Document zQrj2OVR3Gjd9neb0Z4k1Oawn

j[jlJji||^ly^Ej5 AT^T^pFiFIlCiE; , ...^ ^ pAVDSAMP KBJTSB- T *. .S.UX- TBIS* oor CAK. TOIDOK. A...*<in. u::mr-av. AX'-*. r,wiV ptaurofca fo twin mianuwm. arc, a pobpOhatiox oi ataaaaa . . :. ': - ' *?f44sut<Bti6nWti fo * jplodfol'fcr pfo-' .ammonium perctdorste*fo foe hydrochloric vt,> .^5*>*riiai:'dU*otuom peidilormfo* Af foe ii- eidsoIiitionedeKribed. ; . , .. -. -:.TMTV' S'.:v. - " * ' crl.??H*rX,iC. 8. Patent Wo, l,OM,*il,fosoed s '1. The prooees cf producing a disxonium -/Vly^hrusiy S6,1918, propose* a detonating cap perchlorate of a diphenyl derivative com- J.V--WL 'eppfoinfog * diaxonium perchlorate of an aro- prising diaxotixing an amino-derivative of I ' jraatic or of a nitrated aromatic hydrocarbon, diphenyl, reacting the diazotized diphenydl in r"'Hen describee diaxonium derivatives ofben- acid eolation with perchloric acids,. and re- - .it ' ;|/.Xol, toluol,xylol and also nitro-derivatives of moving the precipitated jd:ia--x--o-n-:i--um perchlo-' ' /'Y*.''! these compounds as suitable filling material rate from eolation. for detonators of this type. S. The process of prodacing diaxonium ' ftJ i; j "We have discovered a meeththooddbbyywi hich di- perchlorate of a nitrated diphenyl derivative, I^poniam Belts may readily- be made from di- Comprising diaxotixing an amino-derivative ` &v''if,th__e_n_y_l a_n_d__a_it,_ro__a_in.h--enyl ddeerrivivnativteivee, ,w--h--i-c--h- :of a nitrompbcsxyl, reactin^g the diacotueddi*^' * mIU hate an explosive force comparable phenyl in add solution with perchloric acid, j ' a `frith those prepared from benzol or allied de- and remoovviing the precipitated diaxonium "r` Nvatire*. It is accordingly the principal ob- perchlorate lotion.' -.I--' v- r' v . ieot of oor invention to proViae a prooees 8. A com] the general formu- . * r-f ' TOWOLDMONOQ57444