particle Size, % on 40 Mesh 200 Mesh 8. 300 0-00 D an Kesidual VCM, ppm Inherent Viscosity 8.955 8.600 Not more than 8.5 PPM This material was produced to yield an inherent viscosity in the range of -A-JjP to uy . Laboratory/Supervisor/Lead * VAB.000120960j^ PVC BULK TRAILER ANALYSIS iT t p -: -4 Particle Size Distribution: Screen AnalysisMin On Rotap shaker. 49 gme. Resin phis 1.0 gms. Cub Mesh Size 40 00 Gross Wt. Tare ~J Net Wt. % on Mesh o.<ro /-(o go .t Screen AnUysh Min. On Retap shaker 80 100 49 Qms. Resin phis w 120 140 J2gg 1.0 gms. Carta 200 33 Mesh State Gross Wt. Tare p Net Wt. H on Mesh 40 00 80 100 120 140 -_______________________ _________________________ __________ ___________ ______________________ ____________________________________ . __________ _____ __________ s 200 Qtassy Pan Part. Qlaeey Pan Part. Remarks Star 207A Revised 1/12/87 VAB.0001209IP9 x *mm Vista Pdywrs A Division of Vista Chemical Company Highway 25 tost Ofnea Box 91 Aberd--n, Mississippi 39730 Phono (601) 369-8111 LETTER OF CERTX F X OATION Dat.s: Q-i^-tyO Customer: Athol Manufacturing P.0. Box 105 Butner, NC 27509 Produc Trailer Ho. VIS1A Attention: Tom Baucom, Mgr. Tech. Services Lot Mo.: Date of Shipment:*9L//^<d) Order No.: 3/3 gf-3 S'/ Property Moisture, % Bulk Density, gm/c c Test Method AER-1A 8.410 Analysis .69 . 499 <9 1 1 Brabender Dry Time, mins 8.450 Particle Size , % on 8.300 40 Mesh 200 Mesh Pan 0-0 sz /.+ Residual VCM, ppm Inherent Viscosity 8.955 8.600 Not more than 3.t PFM This material was produced to yield an inherent viscosit in the rpQgg 0o1f to Labor ry Supervisor/Lead AVAB.000120961 PVC BULK TRAILS) ANALYSIS Date Customer Technician Product MOIST CON '*11 FRONT 2. 1 2. | i GEL Trailer Time Order BULK DENSITY DRY TIME tr t' _ COLOR vise M2*7 RVCM MIDDLE END i. j* 1 fr * ** B- I Jt ? Particle Size Distribution Scrun Analysis Mash Slza Grass Wt. Tara Nat Wt H on Mash Scrasn Analysis 40 ,6 6 0 O. O mUmln On Rotap ahakar. 4S llaaln plus 1.0 gma. Carb 100 120 140 l 6^ 9*>tr Min. On Rotap ahakar 49 Rosin plus 1.0 gma. Carb GBaasy Pan f*n* 4 <7/ lLh Wt. Tara Nat Wt. H on Mash 40 Pan Part. 100 120 140 200 Remarks. Star 207A Ravlaad 1/12/87 m&mm mmmmmvm Vofci Mymon Attrition of Vbto Chomical Company highway 25 fori Offico Boot 91 l_iJtL mXm -L'LJK OF Abandon Mwiaippi 39730 Phono (601) 369-8111 IFICATION Date: Customer Athol Manufacturing P.0. Box 105 Butner, NC 27509 Product: Trailer No.: Attention: Tom Baucom, Mgr. Tech. Services Lot Ho.: Date of Shipment Order No. : Property Moisture, % Bulk Density, gm/cc Test Method AER-1A 8.410 1 SIS i / Brabender Dry Time, mins 8.450 Particle Size, % on 8.300 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity 8.955 Not more than 8.5 PPM This material was produced to yieia an inherent viscosity in the range of / 0 0___ to LoiL . Laborator Supervisor/Lead VAB.0001209612 Customer Technic! PVC BULK TRAILER ANALYSIS 1 Particle Size Distribution Screen Analysis Mesh Size 40 Wt Tare Net Wt. H on Mesh it0 Screen Analysis Mesh Size Gross Wt. Tars Net Wt H on Mesh 40 Remarks. Min On Rotap shaker. 49 ams. Resin plus 1.0 gms. Carb 80 100 120 140 200 Glassy Pan Part. i .69 h.7 J.L? jJX_ fi.Y c J Al.s- M. 3.1 Min. On Rotap shaker 40 gms. Resin plus 1.0 gms. Carb Pan 80 00 120 140 200 Glassy Part. Star 207A Revised 1/12/87 T 4* r* VAB.0001209' Vista Polymon A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730 Phone (601) 369-8111 LETTER OE CERTIFICATION Date: Customer: // ?> Athol Manufacturing P. 0. Box 105 Butner, NC 27509 VEIA Product: JV//" Trailer Ho. : Attention: Tom Baucom, Mgr. Tech. Service Lot Ho.: Date of Shipment: // S&^jt, Order No. Property Test Method Moisture, % ABR-1A Bulk Density, gm/cc 8.410 Brabender Dry Time, mins 8.450 Particle Siae, % on 8.300 Analysis _ ____.(& _ 1 40 Mesh 200 Mesh ___ & Pan Residual VCM, PPm Inherent Visco sity 8.955 8.600 ___ jjt Not more than 8.5 PPM This material was produced to yield an inherent viscosity in the range of to___ visor/Lead ******* A VAB.0001209614 A Date Customer Technician PVC BULK TRAILER ANALYSIS ______ Product ____________ Trailer Number /~~ ____________ Silo_____& Time & __________________________________________ Order No. ___________ + __________________ Particle Size Distribution: U1Semen Analysis______ Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Cart> Mesh Size 40 60 Gross Wt. Tare Net Wt. % on Mesh 0-aO 0-> Screen Analysis Min. On Rotap shaker 80 100 !?S6 49 gms. Resin plus 120 140 S',? 1.0 gms. Carb 200 5- Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 100 120 140 200 Glassy Psn Part. 0,70 // Glassy Pan Part. Remarks Star 207A Revised 1/12/87 VAB.0001209615 Villa Mymaw ADivmonof VUa Chamical Company Highway 25 ft* Offic* Box 91 Abardomy Mimwippi 39730 Phono(601)369-8111 LETTER OF CERTIFICATION v *" Date: ^ Customer: Attention: Athol Manufacturing P.0. Box 105 Butner, NC 27509 Tom Baucom, Mgr. Tech. Product: Trailer No.: y. Services Lot No. : Date of Shipment: Cj _ ^70 Order No.: 3/3S-3^V Iggt-Msthod Moisture, % ABR-1A Bulk Density, gra/cc 8.410 Brabender Dry Time, mins 8.450 Particle Size, % on 8.300 40 Mesh O.D 200 Mesh Pan /* Residual VCM, ppm 8.955 Not more than 8.5 PPM Inherent Viscosity 8.600 This material was produced to yield an inherent viscosity in the DO to Laboratory Supervisor/Lead VAB.0001209616 A ?-<? -fo Date 7&LCustomer Technician tD/. ~ V PVC BULK TRAILER ANALYSIS Product Silo /oJO Trailer Number Time 0t:oo Order No. Particle Size Distribution: Screen Analysis Mesh Size 40 Gross Wt Tare Net Wt % on Mesh t>. 6 & G*0 Screen Analysis Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 __________ __________ __________ __________ Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carta 60 80 100 120 140 200 Qlassy Pan Part. /&{ /u4- M- Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carta 60 80 100 120 140 200 __________ __________ __________ i L3_ Glassy Pan Part. ____ ____ Remarks. % Star 207A Revised 1/12/87 VAB.000120*9617 m-  0 timu v myvvwi A uivwon Or oki uwoiQQi vOfnpany Highway 25 Pbt Ofnca Box 91 39730 Phoiw (601) 369-8111 LETTER OF CERTIFICATION Date*. $P"~5' "*7 O Customer: Attention: Athol Manufacturing P.0. Box 105 Burner, NC 27509 * Tom Baucom, Mgr. Tech. Date of Shipment: -2_JGr""*7o yisiA Product: Trailer No.: s Lot No.: Order No.: g3)39e~s3 Moisture, % ABR-1A Bulk Density, gm/cc 8.410 Brabender Dry Time, mins 8.450 Particle Size, % on 8.300 40 Mesh 200 Mesh Pan 4 Residual VCM, ppm 8.955 Inherent Viscosity 8.600 0.0 /. O Not more than 8.5 PPM This material was produced to yield an inherent viscosityj^n the range of 0* to . Laboratory Supervisor/Lead " L , VAB.0001209% 18 Date 2S~ - 6 Customer v&wo Technician PVC BULK TRAILER ANALYSIS Product Silo___ Trailer Number. Time Order No. Particle Size Distribution: Screen Analysis Mash Siza Gross Wt. Tare Nat Wt. % on Mash Scraan Analysis 40 Mash Siza Gross Wt. Tara Nat Wt. H on Mash 40 Min On Rotap sihakar. 49 gms. Rasin |plus 1.01jms. Carb 60 80 100 120 140 200 Glassy Pan Part. 2-Z^ A 2/*? 2'0! tfr O A os- Min. On Rotap shakar 49 gms. Rasin plus 1.0 gms. Carb 4 - 60 80 100 120 140 200 a>. /rO Glassy Pan Part. 1' Remarks Star 207A Raviaad 1/12/87 VAB.0001209619 Vtsia folymwn A Division of Vista Chemical Company 25 Box 91 AbsrJisn, Mississippi 39730 Phone {601} 369-8111 LETTER OE CERTIFICATION Dei til;: Customer: 21 flu.f ?& Athol Manufacturing P.0. Box 105 Butr.er, NC 27509 Attention: Tom Baucom, Mgr. Tech. S Date of Shipment: X) ?e> VK1A Product: '3~V/' Trailer No. : 7"^^4^ s Lot No.: Order No. : 3S2- Property Test Method Moisture, % ABR-1A Bulk Density, gm/cc 8.410 Brabender Dry Time, mins 8.450 Particle Size, % on 8.300 40 Mesh 200 Mesh Pan w Residual VCM, ppm 8.955 Not more than 8.5 PPM Inherent Viscosity 8.600 This material was produced to yield an inherent viscosity in the range of J.M____ to__LlPJiL_____ Laboratory pervisor/Lead A VJ&.0001209620 PVC BULK TRAILER ANALYSIS Rate ^ __________ Product Customer A^hoi SiloiHL Time AAf 0 _____________ Trailer Number / _______ Technician__ _________________________________________ Order No. _________________ Particle Size Distribution: Screen Analysis to Mesh Size 40 Gross Wt. Tare 'ff' Net Wt. % on Mesh 0. oo o-o Screen Analysis Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 Min On Rotap shaker. 49 gins. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glaasy Pan Part. .0* . n.io is. n ./ u.f /O.tt ^-syr-/ *,/ Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb - 60 80 100 120 140 200 .Si A/ - * Glassy Pan Part. - Remarks. Star 2Q7A Ravtaad 1/12/87 WiWH WWII T wwm w' -S J L ' fm rn " VAB.0001209621 :------------------------------ mm % Visfci Polymers ADMaion of Vitki Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730 Phone (501) 369-8111 LETTER OE CERTIElCATION * JS rfu**70 Customer: Athol Manufacturing P.0. Box 105 Butner, NC 27509 Product: S/S Trailer No. : Attention: Tom Baucom, Mgr. Tech. Services Lot No. : Date of Shipment: /S' Order No. : &3/3&17~&SZ) Property Moisture, % l3t_Mthod ABR-1A Bulk Density, gm/cc 8.410 Brabender Dry Time, mins 8.450 Particle Size, % on 8.300 40 Mesh 200 Mesh Pan Residual VCM, ppm 8.955 AL u Not more than 8.5 PPM Inherent Viscosity 8.600 This material was produced to yield an inherent viscosity in the range of to Laboratory visor/Lead Star 207A Revised 1/12/87 A r% .A VAB.0001209622 j/ PVC BULK TRAILER ANALYSIS Date Customer FRONT / JfL_JMPl Product Trailer Number Time Order 7" MOIST Top Bottom l. * CON'T. Top Bottom 1. GEL BULK DENSITY W DRY TIME I. COLOR L= vise A= 2. 2., 2. 2. 2. b'OO B-/ ' i. 1. 1. 1. 1. L= RVCM MIDDLE 2. 1 END 2. 2. A= B= i 1. 1 1. L = A= 2. 2. 2. 2. B= Particle Size Distribution: Screen Analysis Min On Rotap shaker. 49 gins. Resin plus 1.0 gms. Carb Mesh Size Gross Wt Tare Net Wt. % on Mesh Screen Analysis 40 0.0 o e.gi? 60 80 100 120 140 200 0, Min. 2jcxZ-> On Rotap shaker /ittf 49 gms. Resin plus 1.0 gms. Carb Mesh Size Gross Wt. 40 60 80 100 120 140 200 V Tare Net Wt. % on Mesh Glassy Pan Part. l Glassy Pan Part. Remarks star 207A Revised 1/12/87 VAB.0001209623 }f  wo Toijrfnon A Division of Viria Owmicol Company rognway 25 FMOfno Ban 91 AbwtUnn, Mmiitippi 39730 Phono (601) 369-6111 LETTER OF CERTIFICATION Date: S ~/9 Customer: Athol Manufacturing P.0. Box 105 Butner, NC 27509 Attention: Tom Baucom, Mgr. Tech of Shipment: g--o g VB1A Product: ^5^X5^-- f ler No. : */=r "2--1/ Lot No.: Order No.: PxoeiX Moisture, % Bulk Density, gm/cc Brabender DryTime, mins Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A 8.410 8.450 8.300 8.955 8.600 Not more than 8.5 PPM This material was produced to yield an inherent viscosity in the range of to / __ . i VAB.0001209624 PVC BULK TRAILER ANALYSIS Date. Customer Technician Product 5V/S 6 ?/ MOIST CON'T. Top l ./5 Bottom | Top Bottom GEL Trailer Number __ Time Order No. BULK DENSITY DRY TIME 1 COLOR l`/co-vo 0J414 vise RVCM FRONT 2. 1 2. 2. = /.^V B 1. 1. I l. L = MIDDLE 2. t. END 2. 2. 2. 2. A= B= 1. 1. 1. 1. L= A= 2. 2. 2. 2. B= Particle Size Distribution: Screen Analysis Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb Mesh Size 40 Gross Wt Tare Net Wt. % on Mesh a-ad d Screen Analysis 60 0^ Min. 80 100 120 140 200 /r-Z-7 rt.p //n<* 3.07 5ft. S Till U'U foZ On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Mesh Size Gross Wt 40 60 80 100 120 140 200 Tare Net Wt % on Mesh Glassy Pan Part. 0 Glassy Pan Part. Remarks Star 207A Revised 1/12/87 &j- *+_ A VAB.00012l096fzt5 j v > .1 HPQ I LNJfMWI A Division of Vww wiotvivooi vomponjr # lI_ M# I 25 Box 91 jlllliiililiiu.iilli.i.lii1! I:l.i Aberdeen, Mississippi Phone (6015 369-8) 51 JLi JH. T T JEJE2 OF CERTIFICATION Date 'Customer: Jt V TJtuJy 70 Athol Manufacturing P.Q. Box 105 Butner, NG 27509 Attention: Tom Baucom, Mgr. Tech. Date of Shipment: & + U*L/y 70 VIS1A Product: jrpj<r Trailer No. : ~7-2J0 s Lot No.: Order No. = K3/3Sj-J7 property Test Methed Moisture, % ABR-1A ____ ./ Bulk Density, gm/cc 8.410 .97 Brabender Dry Time, mins Particle Size, % on 8.450 8.300 _____its * 40 Mesh 200 Mesh Pan ____ ____0 _____ / V Residual VCM, ppm 8.955 Not more than 8.5 Inherent Visco sity 8.600 This material was produced to yield an inherent viscosity in the range of /m00 to 1.0+__ . ervisor/Lead l T NPMIHMB f VAB.00012O0|26 PVC BULK TRAILER ANALYSIS * Date Customer ML c Technician Product Silo___ MOIST CON'T. Top Bottom Top Bottom GEL Wt. /4~ "7 FRONT 2. 2. 2 ' 1. 1. i. Trailer Number Time Order No. X3/2XT- 3 97 BULK DENSITY 2. DRY TIME 1. tf.S 2. COLOR L = M'7 a = Qm0O vise RVCM 1. 1. b L= MIDDLE 2. END 1. 2. r 2. i. 2. 2. 2. 1. 1. 2. 2. 2. 1. 2. A= B= L= A= B= Particle Size Distribution: Screen Analysis Mesh Size Gross Wt. 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. % on Mesh 6. 0 0.0 Screen Analysis Mesh Size Gross Wt. Tare Net Wt % on Mesh 40 3^5" }0.9/ *.3 XLf- L&X llA ^ *71 Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Pan 60 80 100 120 140 200 Glassy Part. Remarks Star 207A Revised 1/12/87 VAB.0001209 VUa Potymera A Division of Vida Chomicd Company Highway 25 Post Omco Box 91 Aberdeen, Mhimippi 39730 Phono (601) 369-8111 LET TER OB' CERT IFICATION * Property Test Me shod Moisture, % ABB-1A Bulk Density, gm/cc 8.410 Brabender Dry Time, mins 8.45- Particle Size, % o n 8.30 0 40 Mesh S. if > 200 Mesh Pan Kesiduai VCM, ppm Inherent Viscosity 8.013 8.600 / <2 Not mo r e t han 8.5 PPM Thi s mate rial was produced to y:Leld an inh erent viscosity in the range of JiQ a to . ' &SL * Laboratory /Supervisor/Lead VAB.000120962A V PVC BULK TRAILER ANALYSIS Date 7-2/ Customer 0 Technician, Product Silo___ L Trailer Number Time Order FRONT MOIST Top | Bottom 1. 2. CON'T. Top Bottom 2, GEL l 2. fc- BULK DENSITY 1. . i-ir 2. DRY TIME 1. 2, l. 1. 1. 1. I. COLOR L =/*>/,// A = 0*0 0 B = /Jo L= vise RVCM MIDDLE 2. A= 2. B- 1 1 1. 1 1. L = END 2. 2. 2. A= B= Particle Size Distribution: Screen Analysis /o_ Mesh Size Gross Wt. Tare Net Wt % on Mesh Screen Analysis 40 0,00 0*9 Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. zoj/ /3*9Z %2t # t* 40tb HA A 93 3.1 Min. On Rotap shaker 49 gms. Resin'plus 1.0 gms. Carb 60 80 100 120 140 200 f,1 Glassy Pan Part. Remarks. mm T Villa Polynwre A Division of m \jnmmiGm wonipony Highway 25 Pc* Office Box 91 AbwtUwi, Mimippi 39730 Phono (601) 369-8111 LETTER OF CERTIFICATION Date: /t iZLL ?0 Customer: Athol Manufacturing P.0. Box 105 Butner, NC 27509 Attention: Tom Baucom. Mgr. Tech. Date of Shipment: Jt Ju, /y 70 Trailer No. : ~FAff rvices r o. t No.: Order No. : %&~~3PS" Too t__Meth .;d Bulk Density, gm/cc AER-1A 8.410 Brabender Dry Time, mins 8.450 i c I e to i 8.300 40 Mesh 200 Mesh Fan Kesidual VCM, ppm Inherent Viscosity 8.600 _____ M-- __ 45. t_ Not mor< than 8.5 PFM This material was produced to yield an inherent viscosity in the range of / 0& to _____ . isor/Lea VAB.0001209 PVC BULK TRAILER ANALYSIS Date Customer Technicia FRONT MIDDLE MOIST |1 CON'T. Top Bottom 1 Top Bottom GEL .... \:%r. '>./<&. '............ 2. 2. 2. 1 1. 1 1 8 2. 2. 1. 2. 1. i. 1. Trailer Number Time Order BULK DENSITY 1. 2. DRY TIME 1. 4.9 2. COLOR J66-7* A= / 1. 1. 2. 2. 1. 1. L= A= B= L= END 2. A= 2. 2. 2. 2. B= vise RVCM OA , /Rd ' Particle Size Distribution: Screen Analysis /> * Mesh Size Gross Wt. Tare Net Wt. % on Mesh Screen Analysis 40 Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. 0.36> D> *7 Min. 60 /*.!$ tV.&D 7.6% Lol <3.43 0.26, dd. 1 // On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Pan 80 100 120 140 200 Glassy Part. Remarks Star 207A Revised 1/12/87 film raiJrinHI AOMaonof Virto Chmicoi Cowpony Hjghfwoy 25 Rbi Oran Box 91 Abiriwn, Miniippi 39730 Phone (601) 369-8111 LETTER OF CERTIFICATION Date: 17 Customer ly lo Athol Manufacturing P.0. Box 105 Sutner. NC 2750tt VBC\ Produc : s-^/r Trailer 1*16, : 7~?-23?" Attention: Tom Baucom, Mgr. Tech. Service Lot No.: Date of Shipment: fy ^l^ly Order No. : 83 !3*t-24+ Property Moisture, % Test Method AER-1A Analysis Bulk Density, gm/cc 8.41C Brabenaer Dry Time, mins 8.450 Particle Size, % on 8.300 40 Mesh 6.0 200 Mesh d an Residual VCM, ppm 8.0 5 5 Mot more than 8.5 PPM Inherent Viscosity 8.800 This material was produced to yield an inherent viscosity in the range of /*oo to /. 4L ratory bupervi .c .4 m VAB.00012096 PVC BULK TRAILER ANALYSIS Date. 7- n - so Product. bY/s Customer A~1y / Silo 6 f f 7~~~___ Trailer Number ?2-\ ______________ Time Olb Technician n<-- Order No. FRONT MOIST CON'T. Top Bottom ToP Bottom 1*1 2. XA/.t. 2. GEL y 2. BULK DENSITY 1. .si o 2. DRY TIME 1. V? 2. * ii fcpj COLOR vise A = 0-P2- B- f.o? 1. 1. 1. 1. 1. L= RVCM MIDDLE 2. 1. END 2. * 2. i. ________ 2. 2. 2. 1. 1. 2. 2. 4**>^ 1. 2. A= B= LA= B= Particle Size Distribution: Screen Analysis Mesh Size 40 Gross Wt. Tare Net Wt. % on Mesh 000 OOP Screen Analysis Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. O./Y } 2.9/ IS.iY 7. )t 2 ? 2.0% 0-3 37 8 30 * /C> * _ !0.s <1.0 Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 o. MJtl Glassy Pan Part. i Remarks Star 207A Revised 1 /12/87 A VAB.0001209633 Visto Polymer* A Division of Vista Chemical Company LET Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730 Phone (601) 369-8111 CERTIElCAT XON Date: Customer: Athol Manufacturing P.0. Box 105 Butner, NC 27509 Product: S/& T v a i I fj r N o, : Attention: Tom Baucom, Mgr. Tech. services Lot No.: Date of Shipment : U ffi Order Mo. : &3/S&3 Moisture, % Test Meth.-d AER-1A Analysis .....JjC. _ Bulk Density, gm/cc 8.410 Brabender Dry Time, mins 8.450 __XJ-- 00 * }Ca aa ;\ t i^ Particle Size, % on 40 Mesh __AIL- 200 Mesh Pan Kesidual VCM, ppm 8 . d55 __3JL. __A3-. Not more than 8.5 PPM Inherent Viscosity W. 600 This material was produced to yield an inherent viscosity in the range of J.fiO__ V' * isor/Lead VAB.0001209634 Date Customer XL /Hha! Technician FRONT MIDDLE END PVC BULK TRAILER ANALYSIS Product Silo___ ,<?/ Trailer Number. 'T-z<neJ Time Q*fOO Order No. COLOR L= t do n | A = 0<o3 B = 1-07 L= vise RVCM A= B= L= A= B= Particle Size Distribution: Screen Analysisf 0_____________ Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb Mesh Size 40 60 80 100 Gross Wt. _________ ______ Tare y Net Wt. % on Mesh _________ ______ 0* * Z) O *& ?/- sfd 43* O Screen Analysis Min. On Rotap shaker 49 gms. Resin plus 120 140 C**?? f #4? 2 1.0 gms. Carb 200 J>Q Mesh Size 40 60 80 100 120 140 200 Gross Wt. _________ _________ ______ Tare _________ ______ Net Wt. _________ _________ ______ % on Mesh _________ Glassy Pan Part. Glassy Pan Part. Remarks____________________________________________________ ________ A VAB.0001209635 Vista fotymon A Division of Vista Chamiool Company Highway 25 Rost Office Bon 91 Abstdssn, Missitsippi 39730 Phono (501) 369-8111 LETTER of certification Date:-? O 1o Customer: Athol Manufacturing P.Q. Box 105 Butner, NC 27509 Product: S^/sT Trailer No. : Attention: Tom Baucom, Mgr. Tech. Services Lot No.: Date of Shipment: 2o T7lr/ ^ Order No. : Property Moisture, % Bulk Density, gm/cc Method AER-1A 8.410 An^iz^is --j____ . ?o(, Brabender Dry Time, mins Particle Size, % on 8.45s 8.300 __ 0_ 40 Mesh Mesh Pan Residual VCM, ppm Inherent Viscosity 8.955 8.600 Mot more than 8.5 PPM This material was produced to yield an inherent viscosity in the range of /oa____ to __J'OV___ . * VAB.0001209636 r PVC BULK TRAILER ANALYSIS Dfltp Z0-?0 Customer Mo Technician_____ TfyM Product Silo___ __________________________________ Trailer Number 7^7/ Time 0 930 Order No. FRONT MOIST CON'T. Top Bottom Top | Bottom GEL BULK DENSITY /r............ . '.1/. 2. 2. lygT ' , f0(e Ztffr 2. 2. DRY TIME 1. rzo 2. COLOR vise RVCM A= r B= A/f r i. 1. ]. 1. 1. L= MIDDLE 2. 1. END 2. 1 *> 1. 2. 2. 2. 1. 1. 2. 2. ...... 11 V 1. 2. A= B= L= A= B= Particle Size Distribution: Screen Analy# sis .. /o Mesh Size Gross Wt. Tare j Net Wt. on Mesh Screen Analysis 40 0 0. 0 Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. A2. AZ Min. ..W Si>.* ST(. f.H C/o /./_____ /?.-? /az ST. 0 On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 .u Glassy Pan Part. Remarks star 207A Revised 1 /12/87 VAB.0001209637 Vhlo Polymers A Division of Vista Chemied Company Highway 25 Post Office Box 91 Aberdeen, Minissippi 39730 Phone (601) 369-8111 LETTER OF CERTIFICATION Date : / ^ *90 Customer: Athol Manufacturing P.0. Box 105 Butner, NC 27509 Product: Trailer No. : Zlti Attention: Tom Baucom, Mgr. Tech. services Lot No.: Date of Shipment: 'fit**- Jo Order No.: fJfliS'1*'0 Pi'ope Moisture, % Test Meth r~t ABR-1A Analysis J2. Bulk Density, gm/cc Brabender Dry Time, mins 8.410 8.450 *2.1. _ f.o Particle Size, %b on 8.300 40 Mesh 200 Mesh o. o z. z T5 an Residual VCM, ppm Inherent Viscosity 8.9 5 5 8.600 Not more than 8.5 PFM This material was produced to yield an inherent viscosity in the range of / && __ to _____________ . oratory Supervi r7Lead VAB.0001209638% Date tf'IO Customer /Mk<\ Technician 1 PVC BULK TRAILER ANALYSIS Product * m Silo___ 6, JO. 7/ Trailer Number Time Order No. '7'-Z 3-T/ Particle Size Distribution: Screen Analysis JLQ- Mesh Size 40 Gross Wt. Tare "f* Net Wt. % on Mesh O.O'O Ao Screen Analysis Mesh Size Gross Wt. Tare Net Wt % on Mesh 40 Min On Rotap shaker. 49 gins. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. * *12 ZO.tf 12.31 2*? r.& fX,C 10.1- J. IQ ^fa, Min. On Rotao shaker 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 ,7T AX Glassy Pan Part. Remarks Star 207A Revised 1/12/87 --------------A VAB.0001209639 Vista foiymnn A Division of Vista ChamicaJ Compony 25 Ban 91 Abord--n, Mississippi 39730 Phono (501) 369-8111 Date: iff " ^ Customer: Athol Manufacturing P.0. Box 105 Butner, NC 27509 Attention: Tom Baucom, Mgr. Tech Date of Shipment: - /d - JO Product: Trailer No. : "7~S75 s Lot No.: Order No. Moisture, % Bulk Density, gm/cc Brabender DryTime, mins Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity ABR-1A 8.410 8.450 8.300 8.955 8.600 Not more than 8.5 PPM This material was produced to yield an inherent viscosity in the range of / to A?r . Laboratory Supervisor/Lead ii VAB.0001209640 PVC BULK TRAILER ANALYSIS Date. (> -/3.- ?0 Customer Technician. Product Silo ^ / 6?/ Trailer Number Order No. FRONT MOIST Top 1| Bottom ' iJ'L 2. CON'T. Top Bottom 1/ 2. GEL 2. B> jH 5 BULK DENSITY DRY TIME 1. 1. '-S76" 4s~ 2. 2. 1. 1. 1. 1. 1. COLOR vise L /t> O-tf'J 1B = / L= r RVCM / MIDDLE 2. u 1. END 2. T 2. i. 2. 2. 2. 1. I. 2. 2. 2. 1. 2. A= B= L= A= B= 1 Particle Size Distribution: Screen Analysis Mesh Size Gross Wt. Tare Net Wt. % on Mesh Screen Analysis 40 Mesh Size Gross Wt. Tare Net Wt. <M> on Mesh 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 i gms. Carb 60 80 100 120 140 200 Glassy Pan Part. - a? _Jo 3*1,0 Itef 7,t 7 4.-2? 3-n 3t>A L be 1 iM Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb .j 60 80 100 120 140 200 09w - --<f-7- d' 0 d Glassy Pan Part. Remarks____ Star 207A Revised 1/12/B7 VAB.0001209641  mo rovyfnwVft^v lYili (Milan, ADMnonof Vkla Chomieal Company AAtO----M- 1M----iVtii?v--M;--Msnp*p- i 39730 Phono (601) 369-8111 LETTER OB' CERT IFI CATION Date: <> **' /2 ~ Customer: Athol Manufacturing P.O. Box 105 Butner, NC 27509 Product: Trailer No.: Attention: Tom Baucom, Mgr. Tech. Services Lot No.: Date of Shipment: C,`/2.'9o Order No. : VIS1A 3*^7 Moisture, % ABR-1A Bulk Density, gm/cc 8.410 Brabender Dry Time, mins 8.450 Particle Size, % on 8.300 40 Mesh 200 Mesh , <25 1 >. o 4- 4 Residual VCM, ppm Inherent Viscosity 8.955 8.600 Not more than 8.5 PPM This material was produced to yield an inherent viscosity in the range, of A to / Laboratory Supervisor/Lead VAB.0001209644 PVC BULK TRAILER ANALYSIS 1 Dale. L -{l-q-D Customer Technician Product (tS Silo 4^0 FRONT MOIST Top Bottom .[as. 2. CON'T. IP.. J| Bottom l'\ s 2. GEL 'JL 2. 1. ]. i. Trailer Number _____ Time Order No. BULK DENSITY 1. -it i * f DRY TIME 1. 2. 2. COLOR L= iooo A= o*c>3 1. 1. B= L= i vise RVCM F7o<-o MIDDLE 2. 1. END 2. T 2. i. 2. 2. 2. 1. 1. 2. 2. 2. 1. 2. A= B= L= A= B- Particle Size Distribution: Screen Analysis_____ L5?Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb Mesh Size 40 60 80 100 Gross Wt. Tare t-- Net Wt. % on Mesh O- cp 23 >6*7 12-Qo | . lo 2S-.1 Screen Analysis Min. On Rotap shaker 49 gms. Resin plus 120 140 200 Bt<40 2-3.0 Q.<a 16.5 1.0 gms. Carb Mesh Size Gross Wt. 40 60 80 100 120 140 200 Tare Net Wt. % on Mesh Glassy Pan Part. 1-2.1 Z.< Glassy Pan Part. Remarks Star 207A Revised 1/12/87 VAB.0001209643 fwu i my11wit AOMrionof VMa Owmicol Company Highway 25 MOrnct Boat 91 Abwdwn, Mmmippi 39730 Phon* {601} 369-8111 LEXTER OF CERTXEICATION Date: Customer: Athol Manufacturing P.0. Box 105 Butner, NC 27509 Product: Trailer No.: Attention: Tom Baucom, Mgr. Tech. Services Lot No.: Date of Shipment: ^ -9o Order No.:: $3 f3 2 ?-33 Property Moisture, % Zsafc. Method ABR-1A Analysis ,/D Bulk Density, gm/cc 8.410 --Lt 6 Brabender Dry Time, mins m Particle Size, % on 8.450 8.300 40 Mesh OD 200 Mesh Pan L Residual VCM, ppm 8.955 Not more than 8.5 PPM Inherent Viscosity 8.600 This material was produced to yield an inherent viscosity in the range of /. 6 6 to__ ho __ . upervisor/Lead AVAB.000120964 PVC BULK TRAILER ANALYSIS Date Co Customer Technician FRONT 4s~Product ir Silo___ MOIST CON'T. Top Bottom | Top Bottom ,'7.o 1. / Y 2. 2. GEL I 2. 1. i i Trailer Number Time Order No. Sf ? /3 {P ?? BULK DENSITY I. A3 2. DRY TIME 1 2. COLOR L = !tt>. Jo a = o-o4 B - A// i i. L = ^ vise RVM ?/ MIDDLE 1 END 2. 2. 2. A= B= l. 1 I. 1 L= A= 2. 2. 2. 2. B= Particle Size Distribution: Screen Analysis Mesh Size 40 Gross Wt. Tare Net Wt. % on Mesh O < OO Screen Analysis Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 Min On Rotap silaker. 49 j]ms. Resin |slus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. f. .L Min. 60 lUr 77/ jr.lf Jt-Ll14-11 fT -------- r----------- JLJ <??.r /r.4 tf.L 4.1 On Rbtap shaker 49 gms. Resin plus 1.0 gms. Carb 80 100 120 140 200 M3 Lt- Glassy Pan Part. Remarks Star 207A Revised 1 /12/87 * VAB.0001209645 A Vista Fblymen A Division of Vista OiMmoal Company Highway 25 Past Ofnca Bok 91 Abard--n, Mississippi 39730 Phona (601) 369-8111 LETTER OF CERTIFIOATION Date: Customer: Athol Manufacturing P.0. Box 105 Butner, NC 27509 Attention: Tom Baucom, Mgr. Tech. Date of Shipment: ~ Lot No.: Order No. : ff3f-3& Property Moisture, % ABR-1A Bulk Density, gm/cc 8.410 Brabender Dry Time, mins 8.450 Particle Size, % on 8.300 40 Mesh 200 Mesh Pan Residual VCM, ppm 8.955 Inherent Viscosity 8.600 <9-0 <12. 2. Z. Not more than 8.5 PPM This material was produced to yield an inherent viscosity in the range of A && to /.Q+- . Laboratory Supervisor/Lead I MMPN f VAB.00012096 f a PVC BULK TRAILER ANALYSIS Date Customer Technicia fj/ f ~ -- Product Silo^_ Trailer Number Time oo Order No. FRONT MOIST CON'T. Top Bottom Top Bottom Ilf?,. 'C // 2. n 2. GEL DEBNUSLITKY 1. gL, . -S7<? 2. DRY TIME 1. 2. i. 1. i. 1. 1. t~vrCOLOR vise RVCM A =0&UI B L- a> MIDDLE 2. 1. r 1. 2. 2. 1. 1. 2. i. A- B= L= END 2. A= 2. 2. 2. 2. B= Particle Size Distribution: Screen Analysis Mesh Size Gross Wt. Tare Net Wt % on Mesh Screen Analysis 40 Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. /.^3 fLSl 10 Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Pan 60 80 100 120 140 200 Glassy Part. Remarks Star 207A Revised 1/12/87 k A VAB.00012096-47^ tmh nxynwn M OfA nLALM X VMoOwmicd Conpony highway 25 Ant OMn Box 91 Ahirdiw, Mmmmppi 39730 Pfiom (601) 369-8111 Date: Customer: Athol Manufacturlng P.0. Box 105 Butner, NC 27509 Attention: Tom Baucom, Mgr. Tech. 6> -s'- 9oDate of Shipment: s Lot No.: - Order No.: Moisture, % ABR-1A Bulk Density, gm/cc 8.410 Brabender Dry Time, mins 8.450 Particle Size, % on 8.300 40 Mesh 200 Mesh Pan Residual VCM, ppm 8.955 Inherent Viscosity 8.600 ). >Q 4-6 3.0 Not more than 8.5 PPM This material was produced to yield an inherent viscosity in the rayge^of A *4 r - VAB.00012096 t uai ATMustomer PVC BULK TRAILER ANALYSIS Particle Size Distribution: Screen Analysis Mesh Size Gross Wt. Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. % on Mesh Screen Analysis Mesh Size Gross Wt. Tare Net Wt. % on Mesh <f-3 Wt S<Lgo 37& awt 9# w &Qi 3.0 ____ Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 Pan 200 Glassy Part. Remarks Star 207A Revised 1 /12/87 VAB.00012096 VbfaMywin AOMonof VMa Chemical Company Highway 25 feet Offica Box 91 Abrd>n, Mwmtippi 39730 Phon* (601) 369-8111 LETTER OE CERTIFICATION Date: Customer: 3 <?p Athol Manufacturing P.0. Box 105 Butner, NC 27509 VKIA Product: W5 Trailer No.: jz Attention: Tom Baucom, Mgr. Tech. Services Lot No.: Date of Shipment: -7 Order No.: Property Test Method Moisture, % Bulk Density, gm/cc ABR-1A 8.410 >-5~7J5 Brabender Dry Time, mins 8.450 Size, % on 8.300 40 Mesh O, OD 200 Mesh Pan Residual VCM, ppm 8.955 2*1 Not more than 8.5 PPM Inherent Viscosity 8.600 This material was produced to yield an inherent viscosity in the range of A0C to Laboratory OJupervisor/Lead *r M VAB.0001209^|) PVC BULK TRAILER ANALYSIS Date 6 -z? - r d Customer Technician Product Silo L 7 0 /LJL. MOIST | CONT. Top Bottom Top Bottom 1.< Z> 1 Jl GEL FRONT 2. 2. 1. 1 1. Trailer Number. __ Time________ /P/ Order No. ^T/.T 6^ ?3 3 BULK DENSITY DRY TIME COLOR T vise 1. 1. L = /^fc.7*] 41 A = 0.0$ 1. l. B- L= MIDDLE 2. 1. END 2. 2. 2. 2. A= B= 1. 1. 1. .1 L= A= 2. 2. B= Particle Size Distribution: Screen AnalysisMin On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb Mesh Size 40 60 80 100 120 140 200 Glassy Pan Part. Gross Wt. Tare Net Wt. % on Mesh 0*0 .o 12.713 //. H* 7,17 /* 3 $<3 21. S' s.os' i-i US' " - /rO r A -l 7 ----------------- --------------------------------------------------------------------------------------- p--1 Screen Analysis Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Mesh Size .fc- 40 60 80 100 120 140 Pan 200 Glassy Part. Gross Wt. _________ Tare _________ _________ Net Wt. _________ ____ % on Mesh _________ _________ Remarks S3! I VAB.0001209651 Vi*k* Polymers A Division of Voki ChwnicoJ Company Highway 25 FostOfnc Box 91 Abord--a Mississippi 39730 Phono (601) 369-8111 Date 9O Customer: Athol Manufacturing P.0. Box 105 Butner, NC 27509 Attention: Tom Baucom, Mgr. Tech. Date of Shipment: ~ yisiA Product -JST^S Trailer No.: Lot No.: Order No. : 3/33^2, Test Methcd Moisture, % AER-1A Bulk Density, gm/cc Brabender Dry Time, mins 8.410 8.450 . /O 4.V Particle Size, % on 8.300 40 Mesh 200 Mesh jT-^2. Pan Residual VCM, ppm 8.355 Not more than 8.5 PPM Inherent Viscosity 8.600 This material was produced to yield an inherent viscosity in the r^ng|^ of Laboratory Supervisor/Lead 4 *K VAB.0001209652 \ .i \ PVC BULK TRAILER ANALYSIS 1 Date 3 /S-9Z> Customer Th O Product Silo___ 3 /S C'7/ 75?Trailer Number. __ Time_________ Technician FRONT Order No. MOIST CON'T. Top Bottom Top Bottom GEL DEBNUSLITKY TDIMREY . \(l.. Ao 1 A. 'V 'W to , 2. 2. 2. 2. 2. 1. 1. 1. 1. 1. 3; II COLOR vise A = 0-C& B = > L= RVM Cloy MIDDLE 2. 1. END 2. *> A = n 2. 2. 2. B= 1. 1. 1. 1. L = A= 2. 2. 2. 2. B= . Particle Size Distribution: Screen Analysis Min On Rotap shaker. 49 gms. Resin plus 1.0 gifts. Carb Mesh Size 40 Gross Wt. Tare Net Wt. O coO % on Mesh Screen Analysis 60 80 100 120 140 200 V7.7# !2-. 79 %33 J1___ ? 17- C JZJ S~A Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Mesh Size Gross Wt. 40 60 80 100 120 140 200 Tare Net Wt % on Mesh Glassy Pan Part. Glassy Pan Part. Remarks Star 207A Revised 1/12/87 Viski Polymers A Oivinon of Vbta Chamtcd Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730 Phone (601) 369-8111 LETTER OE CERTIFICATION Date: jf-ZS'-f O Customer: Athol Manufacturing P.0. Box 105 Butner, NC 27509 Product: Trailer No.: / Attention: Tom Baucom, Mgr. Tech. Services Lot No. : Date of Shipment: Order No. : #J/J ? s7 -12/ Moisture, % ABR-1A Bulk Density, gm/cc 8.410 Brabender Dry Time, mins 8.450 Particle Size, % on 8.300 40 Mesh 200 Mesh Pan Residual VCM, ppm 8.955 Inherent Viscosity 8.600 Not more than 8.5 PPM This material was produced to yield an inherent viscosity in the r^nge of / && to /.. &. Labor ry Supervisor/Lead VAB.000120n>54 PVC BULK TRAILER ANALYSIS Date Customer Technician Product. Silo___ ifo Trailer Number '7' 7. (/If O Time 0(,3 0 Order No. FRONT MOIST Top Bottom \lt\ t # * CON'T. Top Bottom 1. ****** 2. 2. GEL -rm BULK DENSITY 1. ,rz/ 2. DRY TIME 1. +1 2. I. 1. 1 1. I. COLOR L = Jot\ <n A =J-.of vise B = / OO L= RVCM MIDDLE 2. END 1. 2. 2. 2. A= B= 1. 1I 1 L= A= 2. 2. 2. 2. B= Particle Size Distribution Screen Analysis /0 Mesh Size Gross Wt. Tare rT' / Net Wt. % on Mesh Screen Analysis 40 OiO Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. / jr? J,Z Min. MJ7 /2*67~ 2. 2T 31.7 zr. ^ n.( tr %7 On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 ,/? At Glassy Pan Part. w Remarks t Star 207A Revised 1 /12/87 ---------------- 1 VAB.0001209^5 Vista. Pc/ym*n A Division of Vista Chtnical Company Highway 25 Rost Office Box 91 Aberdeen, Mississippi 39730 Phone (601) 369-8111 LETTER OF CERT I F I CJAT X ON Date: V Customer: Athol Manufacturing P.0. Box 105 Butner, NC 27509 Product: Trailer No.: Attention: Tom Baucom, Mgr. Tech. Services Lot No.: Date of Shipment: j 2*.-" O/> Order No.: Moisture, % Test Method ABR-1A 10 Bulk Density, gm/cc 8.410 Brabender Dry Time, mins Particle Size, % on 8.450 8.300 40 Mesh 200 Mesh i.,9 Pan Residual VCM, ppm 8.955 Not more than 8.5 PPM Inherent Viscosity 8.600 This material was produced to yield an inherent viscosity in the range of to Laboratory f , VAB.00012096 V Date 6 -/a- ? Customer 7un-,,, Technician n5l PVC BULK TRAILER ANALYSIS Product Silo^ . ry<r Trailer Number / Time /^ Particle Size Distribution: Screen AnalysisMin On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb Mesh Size 40 Gross Wt. Tare Net Wt. d >'oO % on Mesh Screen Analysis 60 1 AV A-i" Min. 80 100 120 140 200 J3.$l /? S& C-rll 3,13 i,1/(- 41C 7jT A.1 On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Mesh Size Gross Wt. 40 60 80 100 120 140 200 Tare Net Wt. % on Mesh Glassy Pan Part. o.n At Glassy Pan Part. Remarks____ Star 207A Revised 1/12/87 VAB.0001209 tbpd iviynicri A Division of vmaWm&A ^uLitnaAvhCujumiI ^^cjxunhupuaunuy# Highway 25 PostOmcoBox91 Abord--n, Mississippi 39730 Phono (601) 369-8111 LETTER OE CERTIEX CATION Date: ^ 9& Customer: Athol Manufacturing P.0. Box 105 Butner, NC 27509 Attention: Tom Baucom, Mgr. Tech. Services Lot No.: Date of Shipment: ^ 7* Order No.: Property Moisture, % Test Method ABR-1A U. o Bulk Density, gm/cc Brabender Dry Time, mins 8.410 8.450 */ Particle Size, % on 40 Mesh 200 Mesh 8.300 0> O 4,0 Pan Residual VCM, ppm 8.955 Not more than 8.5 PPM Inherent Viscosity 8.600 This material was produced to yield an inherent viscosity in the range of / 00 to /, . or/Lead VAB.0001209658 PVC BULK TRAILER ANALYSIS 0 Date J5 ~~ *7 ~ J &___ Product Customer Technician _________ Silo ~TT. Order No. ______ Trailer Number ______________________ Time O ~/~ Z7 Particle Size Distribution: Screen Analysis Mesh Size 40 Gross Wt. Tare Net Wt. % on Mesh /?.oo oo Screen Analysis Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 Min On Rotap srlaker. 49 |ms. Resin [)lus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. CP-ZS' l^o IMS 9.H tPS' 34 U 30* 12.3 Y*s i*1 0*0 9.9 4.0 1/2 Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Pan 60 80 100 120 140 200 Glassy Part. Remarks. Star 207A Revised 1/12/87 1^ ^ - KflHMMW r pMrtUHVPBI Af VAB.OOO1209659 wm Vhlo M^idm ADMaionof VMo OiMMoal Company Atonal--n, Miuwippi 39730 Phono (601) 3694111 LETTER OB' CERTIFICATION Date: .5-(* - VISP Customer: Athol Manufacturing P.0. Box 105 Butner, NC 27509 Attention: Tom Baucom, Mgr. Tech. Date of Shipment: Product: Cfl5~ Trailer No. :75~ s Lot No.: Order No.: Moisture, % Bulk Density, gm/cc ABR-1A b> 8.410 Brabender Dry Time, mins 8.450 Particle Size, % on 8.300 40 Mesh 200 Mesh Pan Residual VCM, ppm 8.955 Inherent Viscosity 8.600 Not more than 8.5 PPM This material was produced to yield an inherent viscosity in the .range of to 1*0*4 Laboratory Supervisor/Lead VAB.000120960(7*' PVC BULK TRAILER ANALYSIS Customer 90 Art/oi Product Silo___ Trailer Number Time Technicia Order No. N /nru FRONT MOIST Top Bottom 1 ^ # I * 4 I * t 2. CONT. Top Bottom 2. GEL BULK DENSITY l 497 '/& 2. 2. DRY TIME 1. 4~9 2. 1. I 11 i COLOR L= 1 A =Q%&Z B = 0-28 L= vise RVCM o AC MIDDLE 2. 1 END 2. 1. 2. 2. 2. 1. I 2. 2. 2. 1 A= B L= A= B= Particle Size Distribution: Screen Analysis /O Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb Mesh Size 40 Gross Wt. Tare Net Wt. % on Mesh to-OO o.o Screen Analysis 60 80 100 120 140 200 0,7 Z 6S( 3./S /.4- 47,t> 22./ /3.0 3 21 Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Mesh Size Gross Wt. 40 60 80 100 120 140 200 Tare Net Wt. % on Mesh Glassy Pan Part. o. 7<r /*S Glassy Pan Part. Remarks. Star 207A Revised 1/12/67 T* P WWMH m -- ' i I'F"*................................. VAB.00012096 wu i my11101 > A Division of Viski Chomioal Company Highway 25 Post Office Box 91 Abordoon, Mississippi 39730 Phone {601) 369-8111 LETTER OF CERTIFICATION Date*. / fljAy W Customer: Athol Manufacturing P.0. Box 105 Butner, NC 27509 Product: Trailer No. : T~ 2-4f I Attention: Tom Baucom, Mgr. Tech. Services Lot No.: Date of Shipment:/* /T)aj JO Order No.: fr3/3iS''SZF Property TestMethod Analysis Moisture, % ABR-1A ___ //_ Bulk Density, gm/cc 8.410 _ Brabender Dry Time, mins 8.450 SZO__ Particle Size, % on 8.300 40 Mesh 200 Mesh / /__ Pan Residual VCM, ppm 8.955 Not more than 8.5 PPM Inherent Viscosity 8.600 This material was produced to yield an inherent viscosity in the range of A Jo PVC BULK TRAILER ANALYSIS Date 7'^ Product Customer Technician MTL- MOIST Top Bottom 1. ,// CON'T. Top Bottom GEL l FRONT 2. 2. 2. I. 1. 1 BULK DENSITY 1. 2. 1. Trailer Number Time ^2/04> DRY TIME 1 2. 1. COLOR vise L = /to-7P A= B = /e>3 L= RVCM MIDDLE 2. 1 2. 2. 2. A= B I. 1 I. 1 END 2. 2. 2. 2. A= B= Particle Size Distribution: Screen Analysis____ fQ Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb Mesh Size 40 60 80 100 120 140 200 Glassy Pan Part. Gross Wt. Tare Net Wt. % on Mesh 0-0 o a 20 /&S5 74* 1 ZD 0.%> O*O 4L2 33-f /. 3 /.% /.z- Screen Analysis Mesh Size Gross Wt. 40 Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Pan Glassy Part. Tare Net Wt. % on Mesh Remarks Star 207A Revised 1/12/87 W ----------- A VAB.0001209663 Vista fotymcrs A Division of Vista Chemical Company Highway 25 Pbst Office Box 91 Aberdeen, Mississippi 39730 Phono (601) 369-8111 LETTER OE CERTIEXCATION Dat e: U^.r Customer: Athol Manufacturing P.0. Box 105 Butner, NC 27509 Attention: Tom Baucom, Mgr. Tech. Date of Shipment: Trailer No. Lot No.: Order mt f Property Test--Method Analysis Moisture, % ABR-1A Bulk Density, gm/cc 8.410 Brabender Dry Time, mins 8.450 Particle Size, % on 8.300 40 Mesh 200 Mesh Pan Residual VCM, PPm 8.955 Not more than 8. PPM Inherent Viscosity 8.600 This material was produced to yield an inherent viscosity in the ranffe of /& to ' -9/ ^ tJ&Trux&lt OM Laboratory Supervisor/Lead > A VAB.0001209664 I PVC BULK TRAILER ANALYSIS Date Customer Product 6&t Technician MOIST Top Bottom CON'T. Bottom GEL :,iz. # FRONT 2. / l. i. l. Trailer Number _ Time 1/9- Order No. BULK DENSITY 1 2. DRY TIME I. fb7 2. COLOR L =fC 0- A - A&S" i. i. B L= vise RVCM MIDDLE 1 END 2. 2. 2. 2. A= B= I 1. 1. I. L= A= 2. 2. 2. 2. B= Particle Size Distribution: Screen Analysis Mesh Size Gross Wt. 40 Min On Rotap shaker. 49 gms. Resin plus i .u gms 60 80 100 120 140 200 Glassy Pan Part. 0.00 % on Mesh 0.0 Screen Analysis Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 AX8 #<76? fetf 263 (7 /7A d A1 ___Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Pan 60 80 100 120 140 200 Glassy Part. Remarks Star 207A Revised 1/12/87 Thu, ,J- VAB.0001209C65 Virtu Mywmn ADMiionoi VMo Owimcal Company Highway 25 Rost Ofhc* Box 91 Absrd--n, Miwwiippi 39730 Phono (501) 369-alll Date: *H7-9 Customer: Athol Manufacturing P.0. Box 105 Butner, NC 27509 Attention: Tom Baucom, Mgr. Tech Date of Shipment: VBlA Product Trailer Ho. .-izgfJTl s Lot Ho.: Order No. : Moisture, % Bulk Density, gm/cc Test Method ABR-1A 8.410 -A? 0. Brabender Dry Time, mins 8.450 Particle Size, % on 8. 300 40 Mesh 200 Mesh Pan Residual VCM, ppm 8.955 Not more than 8. PPM Inherent Viscosity 8.600 This material was produced to yield an inherent viscosity in the ran<9 of L ^ to * Laboratory Supervisor/Lead A** A VAB.0001209666 h PVC BULK TRAILER ANALYSIS Top FRONT 2. Bottom Top I 2. Bottom GEL / BULK DENSITY I. DRY TIME l. M 2. 1. 1. ] 1. 1. MIDDLE 2. 2. 2. I I 1 1. I END 2. 2. 2. 2. COLOR Lyv A= B= L= A= B= L= A= B= vise RVCM Particle Size Distribution: Screen Analysis Mesh Size 40 Gross Wt. Tare'll Net Wt. % on Mesh 0. 0 & G.> Screen Analysis Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 h Min On Rotap sttaker. 49 jjms. Resin ptius 1.0 g ims. Carb 60 80 100 120 140 200 Glassy Pan Part. /aSX / Min. 60 fftz- <ff.a MifL On Rotao shaker 49 ams. Resin olus P M* 3LV- 1.0 ams. Carb 80 100 120 140 200 / Pan Glassy Part. 1 Remarks Star 207A Revised 1/12/87 f A VAB.0001209667 Yww rwynm ADMmqroF \wA*4oa mMCOi uomponyjutaukjH|4j Highway 25 Rod Offic* Box 91 Phona (501) 369-8111 LETTER OE CERTIFICATION Date: VGA . * * Customer: Athol Manufacturing P.0. Box 105 Butner, NC 27509 Product: Trailer No. : 'mp=-m2~ftyQ Attention: Tom Baucom, Mgr. Tech. Services Lot No.: Date of Shipment: /L --/If Order No.: $Jj ~ 32.4- Moisture, % ABR-1A Bulk Density, gm/cc 8.410 Brabender Dry Time, mins 8.450 Particle Size, % on 8.300 40 Mesh 200 Mesh Pan Residual VCM, ppm * Inherent Viscosity 8.955 8.600 3.0 _____ L.1/L.. Not more than 8.5 PPM This material was produced to yield an inherent viscosity in the range of to Laboratory ervisor/Lead mI VAB.0001209018 h ** PVC BULK TRAILER ANALYSIS Date Customer Technician FRONT Product Trailer Number Time________ 4 Order MOIST Top Bottom 6 (p 2. CON'T. Top Bottom I/.. n2. GEL BULK DENSITY 1 // 1. ..53/ 2. 2. DRY TIME I. 2. COLOR A= B = $-79 1. 1. 1. 1. 1. L= vise RVCfcf / MIDDLE 2. 1. END 2. * 2. i. 2. 2. 2. 1. 1. 2. 2. 2. i. 2. A= B= L= A= B= i Particle Size Distribution: Screen Analysis Min On Rotap sihaker. 49;gms. Resin |lus 1.0 gims. Carb Glassy Pan Part. Mesh Size 40 60 80 100 120 140 200 Gross Wt. Tare Net Wt. % on Mesh 0 `P 0 -2J.2-7 9<0D o,7 H 2,ag isrf. 7.^ Screen Analysis Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb J. Mesh Size 40 60 80 100 120 140 200 0-6 J- -M-- Glassy Pan Part. Gross Wt. _________ _________ Tare _________ _________ Net Wt. _________ _________ % on Mesh _________ _________ Remarks Star 207A Revised 1 /12/87 VAB.0001209669 Vista RoJymvra A Division of Vista Chemical Company Highway 25 toft Ofnc* Box 91 Aborttaw, Mississippi 39730 Phons (601) 369*8111 Date: Customer: Athol Manufacturing P.O. Box 105 Butner, NC 27509 Product: Trailer No. : pp ? Attention: Tom Baucom, Mgr. Tech. Services Lot No. : 4-Date of Shipment: tl-'VO Order No. : g3/3f?-323 Rraeartz Teat Method Moisture, % AER-1A Bulk Density, gm/cc 8.410 Brabender Dry Time, mins 8.450 Particle Size, % on 8.300 40 Mesh 200 Mesh O <0 Pan Residual VCM, ppm 8.955 Not more than 8.5 PPM Inherent Viscosity 8.600 This material was produced to yield an inherent viscosity in the range of X &Q to . 4i. . + A VAB.0001209670 PVC BULK. TRAILER ANALYSIS Date Customer Technician ft FRONT Product Silo tni 0 t-L k3-L Trailer Number Time / 0 Order No. T '75_3 MOIST Top Bottom CON'T. Top | Bottom ':y.. GEL BULK DENSITY ___ I____ *___ 2. 2. 2. /LH 2. DRY TIME 1. 2. COLOR L= jdojsif- A= vise ' /.or 1. i. i. 1. 1. L= RVCWAu) MIDDLE 2. END 1. 2. r i. 2. 2. 2. 1. 1. 2. 2. 1. 2. A= B= L= A= B= Particle Size Distribution: Screen Analysis Mesh Size 40 Gross Wt. Tare Net Wt. % on Mesh J9 Q.t 0 Screen Analysis Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 Min On Rotap siInker. 49 gms. Resin |plus 1.0 gims. Carb 60 80 100 120 140 200 Glassy Pan Part. * r* >0 MiQd JJ?t UP Jr Os**?t* STO Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 a __ Lb__ Glassy Pan Part. Remarks Star 207A Revised 1/12/87 A Jlkg A A Division of Vista Chemical Company 25 Post Office Box 91 Aberdeen, Mississippi 39730 Phone (601) 369-8111 LETTER OB' CERT IFI CATION Date: /# Customer: Athol Manufacturing P.0. Box 105 Butner, NC 27509 Product 3V/S' Trailer No. : '7*2337 Attention: Tom Baucom, Mgr. Tech. Services Lot No.: Date of Shipment: /$ for. ?> Order No. : Property Ti_Uthod Analysis Moisture, % ABR-1A Bulk Density, gm/cc 8.410 Brabender Dry Time, mins 8.450 ____*,r Particle Size, % on 8.300 40 Mesh ____A& 200 Mesh Pan Residual VCM, ppm 8.055 ____3J LJcl________________ _______________ Not more than 8. Inherent Viscosity 8.600 This material wa produced to yield an inherent viscosity in the range of to__ JtQ*t__ . VAB.0001209^|2 DateJH*^ ZMCustomer o Technician. PVC BULK TRAILER ANALYSIS Product Silo___ Trailer Number 9/ Time Order No. Particle Size Distribution: Screen Analysis Mesh Size Gross Wt. rTare Net Wt. % on Mesh Screen Analysis 40 on Mesh Size Gross Wt. Tare Net Wt % on Mesh 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 &2g t?.' 3A m sj Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. & Glassy Pan Part. Remarks Star 207A Revised 1/12/87 t ~~ * VAB.000120^7 * VtoMyinm A Division of Vteki Chomicol Compony Highway 25 FWOffieiBox91 Abordoon, Miwhrippi 39730 Phone (601) 369-8111 LETTER OF CERTIFICATION Dat e: i 7 MaTC^- Customer: Attention: Athol Manufacturing P.0. Box 105 Butner, NC 27509 * Tom Baucom, Mgr. Tech. Product: SV/lT Trailer No.: Services Lot No.: Date of Shipment: Z"? Order No.: Property; Te5t Method Analysis Moisture, % Bulk Density, gra/cc AER-1A 8.410 __ * //v __V Brabender Dry Time, mins 8.450 ____ Particle Size, % on 8.300 40 Mesh ___ 0* 0____ 200 Mesh 43_____ Pan 7 Residual VCM, ppm 8.955 Not more than 8.5 PPM Inherent Viscosity 8.600 This material was produced to yield an inherent viscosity in the range of Aoo to ___________- ~e6 oratory Supe?vissor/Lead VAB.000120 1 Date Customer /kid Technician PVC BULK TRAILER ANALYSIS Product Silo___ 5>/l Trailer Number Time /03o Order No. Particle Size Distribution Screen Analysis L Mesh Size 40 Gross Wt. Tare / Net Wt. % on Mesh &0O 0,0 Screen Analysis Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. 0.47 /S3S. 0$ 3k. (o l. I ix.q S'. aid & 4,3 in Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Pan 60 80 100 120 140 200 Glassy Part. Remarks Star 207A Revised 1/12/87 VAB.0001209^ VtoaMymtn A OMiion of Vida Chamicai Company Highway 25 fast Office Bax 91 Abardoan, Mbstuippi 39730 Phono (601) 369-8111 Date : 3- 3 ^ ^ Customer: Athol Manufacturing P.0. Box 105 Butner, NC 27509 Attention: Tom Baucom, Mgr. Tech. Date of Shipment: Product: s Trailer No. : ~p- 72 2_ s Lot No.: Order No. = S3/3U~3-z-o Property Moisture, % ABR-1A Bulk Density, gm/cc 8.410 Brabender Dry Time, mins 8.450 Particle Size, % on 8.300 40 Mesh 200 Mesh Pan Residual VCM, ppm 8.955 Inherent Viscosity 8.600 0,0 J.JL A3 Not more than 8.5 PPM This material was produced to yield an inherent viscosity in the range of A 0 0____ to // P V__ . Laboratory Supervisor/Lead VAB.0001209671 Date ..? Customer Technician PVC BULK TRAILER ANALYSIS O Product _ sii &?(>'/-9/ Trailer Number Time c?/s- Order No. Z, Particle Size Distribution: Screen Analysis Mesh Size 40 Gross Wt. Tare Net Wt. % on Mesh o* Screen Analysis Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 Remarks 0 % 0 Min On Rotap shaker. 49 gins. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. HI .2 /3.gr 7-9-TJ.t// /-Sf . (J~ 3 27,7 m.q # 3,2. h3 Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Pan 60 80 100 120 140 200 Glassy Part. f Star 207A Revised 1 /12/87 VAB.0001209677 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Bax 91 Aberdeen, Mississippi 39730 Phone (601) 369-8111 LETTER OF CERTIFICATION Date: Z/ 70 Customer: * Athol Manufacturing P.0. Box 105 Butner, NC 27509 Product: S/$~ Trailer No. : Attention: Tom Baucom, Mgr. Tech. Services Lot No. : Date of Shipment: X! Order No. : T3/3& Te3t Method Analysis Moisture, % ABR-1A ____,/r Bulk Density, gm/cc 8.410 ____ lSM- Brabender Dry Time, mins Particle Size, % on 8.450 8.300 ____ 3-- 40 Mesh ___ M - 200 Mesh Pan ___ ^4.SL._ /^ Residual VCM, ppm 8.955 Not more than 8.5 PPM Inherent Viscosity 8.600 This material was produced to yield an inherent viscosity in the range of 100 __ to 1,0*4.__ . rvisor/Lead % VAB.00012096^ 'M Customer Technlcia PVC BULK TRAILER ANALYSIS Particle Size Distribution: Screen Analysis Mesh Size 40 Gross Wt. Tare 'f' Net Wt. % on Mesh Q.OO >. 0 Screen Analysis Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. &.2J0 /f.e? /S. 6S g.9( 3& / J/.3 /f.O /. ^ 2$ fi.SZ Min. On Rotao shaker 49 ams. Resin olus 1.0 oms. Carb Pan 60 80 100 120 140 200 Glassy Part. Remarks Star 207A Revised 1/12/87 ________ A VAB.0001209679 *> mo rovyvners A Division erf Vista Chemical Company Kfighway 25 FMOfncs Box 91 Aberdeen, Mississippi 39730 Phone (60T) 369-8111 LETTER OB' CERTIFICATION Date * // rtAT&b- & Customer: At-hol Manufacturing P.0. Box 105 Butner, NC 27509 Attention: Tom Baucom, Mgr. Tech. Date of Shipment: /? Product: w Trailer No. : 7- -2J-TV Lot No.: Ord No. ?rQ%Z Test Method Moisture, % ABR-1A Bulk Density, gm/cc Brabender Dry Time, mins 8.410 8.450 sr.o Particle Size, % on 8.300 40 Mesh 200 Mesh Pan Residual VCM, ppm 8.955 Not more than 8.5 PPM Inherent Viscosity 8.600 This material was produced to yield an inherent viscosity in the range of A oO__ to / oV__ . oratory Supe /Lead rrt /. VAB.0001209680 PVC BULK TRAILER ANALYSIS Date 3-/3'?* Customer Technician FRONT Product Silo___ ifo MOIST Top [ Bottom /0 CON'T. Top | Bottom '2-A............. GEL 2. 2. 2. 1. 1. 1. Trailer Number Time 23J Order No $3/3^3/% BULK DENSITY 1. DRY TIME COLOR L yoa.fS vise RVCM 'V 2. 2. 1. 1. A=*r *7 . B = -+* L= * MIDDLE 2. 1. END 2. f 2. 1. 2. 2. 2. 1. 1. 2. 2. 2. 1. 2. A= B= L= A= B= Particle Size Distribution: Screen Analysis /*Min Mesh Size 40 Gross Wt. Tare Net Wt. % on Mesh 0*00 0.p Screen Analysis Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 On Rotap shaker. 49 gms. Resin plus 60 80 100 120 1.0 gms. Carb 140 200 Glassy Pan Part. /.A Min. 60 22*/O /?. 7/ 44,2* 27. <* 7.tr J. it A Si. 7. 2- 3* 0 On Rotao shaker 49 ams. Resin olus 1.0 ams. Carb 80 100 120 140 200 ,/3 y7 Glassy Pan Part. Remarks Star 207A Revised 1/12/87 ________ A VAB.0001209681 Si Vista folymnn A Division of Vista Choimcal Compony Hfehwoy 25 Post Often Box 91 Abfd--n, Miiriiiippi 39730 Phono (601) 359-8111 LETTER OF CERTIFICATION Date : --I 1? ~ *7 0 Customer: Athol Manufacturing P.O. Box 105 Butner, NC 27509 Attention: Tom Baucom, Mgr. Tech. Date of Shipment: 3*/t. 7o Product: Trailer No.: 2-&t> 9 s Lot No.: Order No.: 8*3/3 #'-'3/7 Moisture, % Test.Method AER-1A . 0~S~ Bulk Density, gm/cc Brabender Dry Time, mins 8.410 8.450 --J7 Particle Size, % on 8.300 40 Mesh m>. a O 200 Mesh Pan 1.7 Residual VCM, ppm 8.355 Not more than 8. PPM Inherent Viscosity 8.600 This material was produced to yield an inherent viscosity in the range of t. <> O to A 9 if__ . Laboratory Supervisor/Lead A -1t t '#r *r VAB.0001209682 PVC BULK TRAILER ANALYSIS Date n-?z 2Z5Customer 6. AXTechnician Product S415 Silo L f FRONT MOIST Top Bottom \oS 2. CONT. Top Bottom 1. / 3 2. GEL 2. 1. 1. 1. Trailer Number /-A to J Time A2 S3 * /#<ro Order No. rzt 3 irt BULK DENSITY 1. 2. 1. DRY TIME 1. 4.7 2. 1. COLOR L - A/, /? \ = 0lf vise B = /-*? L= r(* " t> /o. MIDDLE 2. END 1. 2. r1 mi. 2. 2. 2. 1. 1. * 2. , I. 2. A= B= L= A= B= Particle Size Distribution: Screen AnalysisMin On Rotap shaker. 49 gms. Resin plus 1.0 gins. Carb Mesh Size 40 60 80 100 120 140 Gross Wt. Tare ^ Net Wt. / % on Mesh > o 0 *O & 6'H it.tcf is: .3 373 f.fo H<o\ IfA $.6 Screen Analysis Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb 200 /7J Mesh Size Gross Wt. 40 60 80 100 120 140 200 Tare Net Wt. % on Mesh Glassy Pan Part. 0-ff /? Glassy Pan Part. Remarks Star 207A Revised 1/12/87 VAB.0001209683 Vida Falyman A Division of Tim Lonipoviy\/|*4m r JUBUIUHlIhAj unrhoqi Highway 25 Pod Office Box 91 Abardaan, Mwawippi 39730 Phone (601) 369-8111 LETTER OE CERTXEICATION Date: 13 Customer: Athol Manufacturing P.0. Box 105 Butner, NC 27509 Product: S^/jT Trailer No.: T^TJiZ. Attention: Tom Baucom, Mgr. Tech. Services Lot Mo.: Date of Shipment: fji Order No. : Moisture, % ABR-1A Bulk Density, gm/cc 8.410 Brabender Dry Time, mins 8.450 Particle Size, % on 8.300 40 Mesh 200 Mesh Pan Residual VCM, ppm 8.955 Inherent Viscosity 8.600 Not more than 8.5 PPM This material was produced to yield an inherent viscosity in the range of /*A9 to visor/Lead VAB.00012 PVC BULK TRAILER ANALYSIS Date 3-/ Customer fffh Technician Product Silo___ Trailer Number Time Order MOIST Top Bottom l. CONT. Bottom GEL BULK DENSITY DRY TIME COLOR L = /*//<' FRONT 2. 1. W*2. 2. 2. A = a II B = 411 1. 1 1. L= vise RVCM 0 MIDDLE 2. END I. 2. 2. 2. A= B= I 1. 1. 1. L= A= 2. 2. 2. 2. B= Particle Size Distribution: Screen Analysis Min On Rotap shaker. 49 gms. Resin plus 1.0 gins. Garb Mesh Size Gross Wt. 80 100 120 140 200 Glassy Pan Part. &.C6 % on Mesh Screen Analysis S>,3 I?3 l3<h 1-37 Lfr/Z %o.7 2*- Hr* __ Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 60 _________ _________ _________ _________ _________ _________ 80 __ 100 120 140 200 _________ _________ ______ ______ 0.78 ftp Glassy Pan Part. Remarks Star 207A Revised 1/12/87 4 ii VAB.0001209685 mi rovyvnvri A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730 Phone (601) 369-8111 LETTER OF CERTIFICATION Date: 3~ I*3 ~ Customer: Athol Manufacturing P.0. Box 105 Butner, NC 27509 Attention: Tom Baucom, Mgr. Tech. Date of Shipment: Product: Trailer No. r7 Lot No.: Order No.'& P^opextx Test Method Moisture, % ABR-1A Bulk Density, gm/cc 8.410 Brabender Dry Time, mins 8.450 Particle Size, % on 40 Mesh 8.300 &66 200 Mesh Pan /, Residual VCM, ppm 8.955 Not more than 8.5 PPM Inherent Viscosity 8.600 This material was produced to yield an inherent viscosity in the range of to__ LCtZ. Laboratory sor/Lead A VAB.00012(19686 PVC BULK TRAILER ANALYSIS Date 3~(0-*70 Customer Technician FRONT Product Trailer Number __ Time ^ Order No. MOIST CON'T. Top Bottom Top | Bottom GEL BULK DENSITY W\oS ****** 1 ti- **** '1. DRY TIME 'H COLOR L vv/y- f0.2. 2. 2. 2. A= B = (./3 1. 1. l. 1. 1. L= vise RVCM e `ltd MIDDLE 2. 1. END 2. r Am * 1. 2. 2. 2. 1. 1. 2. 2. * 1. 2. A= BL= A= B = TF1 75^ Particle Size Distribution: Screen Analysis Mesh Size 40 Gross Wt. Tare"~7 Net Wt. % on Mesh &0O 0.6 Screen Analysis Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. A&3 Min. 60 QiOt [fry 3sf- !7(p a/ 33 On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb 80 100 120 140 200 6.91 1H~ H Glassy Pan Part. Remarks Star 207A Revised 1/12/87 h VAB.0001209687 iwmM nnyviwra Attrition of "w wUnvooi wOfnponjr m^-g1n-w--v--n--r 25 FbiilOfne Bor 91 AboidMn, MMatiboi 39730 Phono (601) 3694H11 Date:-2 7 LETTER OB* CERTIFICATION VBIA Customer: Athol Manufacturing P.0. Box 105 Butner, NC 27509 Product: &'+!?' Trailer No.: T- 2t/0 Attention: Tom Baucom, Mgr. Tech. Services Lot No. : Date of Shipment: 2.1 frl, f0 Order No. : fS/3ff~ Moisture, % Test Method ABR-1A a 07 1 1 *N Bulk Density, gm/cc 8.410 Brabender Dry Time, mins 8.450 Particle Si2e, % on 8.300 40 Mesh 200 Mesh JL.0 _ ... ^ ^ . . Pan Lm____ Residual VCM, ppm 8.955 Not more than 8.5 Inherent Viscosity 8.600 This material was produced to yield an inherent viscosity in the range of J*00 to Ao4__ . ead A VAB.000120*2688 Customer Technician PVC BULK TRAILER ANALYSIS Particle Size Distribution: Screen Analysis Mesh Size 40 Gross Wt Tare Net Wt. % on Mesh / 6* 0.0 Screen Analysis Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 Remarks On Rotap shaker. 49 gms. Resin plus 60 80 100 120 140 200 3lL> &=r Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Pan 60 80 100 120 140 200 Glassy Part. Star 207A Revised 1/12/87 VAB.00012096^? $ *0 Vista Mysiifi ADfeWonaf w viwiniCKiK uomporvy Highway 25 to#Offic*Bo91 Abwtkwv Mhanippi 39730 Phoiw (601) 349-8T11 LETTER OF CERTIFICATION Date ' 3 -- 3^-5^ ^ ^ VBIA Customer: Athol Manufacturing P.0. Box 105 Butner, NC 27509 Product: 341* -in Trailer No.: / - 25 Attention: Tom Baucom, Mgr. Tech. Services Lot No. : Date of Shipment: ^ Cj Q Order No. : 31 35$" 3 Moisture, % IsaS Etebg ABR-1A Bulk Density, gm/cc 8.410 Brabender Dry Time, mins 8.450 Particle Sise, % on 8.300 40 Mesh 200 Mesh Pan 1,3 Residual VCM, ppm 8.955 Not more than 8.5 PPM Inherent Viscosity 8.600 This material was produced to yield an inherent viscosity in the range of f,0b to /* P*f__ . V Ai aT\~1 Laboratory Supervisor/Lead VAB.0001209690 PVC BULK TRAILER ANALYSIS Date Jl -2 <?o Customer Tefhnirlan Cx> ~S Product Silo Ct 9o, 09/ Trailer Number Time /io 0 Order No. --2//0 FRONT MOIST Top Bottom 2. CON'T. Top Bottom 'i/ 2. GEL BULK DENSITY y 1. to .</9o 2. 2. DRY TIME 1. 2. L ................................................... ... 1. 1. MIDDLE 2. ' * *> i 2. 2. 1. -> COLOR L =/P/.^p A = 0*0 2. B - 0.77 L= vise RVCM %IquJ o A= 7ii~i B= 1. 1. 1. 1. t. L= A= 2. 2. 2. 2. 2. B= Particle Size Distribution: Screen AnalysisMin On Rotap shaker. 49 gms. Resin plus 1.0 gins. Carb Mesh Size 40 Gross Wt. Tare% Net Wt. % on Mesh 6.00 0.0 Screen Analysis 60 80 100 120 140 200 o.i9 Q.y Min. 14.00 /7-j?9 jo. if 4.4o Jf.o 74f 22.0 &JF a.3L 4. 7 On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Mesh Size Gross Wt. 40 60 80 100 120 140 200 Tare Net Wt. % on Mesh Glasay Pan Part. Glassy Pan Part. Remarks Star 207A Revised 1/12/87 A it. VAB.00012096<^ Villa Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730 Phone (601) 369-8111 LETTER OE CERTIFICATION Date: Customer: /2 Feb. Athol Manufacturing P.0. Box 105 Butner, NC 27509 Attention: Tom Baucom, Mgr. Tech. Date of Shipment: /2 F&b. 90 Product: Trailer No. * 7- s Lot No.: Order No. : S3//3&8-&/JL Property Test Method Moisture, % ABR-1A Bulk Density, gm/cc 8.410 t- Brabender Dry Time, mins 8.450 Particle Size, % on 40 Mesh 8.300 __AD 200 Mesh Pan Residual VCM, ppm 8.955 Not more than 8.5 PPM Inherent Viscosity 8.600 This material was produced to yield an inherent viscosity in the range of /./))____ to__/ 09____. rvisor/Lead A > VAB.0001209692 PVC BULK TRAILED ANALYSIS Date Customer Technician FRONT Product Trailer Number MOIST CON'T. Top Bottom Top GEL Bottom BULK DENSITY l. .<!>3 t-***#* + 1. - 1t t4 -4. ,4$7 WZ2. 2. -2. DRY TIME 1. 2. 1. 1. 1. 1. 1. COLOR L 7(X>.54 A=C.Of B = D<%[ L= vise MIDDLE 2. 1. END 2. l * I. 2. -1 2. 2. t. 1. 2. 2. 2. 1. 2. A= B= L= A= B= RVCM //< 0 'tfei Particle Size Distribution: Screen Analysis Mash Size 40 Gross Wt. Tare Nat Wt. % on Mash c>_ 0,0 Screen Analysis Mash Size Gross Wt. Tare Net Wt. % on Mesh 40 Min On Rotap shaker. 49 gms. Resin pitjs 1.0 gmib. Carb h. 60 80 100 120 140 200 Glassy Pan Part. VO J'.O fc<- & 1J >.& fsi- 060 C37 Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Pan 60 80 100 120 140 200 Glassy Part. Remarks Star 207A Ravised 1/12/87 v* VAB.0001209^93 Vista Fotymars A Division of Vista Chemical Company Highway 25 Pbst Office Box 91 Aberdeen, Mississippi 39730 Phone (601) 369-8111 LETTER OE CERTIFICATION Date: Customer: 7 fkb. ?0 Athol Manufacturing P.0. Box 105 Butner, NC 27509 VG1A Product: sv/f Trailer Ho. : Attention: Tom Baucom, Mgr. Tech. Services Lot No.: Date of Shipment: ? 90 Order Ho. : $3/3- Property Test Method Analysis Moisture, % ABR-1A ____ Bulk Density, gm/cc 8.410 ____ uf2_ Brabender Dry Time, mins 8.450 J10- Particle Sise, % on 8.300 ' 40 Mesh ____0.D 200 Mesh Pan A Ml Residual VCM, ppm 8.955 Not more than 8.5 PPM Inherent Viscosity 8.600 This material was produced to yield an inherent viscosity in the range of to___ /jut__ . /Lead .7 fA VAB.0001209694 PVC BULK TRAILER ANALYSIS Date g-tp-'Jo Product. 6 #5 Trailer Number Customer Silo___ Time Technician Order MOIST CON'T. Top Bottom Top Bottom GEL BULK DENSITY 1. FRONT 2. J7 1. 2. 3 pjpTf' 2. DRY TIME 1 1. 1. 1. 1 I. COLOR L a= B = *35 L- vise RVCM MIDDLE 2. l. END 2. 2. 2. A= B= 1 1. 1 I. L = 2. 2. 2. A= B= Particle Size Distribution: Screen Analysis Mesh Size 40 Gross Wt. Tare Net Wt. % on Mesh d 8 O Screen Analysis Mesh Size Gross Wt. Tare Net Wt % on Mesh 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. 6-g& fro(e !& 3.fX 33.! n7 5*5 jr/ Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 &&*(- /3 Glassy Pan Part. Remarks Star 207A Revised 1 /12/87 A VAB.0001209695 Vista Polymer* A Division of Vista Chfniccrt Company Highway 25 Rost Offic0 Box 91 AbenWi, Mississippi 39730 Phono (601) 369-8111 LETTER OE CERTIElCATION Date: ,2 Customer: Athol Manufacturing P.0. Box 105 Butner, NC 27509 Attention: Tom Baucom, Mgr. Tech. Date of Shipment: 2-g-*?0 Product: Lot Order No. : g ZISS*~3 11 Test Method Moisture, % ABR-1A Bulk Density, gm/cc 8.410 Brabender Dry Time, mins 8.450 Particle Size, % on 8.300 40 Mesh 200 Mesh Pan Residual VCM, ppm 8.955 Not more than 8.5 PPM Inherent Viscosity 8.600 This material was produced to yield an inherent viscosity, in the range of to Laboratory Supervisor/Lead VAB.000120969 PVC BULK TRAILER ANALYSIS Date. 8-S Customer Technician. C, FRONT -gy/rProduct LKiSilo___ MOIST CON'T. Top Bottom Top Bottom GEL 6:***G**(*o! ****** ****** 2. 2. 2. 1. 1. 1. T-Trailer Number Time Order No. BULK DENSITY 1. DRY TIME COLOR L = (0 o, ;H 90 2. 2. A = ,0*7 B- ,rI l. 1. L= vise RVCM / to.i MIDDLE 2. 1. END 2. A= 'J i 2. 2. 2. B= 1. 1. i. 1. L- A- 2. 2. 2. 2. B= Particle Size Distribution: Screen AnalysisMin On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb Mesh Size 40 Gross Wt. Tare Net Wt. % on Mesh p&*0 n.D Screen Analysis 60 80 100 120 140 200 Ml nAS ILJJ I<J. 3__________________ L.L .3 331 Z2 0 Min On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 60 80 100 120 _________ _________ _________ _________ _________ 140 200 ________ _________ _________ __________ ________ _________ ________ _________ _________ Glassy Pan Part. .17 _ 1.3 _ Glassy Pan Part. Remarks Star 207A Revised 1/12/87 m ff ;K VAB.00012096 T Vista Polymers ADiviaonof Vista Chawicai Company Highway 25 Post Office Box 91 Abardoan, Mnstssippi 39730 Phone (601) 369-8111 LETTER OE CERTIEICAT X ON 9oDate: -3 VIS1A Customer: Athol Manufacturing P.0. Box 105 Butner, NC 27509 Product: 541S Trailer No. : T-- Z-Vol Attention: Tom Baucom, Mgr. Tech. Services Lot No.: Date of Shipment: Order No. : S3i: C*? Teat-Method Moisture, % ABR-1A Bulk Density, gm/cc 8.410 Brabender Dry Time, mins 8.450 Analysis .w .`5ocs 4/7____ Particle Siae, % on 40 Mesh 8.300 6 o 0 200 Mesh Pan 1.7 Residual VCM, ppm 8.955 Not more than 8.5 PPM Inherent Viscosity 8.600 This material was produced to yield an inherent viscosity in the range of L 00____ to \ 10 4__ . 1Q Labo2$r2<ory Supervisor/Lead iV A VAB.0001209698 PVC BULK TRAILER ANALYSIS Date --*7 & Product ^ __________ Trailer Number___ ^^ Particle Size Distribution Screen Analysis Mesh Size Gross Wt. Tare Net Wt % on Mesh Screen Analysis 40 0 O%0 0 Mesh Size Gross Wt. Tare Net Wt % on Mesh 40 Min On Rotap shaker. 49 gins. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 JtL.t? jAiY 7i Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. S-Y& UZ Glassy Pan Part. Remarks. Star 207A Revised 1/12/87 VAB.0001209699 Vista Polymers A Division of Vnta Chemical Compony Highway 25 Past Office Box 91 Aberdeen, Mississippi 39730 Phone {601) 369-6111 LETTER OF CERTIEXCATXON Date: SI VBlA Customer: Athol Manufacturing P.0. Box 105 Butner, NC 27509 Product: STf/S* Trailer No. * Attention: Tom Baucom, Mgr. Tech. Services Lot No.: Date of Shipment: S/ Order No. Tegt-Method Ansizsis i n l l Moisture, % Bulk Density, gm/cc ABR-1A 8.410 . rot Brabender Dry Time, mins 8.450 ___ _______ Particle Size, % on 8.300 40 Mesh 200 Mesh Pan 4.1___ J.S Residual VCM, ppm 8.055 Not more than 8.5 PPM Inherent Viscosity 8.600 This material was produced to yield an inherent viscosity in the range of__ /* 06 __ to . ratory Superv /Lead VAB.0001209700 PVC BULK TRAILER ANALYSIS j/ Date Customer Technician FRONT MIDDLE END Product Silo >4/ ]____________ Trailer Number 7" "2t ? ______________________ Time 0^0* _____________________________ Order No._______________________ MOIST | CON'T. Top Bottom | Top Bottom ........ \~z '.o? -rr GEL BULK DENSITY :f ` . &2 3fr 2. 2. 2. 2. DRY TIME `W 2. 1. 1 1 1. ]. 1. COLOR L -/Ai.ol vise + B- *9/ L= V/f.f .............. 2. 111 "> v 2. 2. 2. A= B= 1. 1. 1. 1. 1. L= A= 2. 2 2. 2. 2. B= RVCM Particle Size Distribution: Screen Analysis______ L?Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb Mesh Size 40 60 80 100 Gross Wt. Tare < Net Wt. % on Mesh 0*0o 0*0 M/ xi.U l I?.** 2-Z^ 4-3* 2- 27,o Screen Analysis Min. On Rotap shaker 49 gms. Resin plus 120 7*4^ /r.7 140 200 7.74 z.w err *,9 1.0 gms. Carb Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 _________ 60 80 _________ _________ _________ _________ _________ ____ 100 120 140 _________ _________ 200 Glassy Pan Part. .74 /4' Glassy Pan Part. ^_ Remarks Star 207A Revised 1 /12/87 y VAB.0001209701 Visla fotyman A Division of Vblo Chomicoi Gxwpony Highway 25 to* Office Box 91 Abfd--v Miwiwippi 39730 Phono (601) 369-8111 Date: j.3 90 Customer: Athol Manufacturing P.0. Box 105 Butner, NC 27509 Attention: Tom Baucom, Mgr. Tech. Date of Shipment: 23 Product: S/S*~ Trailer No. : 71 ?2X s Lot No.: Order No. : &3/S&2'~m30fa Moisture, % ABR-1A Bulk Density, gm/cc 8.410 Brabender Dry Time, mins 8.450 Particle Size, % on 8.300 40 Mesh 200 Mesh Pan Residual VCM, ppm 8.955 Inherent Viscosity 8.600 /..r Not more than 8.5 PPM This material was produced to yield an inherent viscosity in the range of 1.00 rvisor/Lead VAB.0001209702 PVC BULK TRAILER ANALYSIS Date f-^3 -7 Customer /Mi* Technician Product Silo___ Trailer Number Time //'JO *^<5^ Order No. 3 ffSe C FRONT MOIST Top Bottom 1A. S CON'T. Bottom GEL BULK DENSITY l 2. DRY TIME 1. M 2. COLOR &0 A = >. vise B == 1. 1 1. 1. 1 L= RVCM MIDDLE 2. 1 2. 2. A= B= 1. 1. 1. 1 L= END 2. A= B= Particle Size Distribution: /7e /Tlefstl Screen Analysis Mesh Size 40 Gross Wt. Tare Net Wt % on Mesh >. 0 Ad Screen Analysis Mesh Size Gross Wt Tare Net Wt % on Mesh 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. a.36, -a 7 3oif} 33-6 /'y^ 7^----- ---- ----- ------------------ ---f- 0 -'-- ------------- 3?)+' Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 a-fV Glassy Pan Part. Remarks Star 207A Revised 1/12/87 A VAB.0001209703 T Villa Wyman A Division of Villa Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730 Phone <601) 369-8111 LETTER OB' CERTIFICATION Date: Customer: n iff Athol Manufacturing P.0. Box 105 Butner, NC 27509 VISIA Product:&Y/6" _,, Trailer No. : T~7J3 Attention: Tom Baucom, Mgr. Tech. Services Lot No.*. Date of Shipment: /7 "J/fM ^0 Order No. : Teat Method Moisture, % ABR-1A UHL. Bulk Density, gm/cc Brabender Dry Time, mins 8.410 8.450 Jf.9 Particle Size, % on 8.300 40 Mesh JUL-- 200 Mesh Pan JUt L Residual VCM, ppm 8.955 Not more than 8.5 PPM Inherent Viscosity 8.600 This material was produced to yield an inherent viscosity in the range of / AO __ to /.^V__ . ervisor/Lead A VAB.0001209704 PVC BULK TRAILER ANALYSIS Date n 70 Customer COlrJL* Technician C. Product Silo fcq/ Trailer Number Time 0 Order No. 123 FRONT -------------------V- ----------------------- ___ *____ _ MOIST CONT. Top Bottom Top j Bottom f t1 t fl 1 t 1 * * 1 ****** GEL ii<?/ fa BULK DENSITY 2. 2. 2. 2. DRY TIME 1. (f -9 2. COLOR vise l =|08-W 1 RVCM A- . 10 - /< 1 2- 7i 1. 1. 1. 1. 1. L= MIDDLE 2. END 1. 2. t 2. 1. 2. 2. 2. 1. 1. 2. 2. 2. 1. 2. A= B= L= A= B= Particle Size Distribution: Screen Analysis Mesh Size 40 Gross Wt. Tare Net Wt. <h.o 0 % on Mesh 0.0 Screen Analysis Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 Min On Rotap siiiaker. 49 gms. Resin plus 1.0 gnvs. Carb 60 80 100 120 140 200 Glassy Pan Part. l%9 /xxr US' 3or 2.30. ,13 23*9 v.\ /*.<? c. / 1,3 Min. On Rotap shaker 49 gms. Resin 1plus 1.0 gms. Carb Pan 60 80 100 120 140 200 Glassy Part. 1 Remarks Star 207A Revised 1/12/87 VAB.0001209705 Vista Myrntrs A Division of Vida Chmieoi Company Highway 25 Rod Offica Bax 91 Abfd--, Mhiiitippi 39730 Phon* (601) 369-8111 LETTER OE GEKTIFICATION Date ` Customer: Athol Manufacturing P.0. Box 105 Butner, NC 27509 Attention: Tom Baucom, Mgr. Tech. Date of Shipment: Z-/<T-*7 Trailer No. *Lot No.: Order No.: Moisture, % ABR-1A Bulk Density, gm/cc 8.410 Brabender Dry Time, mins 8.450 Particle Size, % on 8.300 40 Mesh 200 Mesh Pan Residual VCM, ppm 8.955 Inherent Viscosity 8.600 QK Not more than 8.5 PPM This material was produced to yield an inherent viscosity in the range of A * to *ltl Laboratory Supervisor/Lead VAB.0001209706 HG'-I* Customer PVC BULK TRAILER ANALYSIS FRONT I2E Bottom IE 'M '3 2. 2. Bottom GEL / M BULK DENSITY l 2. DRY TIME 1 1. 1. I 1 MIDDLE 2. 2. i. I. 1. 1. 1 END 2. 2. 2. 2. 2. COLOR L= A = // BO L= A= vise RVCM e> B= L= A= B= Particle Size Distribution: Screen Analysis Min Glassy Pan Part. Mesh Size 40 60 80 100 120 140 200 Gross Wt. Net Wt. % on Mesh Screen Analysis Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 _________ _________ _________ _________ a7& I&J7& i3t=L (STfr tfs?- Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Garb Pan 60 80 100 120 140 200 Glassy Part. _________ _________ _________ _________ _________ ____ _________ _________ ____ _________ ____ _______ Remarks Star 207A Revised 1/12/87 . r. |4 VAB.0001209707 Vfato Potym#n A Divirion of vm witmvcQi v.ovnpony Highway 25 fort Offic* Bax 91 Abmdmiy Mlninipri 39730 Phom (501) 369-8111 LETTER OB' CERTIFICATION Date: h 1 ^ VlSIA Customer: Athol Manufacturing P.0. Box 105 Butner, NC 27509 Attention: Tom Baucom, Mgr. Tech. Date of Shipment: Product: Trailer No. : yi 2,*/^ s Lot No.: Order No. : gSl 3 .gperty Teat Method Moisture, % ABR-1A Bulk Density, gm/cc 8.410 Brabender Dry Time, mins 8.450 Particle Size, X on 40 Mesh 200 Mesh Pan 8.300 0.0 v5T / __LJL_ Residual VCM, ppm 8.955 Not more than 8.5 PPM Inherent Viscosity 8.600 This material was produced to yield an inherent viscosity in m .the range of to /ftr Laboratory Supervisor/Lead t VAB.0001209704 PVC BULK TRAILER ANALYSIS Date Customer Technician 1*> Product Silo___ S'ifS MOIST Top Bottom 1 P. CON'T. Bottom GEL l FRONT 2. 2. 2. l l i. Trailer Number Time Order No. BULK DENSITY 1. DRY TIME 1. COLOR L 2. i. l. = B = dM L= vise RVCM MIDDLE 1. END 2. 2. 2. 2. A= B= I 1 ]. 1. L= 2. 2. 2. A= B= Particle Size Distribution: Screen Analysis Mesh Size Gross Wt. 40 % on Mesh 0.0 0.0 Screen Analysis Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. 04* >rLf-' XU /a ofe SI 13 Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Pan 60 80 100 120 140 200 Glassy Part. Remarks Star 207A Revised 1/12/87 VAB.000120 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730 Phone (601) 369-8111 Date: Customer: LETTER OE CERTIFICATION VISIA t 90 Athol Manufacturing P.0. Box 105 Butner, NC 27509 Product: fV/S* Trailer No.: 7-2.9S0 Attention: Tom Baucom, Mgr. Tech. Services Lot No.: Date of Shipment: F 90 Order No. : 93J3ffm99 l?E2Eety Moisture, % ABR-1A Bulk Density, gm/cc 8.410 Brabender Dry Time, mins 8.450 Particle Size, % on 8.300 40 Mesh 200 Mesh Pan Residual VCM, ppm 8.055 Inherent Viscosity 8.600 ____ ZT____ Not more than 8.5 PPM This material was produced to yield an inherent viscosity in the range of AA0____ to A0____. rvisor/Lead VAB.000 PVC BULK TRAILER ANALYSIS 'I Date Customer Technician FRONT Product Silo___ Co'lO h'y/ Trailer Number Order No. /A Te0 MOIST CON'T. GEL BULK DENSITY 1. DRY TIME 1 COLOR vise L (cb? 6 A = &(*f- w2. 2. B. 6 8f l. 1. ! 1 1. L = RVCM MIDDLE 2. 1. END 2. T ] 2. 2. 2. 11 2. 1 2. A= B= L= A= B- Particle Size Distribution: Screen AnalysisMin On Rotap shaker. 49 gms. Resin plus I.Ogms. Carb Mesh Size Gross Wt. Tare'~7 Net Wt. % on Mesh Screen Analysis 40 0b 60 80 100 120 140 200 Lsr Min. 9f$ <>?% On Rotap shaker 49 gms. Resin plus 3? 1.0 gms. Carb Mesh Size Gross Wt. 40 60 80 100 120 140 200 Tare Net Wt. % on Mesh Glassy Pan Part. Glassy Pan Part. Remarks. Star 207A Revised 1 /12/67 VAB.0001209 Vista foiymors A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730 Phone (601) 369-8111 LETTER OE CERTIFICATION Date: 3 zr** f0 Customer Athol Manufacturing P.0. Box 105 Butner, NC 27509 Product: Trailer No.: 7 Attention: Tom Baucom, Mgr. Tech. Services Lot No.: Date of Shipment: 3 Order No. : VIS1A Teat-Method Analysis Moisture, % ABR-1A -ijL Bulk Density, gm/cc Brabender Dry Time, mins 8.410 8.450 __ __ iiJ Particle Size, % on 40 Mesh 8.300 __ JJL. 200 Mesh Pan 2.3 Residual VCM, ppm 8.955 Not more than 8. Inherent Viscosity 8.600 This material wa produced to yield an inherent viscosity in the range of )00 __ to ____ . Laboratory rvisor/Lead A VAB.000120^a2 PVC BULK TRAILER ANALYSIS Date Customer Technician FRONT Product , &Silo ^ _____________ Trailer Number _____ Time _______________ Order No. MOIST Top * Bottom '.04- 2. CON'T. Top Bottom GEL BULK DENSITY 1. >2J_ 1. ** fW 2. 2. 2. DRY TIME 1. -3 2. COLOR L- loo. A= Or O'"? vise RVCM flop* B = l-t 1. 1. 1. 1. 1. L- Of-a MIDDLE 2. 1. END 2. t * 1. 2. 2. 2. 1. 1. 2. 2. 2. 1. 2. A= B= L= A= B= Particle Size Distribution: Screen Analysis /Z? Mesh Size 40 Gross Wt. Tare Net Wt. % on Mesh n-> Screen Analysis Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. tp.st* Sabi /,>& 3 <#./< LL 4/,3 /bn y/ 4,? Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Q.6?, L3. Glassy Pan Part. Remarks Star 207A Revised 1 /12/87 VAB.00012097 Vista Polymers A Division of Vista Chemical Company Highway 25 Pad Office Box 91 Date: /--2~ Customer: Athol Manufacturing P.O. Box 105 Butner, NC 27509 Attention: Tom Baucomj Mgr. Tech. Date of Shipment: /- 2 ~ Aberdeen, Mississippi 39730 Phone (601) 369-6111 Product Trailer No. : s Lot No.: a Order No. : VE1A * / /J -2?7 Moisture, % ABR-1A Bulk Density, gm/cc 8.410 Brabender Dry Time, mins 8.450 Particle Size, % on 8.300 40 Mesh 200 Mesh Pan Residual VCM, ppm 8.955 Inherent Viscosity 8.600 . /O .49s QzOO 4.1 /.4 Not more than 8.5 PPM This material was produced to yield an inherent viscosity in the ranfe. of / && to ^ . 4 Laboratory Supervisor/Lead A VAB.0001209714 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730 Phone (601) 369-8111 LETTER OE CERTIFICATION Date: Customer: x? /l/eu, Z9 * Athol Manufacturing P.0. Box 105 Butner, NC 27509 Attention: Tom Baucom, Mgr- Tech. Date of Shipment: Ahtt* 9 VISIA Product: &/$* Trailer No. : 7- 7X3 * p s Lot No.: Order No. : J/3?Z-X9> Moisture, % ABR-1A Bulk Density, gm/cc 8.410 Brabender Dry Time, mins Particle Size, % on 6.450 8.300 40 Mesh 200 Mesh Pan Residual VCM, ppm 8.955 Inherent Viscosity 8.600 Analysis a L Not more than 8.5 PPM This material was produced to yield an inherent viscosity in the range of A4& to Labo rvisor/Lead A VAB.000120971*5^ PVC BULK TRAILER ANALYSIS U-S. Particle Size Distribution: Scrawi Analysis Mesh Size 40 Wt Tara Net Wt H on Mesh 9.00 OrO Screen Analysis Wt Tara Net Wt 40 Min On Rotap shaker. 49 gme. Resin plus 1.0 gms. Carb 60 100 120 140 200 Glassy Pan 6,0 Min Rotap shaker gms. Resin gms, Qlmy Pan Part. 100 120 140 200 Remarks Star 207A Revised 1/12/67 VAB.00012097't6