Document z6QjxLMMw4oKGkn1X29kX9r6

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I 'I L I- i- I i i i i i i i i ii i i i i i i i i !i i i i 4 VAB.0001198091 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 1 1 A CERT I F I CATE CD F7- ^ M L_ V S I S Date: -9 . 9/ Customer: United Technologies 2500 Highway 6E Iowa City, IA 52240 VIS1AProduc t: 5415 Trai1er No. : 'W0 Attention: Quality Control Manager Order No.: ooo q 332 -000 Ship Date: y >&c.. <?/ Customer P.0. No.: 06ror* Propertv Moisture, V, Contamination, BLK/BRN Hard Particles @ 7 mins. Bulk Density, gm/cc Brabender Drytime, mins. Resin Flow Time, tap/sec Particle Size, V. on 40 Mesh 200 Mesh Test Method ABR-1A ABR-5A ABR-12 ABR-2B ABR-7 ABR-8 ABR-3 Residual VCM, ppm ABGC-26 Inherent Viscosity ABR-10 METS IR, V. of Control ABR-13 ** Values for this property has been determin and is not tested on truck shipments. Ana 1vsis _______________________ 2 / s0 I ft * * / //.* AH /,* /. o 3 /2 0____ * t by our SQC Program (601) 369-8111 VAB.0001198092 PVC BULK TRAILER ANALYSIS A Date Customer Technician Product Silo___ MOIST CONT. GEL I. Trailer Number. Time Order No. BULK DENSITY DRY TIME I COLOR L= FRONT 2. 2. II A= B= L= vise RVCM MIDDLE 2. A= B= l I L= END Particle Size Distribution: <T CAM*-' SVL^jJi-eJs^ A B= Screen Analysis Mesh Size Gross Wt. Tare Net Wt. H on Mesh Screen Analysis 40 f)r-<P Mesh Size Gross Wt. Tare Net Wt. H on Mesh 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. .3 Min. /. 60 13.7 o Z?.V Ht-H 33.1 to. LL .10 f.r Z.to - LI On Rotap shaker 49 gms. Resin plus 1.0 gms. . Carb 37-43 sr.&r n. /A 3 7 X 80 100 120 140 200 # 3 nt* Glassy Pan Part. Remarks ft Date._______ ____ Customer UCT& Technician lL. PVC BULK TRAILER ANALYSIS Product sv/SL Silo___ Trailer Number -JZ*/8o Time Order No. <QQO <0 00 A Particle Size Distribution Screen Analysis Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb Mesh Size Pan 40 60 80 100 120 140 200 Gross Wt Tare Net Wt % on Mesh Q.O* .3L 0 iS 16.07 3-3$~ 33A -23.7 JJA A1 Screen Analysis ;i .E i Min On Rotap shaker 49 gms. Resin plus 1.0 gms. Carta Mesh Size Gross Wt. Pan 40 60 80 100 120 140 200 Tare Net Wt. % on Mesh Glassy Part. 0 Remarks Star 207A Revised 1/12/87 .0001198094 Vista Polymers A Division of c Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIF I.CATE OB' ANALYSIS Date: j f~ 3 - *? I Customer: United Technologies 2500 Highway 6E Iowa City, IA 52240 Attention: Quality Control Manager Product: 5415 V1S1ACode No.: RMS-XK-21 Trailer No.: Ml Order No.: OOO 3cG 7-D&0 Date of Shipment: (j-`3-^ | Cust. P. 0. No. : 0<*T'o%Z Property Test Method Specification Analysis Moisture, % Contamination, blk/brn Hard Particles @ 7 mins. Bulk Density, gm/cc Brabender Drytime, mins. Resin Flow Time, tap/sec Particle Size, % on ABR-1A ABR-5A ABR-12 ABR-2B ABR-7 ABR-8 ABR-3 .30 max. 35/100 max. 25 max. .460 min. 6.0 max. 1 / 15 max i 3/y 3 O 40 Mesh (0.1 Max.) 0.^ 200 Mash K sr Pan (5.0 Max.) /.L Residual VCM, ppm ** Inherent Viscosity ABGC-26 ABR-10B 8.5 ppm max 1.00 - 1.04 . 00*5* < 8.5ppmv I-OI _ *bax~ . + Specification of 25% 200 mesh and the pan). max. thru 140 mesh sieve No specification for 200 (includes the mesh alone. CUiwuCt&K ** andUarefnotttiftenrtrucnh^e,,teter,nined by Ur SQC Program Laboratory Supervisor/Lead VAB.0001198095 PVC BULK TRAILER ANALYSIS 4\ Date Customer mduct Trailer Number Order FRONT MOIST Bumnii JS CONT. Buunm 1 BULK GEL | DENSITY \S/ T7 / \jtfe * ni * r DRY | TIME |7 49 11 1 COLOR 1L J A - JZ. I B - /* /2. I I i L- vise RVCM MIDDLE lI END Particle Size Distribution Scrawl Analytic Mtih Sin 40 Gross Wt - ------------------- Tara Nat Wl H on Math e>.oe> Scrawi Analytic Mach Sin Groat Wt. Tara 40 Min On Rotap shafcw. 40 am. Resin phis 1.0 gmt- Ctrti 100 120 140 Pen Part .3 QM ILJL 22A On Rotap ihaktr 40 gma. Ratin plut P.ir r*z.s 1.0 gmt. Carto ,1% /. t Qlatty 100 120 140 H on Math Remarks __________________ ^--------- ------- -------- VAB.0001198096 - ---------------------------------------------------------------------- --------- Vista Polymers A Division of Vista Chemical Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601)369-8111 A CERTIFICATE OB' ANALYSIS Date: Customer: United Technologies 2500 Highway 6E Iowa City, IA 52240 Attention: Quality Control Manager Product: 5415 VISTACode No.: RMS-XK-21 Trailer No.: Order No.: ^oO Property Test Method Specification Analysis Moisture, % Contamination, blk/brn Hard Particles @ 7 mins. Bulk Density, gm/cc Brabender Drytime, mins. Resin Flow Time, tap/sec Particle Size, % on ABR-1A ABR-5A ABR-12 ABR-2B ABR-7 ABR-8 ABR-3 .30 max. 35/100 max. 25 max. .460 min. 6.0 max. 1/15 max. - /o J// / .49/ S'./ a//o. 0 40 Mesh (0.1 Max.) 200 Mash 0.00 Pan (5.0 Max.) /1 Residual VCM, ppm Inherent Viscosity ABGC-26 ABR-10B 8.5 ppm max 1.00 - 1.04 < 8.5ppm /*3 onnPeCi5iCa^ 1l f 25% max* thru 140 meeh sieve (includes the 200 mesh and the pan). No specification for 200 mesh alone. ** Valuee and are for * not th* is Property have been determined tested on truck shipment. by our SQC Program Laborfftrory Supervisor/Lead VAB.0001198097 TtcMriaii UTT.C- PVCBULKIRMtBF ANALYSS % A Ordtr MJUC OCNSITY COLOR VISC RVCM FRONT 12. 1 IT---- l MIDDLE [2. [ 1. I END T J 12. I 11. 1 1w 2* 11 ji. I 12. 1 1; n Ji I^ Panicle Size Distribution On 1.0 fttosli 81x9 40 Omsx Mfl* Tam Not Wt. n on Moon O. O 0 OQ- Sevoon jUiolylo 2/7 Mr. ISO UM MJ2 MU LL2. On 40 140 tJ Moon Otoo Imoo MR. T 40 I 140 a H on mail Remarks 04 9/ aid. fr 4 VAB.0001198098 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 A CERTIFI CATE OB' ANALYST 3 Date: Customer: 3 91 United Technologies 2500 Highway 6E Iowa City, IA 52240 Product: 5415 VK1ACode No.: RHS-XK-21 Trailer No.: "p Attention: Quality Control Manager <900/ 93 3- 3>W Date of Shipment: J Oust. P. 0. No.: ObS'0%'3 Property Test Method Specification Analysis Moisture, % ABR-1A .30 max. Contamination, blk/brn ABR-5A 35/100 max. Hard Particles 9 7 mins. ABR-12 25 max. Bulk Density, gm/cc ABR-2B .460 min. Brabender Drytime, mins. ABR-7 6.0 max. Resin Flow Time, tap/sec. ABR-8 1/15 max. Particle Size, % on ABR-3 40 Mesh (0.1 Max.) 200 Mash * o.o J.9 Pan (5.0 Max. .., ! ^ Residual VCM. ppm ABGC-26 8.5 ppm max. < 8.5ppm Inherent Viscosity ABR-10B 1.00 - 1.04 Specification of 25% max. thru 140 mesh sieve (includes the 200 mesh and the pan). No specification for 200 mesh alone. ** Values for this property have been determined by our SQC Program and are not tested on truck shipment. i VAB.0001198099 PVC BULK TRAILER ANALYSIS fZ Date. 9 2-9/ CiMtomer Technician FRONT Product S't J lT i fo MOIST Bottom CONT. nci '.cl .yj ......... yj^ f / Pc- I II Trailer Number Time Order No. 7~-So? BULK DENSITY . ro DRY TIME C-0 COLOR /c*.7 * C/o vise RVCM B - /i,/ I L* MIDDLE II END Particle Size Distribution: Scraan Analysis_______ /JL_______ Min On Rotap shafcsr. 49 gms. Rssln plus 1.0 gmt. Csrb Mas* Slza 40 00 00 100 120 140 200 Olssty Pan Part. Gross Wt. Tara ^-- Nat wi. H on Mash __________ __________ __________ __________ ____________ ____________ ____________ ____________ __________ _________ _____________ ____________ __________ AO? 2o-LC LC.tr ________ 7. 93 ________ _________ _ . _ J-.ST A 4JC . 90 ______ _______ ^0 2. V / i/7 AA JT 7. / 2.. 7 /,Q _______ Scraan Analysis ------------------------- Min. On Rotap shakar 40 gms. Rasin plus 1.0 gms. Csrb Mash Slza Gross Wt. Taro Nat Wt. 44 on Mash 40 ______ ______ ______ ______ 120 140 Remarks Star207A Ravtsad 1/12/87 ii 198100 PVC BULK TRAILER ANALYSIS 4 Dale Customer IP Technician FRONT Product --T^^ltw Silo Trailer Number Time Order No. MOIST Bottom CON'T Bottom GEL r ^ ........... *>*V ..........p?" am. ii ^*> |2* BULK DENSITY I DRY TIME I COLOR L * /(> D,f& A = ~ O'lb 'r 1. |i. /</? La vise RVCTfl MIDDLE 4a 7------- am i. 11 i |i. A= END Particle Size Distribution: Scraan Analysis Mash Slza 40 Gross Wt Tars Nat Wt H on Mash O 6* a*5 Scraan Analysis Mash Siza Gross Wt Tara Nat Wt H on Mash 40 Min On Rotap shakar. 40 gats. Rasin plus 1.0 gms. Carto 60 100 120 140 200 Glassy Pan Part. m 2.? usrt 2.t>2 3. /4 4<.X up L. c> 4.3 Min. On Rotap shakar 49 amt. Rasin phis 1.0 gms. Carto 60 80 100 120 140 200 o.d? /.f Glassy Pan Part. Remarks S Star 207A Ravissd 1 /12/87 VAB.UUU1198ID1 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mesissippi 39730-0091 Phone (601) 349-S111 4 CERTIFICATE OF ANALYSIS Date: 8- (& - / Customer: United Technologies 2500 Highway 6E Iowa City, IA 52240 Product 5415 Code No VIS1A-XK-21 Trailer No Attention: Quality Control Manager Order No. Date of Shipment: 8-->-*?/ Oust. P. 0. No. Property Test Method Specification Analysis Moisture, X ABR-1A .30 max. ./O Contamination, blk/brn Hard Particles 9 7 mins. ABR-5A ABR-12 35/100 max. 25 max. 2 Bulk Density, gm/cc Brabender Drytime. minB. Resin Flow Time, tap/sec. Particle Size, % on ABR-2B ABR-7 ABR-8 ABR-3 .460 min. 6.0 max. 1/15 max. o/%9 40 Mesh (0.1 Max.) .O 200 Mash * Y-Z Pan (5.0 Max.) Residual VCM, ppm Inherent Viscosity ABGC-26 ABR-10B 8.5 ppm max 1.00 - 1.04 < 8.5ppm /.OX * Specification of 25% max. thru 140 mesh sieve (includes the 200 mesh and the pan). No specification for 200 mesh alone. ** Values for this property have been determined by our SQC Program and are not tested on truck shipment. Laboratory Supervieor/Lead VAB.0001198102 Date: ^S''9/ Product: 5415 Customer: United Technologies 2500 Highway 6E Iowa City, IA 52240 Code No. : RMS-XK-21 Trailer No. = Attention: Quality Control Manager Order No. : 6000 *j-ol-060 Date of Shipment-2-5-^/ Cust. P. 0. No. : 0 Co ST) 3 <3 Property Test Method Specification Analysis Moisture, % ABR-1A Contamination, blk/brn ABF-5A Hard Particles 9 7 mins. ABR-12 Bulk Density, gm/cc ABR-2B Brabender Drytime, mins. ABR-7 Resin Flow Time, tap/sec ABR-8 Particle Size, % on ABR-3 40 Mesh (0.1 Max.) 200 Mash * e-6o 3./ .30 max. 35/100 max. 25 max. .460 min. 6.0 max. 1/15 max. .2/ 4-/3 / . Sea s.z/ Pan (5.0 Max.) 2.0 Residual VCM, ppm ABGC-26 8.5 ppm max. < 8.5ppm Inherent Viscosity ABR-1OB 1.00 1.04 * Specification of 25% max. thru 140 mesh sieve (includes the 200 mesh and the pan). No specification for 200 mesh alone. ** Values for this property have been determined by our SQC Program and are not tested on truck shipment. Laboratory Supervisor/Lead VAB.0001198103 PVC BULK TRAILER ANALYSIS Particle Size Distribution: Scroon AmlyNaNHn On Wetap stater. 4t gm. Wsain plus 1.0 gm. Caife Mash Six* 40 Own Wt. ______ Tm Net Wt. H on Mosli a 60 ao Seiran Anaiysia On flotep ahakar 40 Raabiptea 1.0 pm. CmU Maah Sin Oran Wt. Tara Not Wt. H on Most) -4 100 120 140 Remarks Part. i I Star 207A naalaai 1/12/07 1 I' VAB001198104 -'Hi-' V;s*o ;'o yme|rs A Division of Vtsio Chemical Company '-'igSway 25 >t>s! Office Box 91 Aderdeen, Mississippi 39730-0091 Phone {6011 369-8111 CERTIFICATE OB* ANALYSIS Date: Customer: X? flt+y 9/ United Technologies 2500 Highway 6E Iowa City, IA 52240 Product: 5415 * Code No.: RMS-XK-21 Trailer No.: 7= ?7 Attention: Quality Control Manager Order No.: 90X2S0' 009 Date of Shipment: X&Jflfoy 9/ Cust . P. 0. No. .* Property Test Method Specification Analysis Moisture, % ABR-1A .30 max. JL Contamination, blk/brn ABR-5A 35/100 max. Hard Particles 9 7 mins. ABR-12 25 max. Bulk Density, gm/cc ABR-2B .460 min. Brabender Drytime. mins. ABR-7 6.0 max. Resin Flow Time, tap/sec ABR-8 1/15 max. Particle Size, % on ABR-3 40 Mesh (0.1 Max.) At Residual VCM. ppm Inherent Viscosity 200 Mash * S.J ABGC-26 ABR-10B Pan (5.0 Max _ 8.5 ppm max 1.00 - 1.04 < 8.5ppm * Specification of 25% max. thru 140 mesh sieve (includes the 200 mesh and the pan). No specification for 200 mesh alone. ** Values for this property have been determined by our SQC Program and are not tested on truck shipment. Lab vlsor/Lead VAB.0001198105 7VC BULK TRAILER ANALYSIS Date Customer Technician prod uct_ Silo &2A /9f 2><L MOIST Tup 1 Bottom I CONT. Top Bottom GEL A Trailer Number Tlnw /CJi. Order BULK DENSITY DRY TIME i COLOR vise RVCM FRONT I ii i A = -0<OL B = A 7-2- L* MIDDLE I i ii END Particle Size Distribution Seresn Analysis Mfei On Rotap shaker. 49 gms. Huh plus 1.0 gms. Carta Mash Size 40 00 100 120 140 200 Gross Wt. ---- - --- --- ~------- Tars (D Nst Wt. H on Mssh 0.00 afi 22SO _Z2/ o, o 2.0 4^.0 27./ /5As> Scrssn Analysis ---- ------ ____ Min. On Dotap shaker 40 gms. Resin plus 1.0 gms. Carta Mssh Size Gross Wt. Tars Nst Wt. H on Mssh 40 00 100 120 140 Glassy Pan Part. 42 /,-2 Gtessy Pan Part. j Remarks. Star 207A 1/12/07 VAB.0001198106 Visla Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730*0091 Phone (601) 369-8111 A IFICATE OF AM A VS X S Date: Load Date r- y / VIS1A Product: 5415 Customer: United Technologies 2500 Highway Iowa City, Iowa 52240 Code No zr No : 7^ *72-3 Attention: Quality Control Manager Order No Date of Shipment: Customer P.0. No oof o 6v5~o S3 Propertv Test Method Moisture, 7. ABR-1A Contamination, blk/brn ABR-5A Hard Particles <9 7 min ABR-12 Bulk Density, gm/cc ABR-2B Brabender Dry Time, min ABR-07 Resin Flow Time, tap/sec. ABR-08 Particle Size, % on ABR-03 40 mesh Residual VCM, ppm Inherent Viscosi tv ABGC-26 ABR-10 Analysis ____ ^Z_ S' 200 mesh .7. ST P*n Laborato Supervisor/Lead VAB.0001198107 PVC BULK TRAILER ANALYSIS %t Qaie _________ Product SK(/S~_____________ Trailer Numb*r_H2ii Customer Uru4-t^f 'Tr'g-k. Silo Uiv Time ^^^3" Technician wOPS__________________________________ Order No. 9'/3 Q &/ Particle Size Distribution: Screen Analysis Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb Mesh Size Gross Wt. 40 60 60 100 120 140 200 Tare Net Wt. % on Mesh /. 06 V?. fc 2.*4 1.81 \3.\o *7 3.8 Screen Analysis -------------------------Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 60 80 100 120 140 200 Pan PH Olaaay Part. S -a 1 SO. 2- O'66 1.3 Glassy Pan Part. Remarks. * VAB.0001198108'; PHfTHHMUmiim! I'll i-HI4llllMiir||l-ki4lllitli|^" MMHpppilHipMMirPH^rH' i iiqippud i. h'Iv-i J'ii;pii|->-M-' iriipnp'] ......................... .`<npnr ' iMP^*iffiiimtitfrtfnvnnfi'ftfmi'fvtfmn..........MmitiiimpnniMiiilkTnFmtwjtipfiiim-innnnifiimftPnyiiniuilfftim.- ,| Eiit1|mmm'iff1|rfri'Ml'r| flpftff'imMi'Pi' !iHftiHM'"i'lPHii!ii'piiipi' -himhh =n'|inini'p- 1 rr^imMi>iPrifip|rM^M|MmMi'^P'PPiP '- <i|ir :3iur: i.ppiri|. p.MiiH': H.l' . ^pi-un ,-.iki tltrii' iM.p-i:!icr|l|lr-L^d|l.l|l: IP"! z 1 I I I I I I I I I i I I I I 4 H VAB.0001198109 Visto Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 A 4 VIS1ALETTER OB' CERTIFICATION . #ISW"A Date: September 13, 1991 Customer: Customer Service Suite 223D Houston, TX Attention: Mark Volz Date of Shipment: Sept. 11, 1991 Product: 5305 Railcar No.: UTCX 46591 Order No.: 0001720-000 Location: United Diet. Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Contamination Blk./Brn. B Color ABR-1A ABR-2A ABF-3 ABGC-26 ABR-10 ABR-5A ABR-9 . 10 .547 0.0 20.0 2.2 .073 .72 14/8 1.67 Laboratory Supervisor/Lead VAB.0001198110 V'*f:a Pol & Load Date Tine fflghMr~2Xr Amremmut -if/-* *' ' *> < * Contamination Syntron Method Screen Analysis Mesh 40 Weight <9.00 X Static Flow; Color L: 60 O* A 80 100 v 7.(o W-Z' 120 HO 200 Pan /o.oo 2o.o z.z X Glassies /Vo Avg. Microns b CPA: * (4T-3 f Technician: i| VAB.0001198111 Visla Polymers A Division of Villa Chemical Company Highway 25 Poll Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 Date: Sept. 13, 1991 Customer: Customer Service Suite 223D Houston, TX Attention: Mark Volz Date of Shipment: Sept. 11, 1991 VKt\I i I ON Product: 5265 Railcar No.: UTCX 46483 Order No.: 0001719-000 Location: United Dist. TX Propertv Moisture, 7. Bulk Density, gm/cc Particle Size, 7. on 40 Mesh 200 Mesh Test Method ABR-1A ABR-2A ABR-3 Residual VCM, ppm Inherent Viscosity Contamination Blk./Brn. B Color ABGC-26 ABR-10 ABR-5A ABR-9 Amy E. Bagwel Laboratory Supervisor/Lead Analysis 0.14 0.544 0.00 11.2 2.2 0.077 0.67 8/ 15 1.75 VAB.0001198112 1 Vista Polymers Highway 25 AbardMDt NS 397342^^ A KT A T VS T <? h Load Date ,hU Product 5265 Time Logged In: Q(^$P Logged Ship Date Silo(s): .. UI.C/S3 Car No Customer: Moisture Contamination Bulk Density BD w/antistat Viscosity RVCM Mirrex Shipments ONLY 2nd 1st 2nd 1st 2nd ./s I Jl n| 1 ~/z -y 1 ** C4-J 1 rSPfL 1, 2nd Screen Analysis Mesh Weight 40 4).oa X Ct 0 60 /< D 80 s.tl It > t 100 //.-? 23,1 Static Flow: Avg. Microns: Color L; . . 7 b _A7T 200 Pan 4 .? Technician: VAB.0001198113 KWfflHtttltflHllllltf|IPIllHlllimilt|HIMIlHllimiPFMHmillHmMMIMII|IPI't:^PMmHipp i<IIP||l'll-j^ll!lh1PMprMP'MIIP<IMmpiFi|IFM............... ll|ip|E<PMMMtl|*rL^iMM>-M4-:dr|ll|4nill|MMMilMnMli^M'in!n^l*MIIMl|piM^?~l^lM|inM<IE|kimi|P|IMII^plltllniMin!nillEIPI|ir>l(IP|Mlnhl^nMMM|IMn!arEII''fe'HaMMI<MMl!H^ni|IFfMM31^PIPlMlM^|PM>l!r^l|H^|l|||IMMIIPMrMllP|ll^ --rimMPMPaMlfeME4lll|irnfe9MMimi^<>lMII|*IIP^|rp*MM<||MIM|HMl^ElllM<IIPM91<^|pip*lhMIPI|r'IP!irMMmpt-!44|yi|dErLnNri .................... MUlMipppiHipri^N-'iP^PUp^HFUlFMr^iPMisfl^HmillMl'Mi?^?^................................................................................................................................................................................................................................... H F t \XK>iTU&Sictt r ji\I 'I r .I L I it I I I I r t L I I \ I I [ I [ I I I I I f t I I I L I I I H I I I I I I I * 4 VAB.0001198114 Vista Polymers A Division of Vista Chemical Company x Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730*0091 Phone (601) 369-81 1 1 *=* INI L_ N'S I S Date: .November 27, 1991 Customer: Attention: United Technologies 511 Hay Street P.0, Box 807 Mt. Airy, NC 27030 Quality Control Manager Ship Date: November 25, 1991 Product VtSlA Railcar No. UTCX 46411 Order No. 0004033-000 Customer P.0. No 050-01881 Propertv Volatiles, 7. Bulk Density, GM/CC Brabender Dry Time, Mins Particle Size, V. on 40 Mesh 200 Mesh Pan Vinyl Chloride Monomer Inherent Viscosity Hard Particle @ 7 Min Contamination, BLK/BRN METS IR, 7. of Contro1 Test Method ABR-1A ABR-2B ABR-7 ABR-3 ABGC-26 ABR-IO ABR-12 ABR-5A ABR-13 Ana 1vsis . 10 5.0 0.0 6.4 0.2 .001 1.01 1 7/8 123 Laboratory Sup (601) 369-3624 isor VAB.0001198115 |i|4' fir"' ' ! ` 1 -''I ,M 1 ' ,f VlltK BlIlfMli 'ri'M'r hi< ft* ir T ,' ' rf: Tfcff; % J Jfe il :i H- IK p*i win' 'n- SfrWV'! - /` * . | * i * Load Date: Timm Logged Ship Date; Product: i 5415" Car Ho.: %* Logged In By: Sllo( a): _&3S' Ghat -Aao Moisture Contamination Bulk Omnaity BD wo/antistat Hard Particie A GA 1 yC8 11st I 2nd l 16 | .^y fer1 s 1 2nd |r 7 L#"3T, /<? 1^ 1 1st 1 1 .t>t? 1 1 1| ~zr 2nd 1 1st I . 6*7 "p7 ?1 g Sr* | 41 . iT^C# 1 1 5*& 2nd Viscosity RVCM Screen Analysis Mesh U<i ight X 40 t, #*-? CiC 60 #V / ?6 BO 100 /*7 Drytime: Static Plot#: Color L; 120 140 200 Pan 0,0 Avf* Microns Ir 117 0- NETS: Technician: .. >;-> . I " Wl I|I Bit VAB.000119811 4 4 V Vista Polymen Highway 25 A Division of Post Office Box 91 Vista Chemical Company Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OF ANALYSIS Date: November 8, 1991 Customer: Attention: United Technologies 511 Hay Street P.O. Box 807 Mt. Airy, NC 27030 Quality Control Manager Ship Date: November 7, 1991 VIS1AProduct: 5415 Railcar No.: VIPX 45801 Order No.: 0003310-000 Customer P.0. No.: 050-01790 Property Volatiles, 7, Bulk Density, GM/CC Brabender Dry Time, Mins Particle Si2e, 7, on 40 Mesh 200 Mesh Pan Vinyl Chloride Monomer Inherent Viscosity Hard Particle @ 7 Min Contamination, BLK/BRN METS IR, 7m of Control Test Method ABR-1A ABR-2B ABR-7 ABR-3 ABGC-26 ABR-10 ABR-12 ABR-5A ABR-13 Analysis .10 .490 4.8 0.0 5.5 1.9 .004 1.01 3 10/15 121.5 Laboratory Supervisor (601) 369-3624 VAB.0001198117  w ''w *" :J I* 1,t '' .'V -T ''I ,Mi ' ` H'J M If ',ri,rl' '*'' ^,(113-nr!'h' M V ITlatai EbDnfar BtUMU SBC PVC RAXnC<AJE Date: v* v- V I If, Yf-wSS -- I. f 4> Screen Analysis Mesh 40 W? i tfii t % 0,0 60 80 100 /S' ic.zlo SS* 7 Si7. J 120 140 t%o ` ^4>o 200 s.lt 4.? Drytime: *.t Static Flos#; Atfg. Microns: Color L; /0t.-f7 SJL Ir ,NETS: %ZO, /Z/-S Pan .* i r! i Technician: f*i- -rr>->4i; .arta44MhrtW'JN M4TM-I IPipi II>1 P I I^P^WfTF* VAB.000119811 WW *'^ -HFWw'itVi v'V i<vr>*. :- nri,. . V- - |lhdtfiJlhp|J`'<'i- ......................... ... Vlitn Rdiwnt U -J' I il ** .1.'I tmj I* 4 I V iK i iUll |V Load Date; //- <?/ Tine Logged In: Product: S4ir Car No* iSgoJ % Lagged In By: Ship Date: SiiofsJ: ~ctze CUatooer Y/ "ti'1. 4* > I fc Screen Analysis Mesh W<? igh t X 40 Ot>o 0*& a- 32-1 100 IS,*? 120 140 V'3sr (?.? o?i94 5-5 Pan 0.9b ).<i Drytiae: Static Pleat ivf. Mlcrona: !( % Color L: (r NETS; * 4 r i! ( Technician: VAB.000119811 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE O YS X S Date 12/23/91 Customer: Attention: United Technologies 511 Hay Street P.0. Box 807 Mt. Airy, NC 27030 Quality Control Manager Ship Date: 12/20/91 Product: 5415 Railcar No.: PTLX 41597 Order No.: 0004995--000 Customer P.0. No.: 050-01972 Property Volatiles, 7. Bulk Density, GM/CC Brabender Dry Time, Mins. Particle Size, 7. on 40 Mesh 200 Mesh Pan Vinyl Chloride Monomer Inherent Viscosity Hard Particle @ 7 Min Contamination, BLK/BRN METS IR, 7. of Control Test Method ABR-1A ABR-2B ABR-7 ABR-3 ABGC-26 ABR-10 ABR-12 ABR-5A ABR-13 Analysis 0.14 0.493 4.7 0.00 3.3 1.3 0.001 1.02 1 5/8 117 H.D. Lucas Laboratory Supervisor (601) 369-3624 VAB.0001198120 Vtatmx Pt lymm Load Prt->c Screen Analysis Mesh 40 W<* i i$h t X 0-0 Drytine: 60 <3-7? 80 100 120 IT,^3 15-31 JO- \ r4 140 1^3 >. S 200 /63 Pan L2 mo/ Static Flov: ^ 9,3 Avf. Microns: Color L: ^ 0 }-) tr I'll : 43O h7.4~ LX Technician: VAB.0001198121 Vista Polymers A Division of Vista Chemical Company Highwoy 25 Post Office Box 91 IFIC O Aberdeen, Mississippi 39730*0091 Phone (601) 369 81 1 1 a r\j a V S I s b Date: Customer United Technologies P. 0. Box 807 Mt. Airy, NC 27030 Attention: Quality Control Manager Ship Date: -to- <?/ VISIAProduct: 5415 Trailer No/^0//) Order No.: QCO 4bD0'6 0& Customer P.0. No.: 0/rfalSL. Property Moisture, X Contamination, BLK/BRN Hard Particles @ 7 mins Bulk Density, gm/cc Test Method ABR-1A ABR-5A ABR-12 ABR-2B Analysis .06 /& I ,443 Brabender Drytime, mins ABR-7 Resin Flow Time, tap/sec ABR-8 0 / // / Particle Size, X on 40 Mesh 200 Mesh ABR-3 DO .$ Pan / b Residual VCM, ppm ABGC-26 .00! Inherent Viscosity METS IR, '/. of Control ABR-10 ABR-13 t. 03 % % !o * * ** Values for this property has been determined by our SQC Program and is not tested on truck shipments. / Labora t (601) 369-8111 VAB.0001198122 PVC BULK TRAILER ANALYSIS f Hat* 19.' ?'?/ Customer Technician. Jssrr^H>L^ Product Silo___ Trailer Number 7=%to Time /Pf* Order FRONT MOIST Bottom I I*ft4 * CONT. Bottom I. I t9 GEL BULK DENSITY i 1 1. ?-3 DRY TIME 1. COLOR L = fj/tO ? A= vise RVCM I ii i MIDDLE A= i. i i END Particle Size Distribution: Screen Analysis Mesh Size 40 Min On Rotap shaker. 49 gms. Resin pilus 1.0 grns. Carb 60 80 100 120 140 200 Glassy Pan Part. Gross Wt. Tare Net Wt. % on Mesh i>. a? L37 0, O *7 tf&.y' 36*e> /. 7te 0 tS ST? Kg' it* Screen Analysts Min. On Rotap shaker 49 gms. Resin plus 1.0 gnus. Carb Mesh Size Gross Wt. Glassy Pan Part. 40 60 80 too 120 140 200 Tare Net Wt. % on Mesh 1 1 ----- - Remarks. 'hiia** ^ Star 207A Revised 1/12/87 l m .-l. u .. ' KIW- inh 01198123 ** Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERT I F" I CATE - Date: /Z-,-<?/ Customer: United Technologies P. 0. Box B07 fit. Airy, NC 27030 Attention: Quality Control Manager ANALYSIS *Jni VISIAProduc t: 5415 Trai1er No.: /UflrrxAcic Order No . : ODO^S 1*1- 00O Ship Date: /2--3 Customer P.0. No.: Property Moisture, 7. Contamination, BLK/BRN Hard Particles @ 7 mins. Bulk Density, gm/cc Test Method ABR 1A ABR-5A ABR-12 ABR-2B Analysis . o& 15/ 7 l .V78 Brabender Drytime, mins. Resin Flow Time, tap/sec. Particle Size, 7. on 40 Mesh 200 Mesh Pan ABR-7 ABR-8 ABR-3 ___50 o , f.a 0-0 5:3 /.s" Residual VCM, ppm Inherent Viscosity METS IR, 7. of Control ABGC-26 ABR-10 ABR-13 ,0lC? /.OS a4 , ** Values for this property has been determined by our SQC Program and is not tested on truck shipments. Labo y Supe (601) 369-8111 sor/Lead + mm pi e 111 * I ! VAB.0001198124 Tt; AMy S^6 U) C<- TH-is n A s/Vi^Att>/C $e AtA-Ofr 1~H* ^6^ h- Ai />C My C&A- Tt> WIRE ME DATE 7A is MPT. -rt-M-0 K- CAC TERMINAL! ATTENTION i fblDS I (^ | (0 NJ I PLEASE NOTE THE FOLLOWING ORDER: SHIP TO* tlwf +14. Te-C^ yjo j Z>^.)'e. i Co PRODUCT t S"ll P.O. K,r/ <\Ao w.a.+ a t> (a. , \)cy sr ftiOJ-ja.piJC &sI*a QUANTITY J 0C*O / t?5 DELIVERY DATE: i ^ /*! /*\ * DELIVERY TIHB: VISTA ORDER #: >>0 CUSTOMER P. 0. #1 tT 7 H 0 VBIA ACCT. NO. / SPECIAL INSTRUCTIONS: ? V$ .C*n.r*`ir% U4c. uI j u .'pp r\A. 'i { A. f*> . CM IF YOU HAVE ANY QUESTIONS CONCERNING THIS OfcDER, PLEASE CALL ME* /VH MARVA NELSON PVC CUSTOMER SERVICE 1-800-231-8212,' EXT. 3407 FAX #: 713-588-3429 * RCR.038/lf nss foM, 14 T0d 12T8 :0N 131 VAB.0001198125 Hit? SlfcJOIUI3H0 bisinsai S0:T T6<-90-030 ifHffi Vlit Poly--r Load Date: //?-/r~- ?/ Time Logged Ship Date: >-** , High--jr 2E ** V . * . *- v; A h. 'V HT 09730: / * Product: 5415 Car No PLCf *6 - Logged In By: Ai^<J 1st 2nd 1st 2nd 1st 2nd 1st 2nd Moisture *8 T HContamination j Bulk Density m BD wo/antistat Hard Particle Viscosity r jf /| __/ * //\ I1 /.Pols' '' RVCM 1 .Ol0> MO Screen Analysis Mesh 40 t/c* i ght X 0,00 OO 60 80 100 120 140 fcfto 70 &'I Pan 0.9-3 L_ Drytine: Static Flow: Avg. Microns: Color L: J3- b NETS Technician: VAB.0001198126 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 i c^*r OF ANALYSIS h Date: October 25, 1991 Customer: Attention: United Technologies 511 Hay Street P.O. Box 807 Mt. Airy, NC 27030 Quality Control Manager Date of Shipment: October 24, 1991 Product: 5415 Railcar No.: PLWX 44351 Order No.: 0002802-000 Customer P.0. No.: 050-01716 Prooertv Volatiles, 7. Bulk Density, GM/CC Brabender Dry Time, Mins. Particle Size, 71 on 40 Mesh 200 Mesh Pan Vinyl Chloride Monomer Inherent Viscosity Hard Particle @ 7 Min Contamination, BLK/BRN METS IR, X of Control Test Method ABR-1A ABR-2B ABR-7 ABR-3 ABGC-26 ABR-10 ABR-12 ABR-5A ABR-13 Analysis 0.02 0.493 5.0 0.00 3.3 0.6 0.001 1.02 6 5/7 124 Laboratory Supervisor/Lead VAB.0001198127 =1 + i Vista ftliwra Load Date: Ship V *h MT 39T30 h ANALYSX S Analysis Mesh t/o i gh t 40 % 60 100 a(p.& Drytime: Static Flow: Color L: & NETS . 96 2-0 120 140 200 Avf. Microns b /Z Pan <* t Technician: hi VAB.0001198128 Viata Pelyaars lldnrV Abardaair, MT 3T30f ^ * Load Date: Time Logged Ship Date: Product: Car No.; Logged In By: Silo(s) Customer Screen Analysis Mesh 40 60 80 100 W* i ght % Drytime: Static Flow: Color L; NETS: 120 140 200 Pan Avg. Microns: b Technician: VAB.0001198129 , ** Vista Polyman A Division of Vista Chemical Company Highway 25 Post Office Bon 91 Aberdeen, Mississippi 39730*0091 Phone (601) 369-8111 LETTER OF CERTIFICATION Date: October 11, 1991 Customer: Attention: United Technologies 511 Hay Street P.O. Box 807 Mt. Airy, NC 27030 Quality Control Manager Date of Shipment: October 8, 1991 VK1AProduct: 5415 Railcar No.: PLCX 42984 Order No.: 0002419-000 Customer P.O. No.: 050-01651 Property Volatiles, X Bulk Density, GM/CC Brabender Dry Time, Mi ns Particle Size, X on p 40 Mesh 200 Mesh Pan Vinyl Chloride Monomer 4 Inherent Viscosity Hard Particle 8 7Min Contamination, blk/brn METS IR, X of Control Test Method ABR-1A ABR-2B ABR-7 ABR-3 ABGC-26 ABR-10 ABR-12 ABR-5A ABR-13 Analysis 0.11 0.493 4.9 0.00 5.8 1.8 0.028 1.01 1 4/ 8 118 Vj-M-iJa pi j to-- : HPHiSHh-- II Nltfi i i- VAB.0001198130 Viata Polymers Highway 25 * Aberdeen, MS 39730 * Load Date: Product: Car No.: Time Logged In: Logged In By: Ship Date: Silo(s): 00/657 Customer: coozt+rt Moisture Contamination 1st [ 2nd I 1st I 2nd I 1st 2nd 1st 2nd o'? 1 1 *t( 1 .o' Bulk Density wo/antistat Hard Particle vie Viscosity RVCM 02$ Screen Analysis Mesh Weight 40 X 60 Drytime: 402. 80 100 <??.01 120 140 200 2 9 2-* Pan 3 ZZ Static Flow: ^ ^7 Avg. Microns: /&2L* ( Color L: f METS : --L b /-// Technician: VAB.0001198131 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-811 I ^ ffi September 26, 1991 Customer: Attention! United Technologies 511 Hay Street P.0. Box 007 Mt. Airy, NC 27030 Quality Control Manager Date of Shipment: 6 Sept. 91 VISIAProduct: 5415 Railcar No.: UTCX 46474 Order No.: 0001944-000 Customer P.0. No.: 050-01599 Property Vo 1 a t i 1 es , 7. Bulk Density, GM/CC Brabender Dry Time, Mins. Particle Size, V. on 40 Mesh 200 Mesh Pan Vinyl Chloride Monomer Inherent Viscosity Hard Particle @ 7Min Contamination, blk/brn METS IR, 7. of Control Test Method ABR-1A ABR-2B ABR-7 ABR-3 ABGC-26 ABR-10 ABR-12 ABR-5A ABR-13 Analvsis 0.12 0.506 5.0 0.00 6.1 1.7 0.001 1.02 1 3/ 15 124 dQwe Laboratory Super r/Lead VAB.0001198132 > * Land Ontm Alp Senmn ^nmJLyttjLjg Hash MrriJxt i X. 40 Orrci TMmics i VAB.0001198133 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 ETTER OF CERT I F I CAT I ON * Date: 11 Sept. 91 Customer: Attention: United Technologies 511 Hay Street P.0. Box 807 fit. Airy, NC 27030 Quality Control Manager Product Railcar No. Order No. - VK1A VIPX 45871 0001636-000 Date o-f Shipment: 6 Sept. 91 Customer P.0. No.: 050-01560 Propertv Test Method Vo 1 a t i 1 es , */. ABR-1A Bulk Density, GM/CC ABR-2B Brabender Dry Time, Mins ABR-7 Partic1e Size , V. on ABR-3 40 Mesh 200 Mesh Pan Vinyl Chloride Monomer ABGC-26 Inherent Viscosity ABR-10 Hard Particle @ 7Min ABR-12 Con tarnina tion , b1k/brn METS IR, 7. of Contro1 ABR-5A ABR-13 Ana lysis 0.13 0.494 5.1 0.00 5.4 1.6 0.001 1.01 3 5/ 8 113 Laboratory Supervisor/Lead VAB.0001198134 Ijppll WH -Mrty'iiy .*. ' '-,W; ;Iih^- ^ *** 1! hr M |H I- 'I ^ V- Hafc:_2 Ship 4lf tPVWipiH^Nf *: ... " i toff; -" - ajij:. I14? ''SatjlfSiiijiSjii.-JW. j;lr; . ; y*v . -i:- ,: :. ; i ' + >, f<h .1 : fe 4 si rt-- * f- - 3aman Annlymim Hash 40 MffiyliC #d 33-7 o"2_ Oryti 00 Static Float Color U '>./ i fccImtciMi /A i i i VAB.OOOl 198135 Customer Technical PVC BULK TRAILER ANALYSIS Trailer Order 4 Particle Size Distribution Scrami Analyst* On flotap shafcar. 40 gras. Rasin plus t.O gms. Carte Mas* Size 40 Gross Wt Tara Nat Wt H on Masli 4>.DO o.qo Scrasn Analysis 100 120 140 /2.M /L.ca //.cJ SJS 3.u> 0.7 2LS M7 Min. On Rotap shafcar 40 gms. Rasin plus 1.0 gms. Cat /oy / Masli Six* Wt Tara Nat Wt % on Masli 40 100 120 140 Remarks Star 207A nasisad 1/12/ar *! 98136 A OMAw LSTTBR OW CERTIFICATION Date: J Product: 5415 Customer: Attention: United Technologies 511 Hay Street P. 0. Box 807 Mt. Airy, NC 27030 Quality Control Manager Code No.: HMS-XK-21 Trailer No.: 7* Order No. : 0CO Date of Shipment: ^ & "?/ Customer P.0. No.: 600 Moisture, % Igg&JIfijthsd ABR-1A Analysis jS Bulk Density, gm/cc 8.405 Brabender Dry Time, Mins. 8.450 Particle Size, % on 8.300 40 Mesh 200 Mesh Pan ./ Residual VCM, ppm Inherent Viscosity 8.955 8.600 Not more than 5.0 PPM / Hard Particles Q 7 min Contamination, blk/brn METS IR, % of control ABR-12 ABR-5A ABR-13 / /sls * Values for this property have been determined by our Statistical Quality Control Program and do not represent an actual analysis of a sample from this shipment. 4 Laboratory Supervisor/Lead VAB.0001198137 -r Visto Polyman A Division of Visto Chemical Company Highway 25 Pint Office Box 9! Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 Date: <7--S VBIA Product: 5415 Customer: Attention: United Technologies 511 Hay Street P. 0. Box 807 Mt. Airy, NC 27030 Quality Control Manager Code No.: HHS-XK-21 Trailer No. : *2. t Order No.: Date of Shipment: Customer P.0. No.: OSO^Ol^UO Property Moisture, X Test Method ABR-1A . Dt Bulk Density, gm/cc Brabender Dry Time, Mins. 8.405 8.450 S. 0 Particle Size, % on 40 Mesh 200 Mesh 8.300 o.o S. (o Pan - !<1 Residual VCM, ppm Inherent Viscosity Hard Particles 9 7 min Contamination, blk/brn METS IR, % of control 8.955 8.600 ABR-12 ABR-5A ABR-13 Not more than 5.0 PPM 1.02. 22/3 I2sr , *Values for this property have been determined by our Statistical Quality Control Program and do not represent an actual analysis of a sample from this shipment. Laboratory Supervisor/Lead VAB.0001198138 PVC BULK TRAILS) ANALYSIS - 9/ Customer 4 7TC, Product MOIST CONT. Bottom GEL Trailer Number. Time /*3o Order BULK DENSITY DRY TIME COLOR lo^Sy vise RVCM FRONT TT TT | 1 1 1. T - .01 - 1,12- L* MIDDLE I1 #2> II K11 VT-a w11 |2- 1 n* 11. I ll. 1 11 1T 1. I END 1I ^* 11 jl f I1 n* -11 7 na 11 H- Particle Size Distribution: Sewn Anaiyaia Mesh Size 40 Groas Wt Tare Net Wt. b-VO % on Meeh i. Screen Analysts Mesh Size Wt Tare Net Wt H on Meeli 40 On Ratap shaker. 49 gate. Resin plus t.O gms. Certo 100 120 140 Gtmy Pan Part. ML 19 Ml 3U 3. /& / 7.9 On Rotap shaker 40 gms. Resin phis 1.0 gms. Certo 100 120 140 ,%C? LI Hid Qlsaey Part. Remarks Star 207A Reeieea 1/12/07 .i_^ --. ----------- ---- - ABHQ01198139 di Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 LETTER OE CERTIFICATION * Date: 26 Aug. 91 Customer: Attention: United Technologies 511 Hay Street P.0. Box 807 lit. Airy, NC 27030 Quality Control Manager Product Railcar No. Order No. - VKIA UTCX-46415 0001313-000 Date of Shipment: 22 Aug. 91 Customer P.0. No.: 050-01463 Propertv Test Method Volatiles, 7. ABR-1A Bulk Density, GM/CC ABR-2B Brabender Dry Time, Mins ABR-7 Particle Size , 7. on ABR-3 40 Mesh 200 Mesh Pan h Vinyl Chloride Monomer Inherent Viscosity ABGC-26 ABR-10 Hard Particle @ 7Min Contamination , blk/brn METS IR, 7. of Control ABR-12 ABR-5A ABR-13 Analysis .08 . 511 5.1 0.0 4.6 1.5 .038 1.010 3 12/8 120 Laboratory Supervisor/Lead ""MW* i VAB.0001198140 *^ Screen Analysis Mesh 40 60 60 100 120 140 200 Pan Technician 11 ! f/rWM-- * mmmfmmmrn tm VAB.0001198141 707 VAB.0001198142 Visto Polyman A Division of Visla Chemical Company Highway 25 Post Office Box 91 Aderdeeg Masiwippi 39730-0091 Phone (601) 369-8111 * O IFICA X ONI 8/13/91 Product: 5415 VK1A Customer: Attention United Technologies 511 Hay Street P.0. Box 807 Mt. Airy, NC 27030 Quality Control Manager Railcar No Order No ACFX-41170 0001098-000 Date of Shipment: 8/12/91 Customer P.0. No.: 050-01430 Proper tv Test Method Volatiles, % ABR-1A Bulk Density, GM/CC ABR-2B Brabender Dry Time, Mins ABR-7 Particle Size, 7. on ABR-3 40 Mesh 200 Mesh Pan Vinyl Chloride Monomer ABGC-26 Inherent Viscosity ABR-10 Hard Particle @ 7Min ABR-12 Contamination, blk/brn ABR-5A METS IR, 7. of Control ABR-13 Analysis 0.21 0.511 5.1 0.00 3.1 1.3 0.005 1.03 2 4/5 121 4 1 H.D. Lucas Laboratory Supervisor/Lead VAB.0001198143 Vista- Pblyners PVC Highway 25 4 "r?r ' :?u. ^ ; ? vt 'h. *** s*.t: ` " Aberdeen. MST 39730 1t y- RAILCAR ANALYSIS Load Date: Tine Logged Ship Date: mm Product:I 5415 Car No.: /foo Logged In By:. Silora): Cue to 4//7o NO 'T'fl&f* Screen Analysis Mesh Weight % 40 O. OO o.O 60 X/s .3 80 ~ 100 120 g-g.g 140 200 Pan /sSY- 0.Vh 3.1 ____UL Drytine: :/ Static Plow: Avg. Microns : nil a Color L: /*/*/ <Z0& b l-e NETS: t Technician: VAB.0001198144 Vista Potymws A Division of Vista Chomkoi Company Highway 25 Post Orac* Box 91 39730ALa|m|u|| ly|s^^i|M Phono (601) 369-8111 LETTER OF- CERTIFICATION 7/31/91 Product: 5415 VEt\ Customer: Attention: United Technologies 511 Hay Street P.0. Box 807 Mt. Airy, NC 27030 Quality Control Manager Railcar No-: ACFX--41137 Order No.: 0000847-000 Date of Shipment: 7/30/91 Customer P.0. No.: 050-01369 Prooertv Test Method Volatiles, 7. ABR -1A Bulk Density, GM/CC ABR --2B Brabender Dry Time, Mins. ABR -7 Particle Size, 7 on ABR -3 40 Mesh 200 Mesh Pan Vinyl Chloride Monomer ABGC-26 Inherent Viscosity ABR--10 Hard Particle @ 7Min ABR--12 Contamination, b1k/brn ABR--5A METS IR, 7. of 1Control ABR--13 Analysis 0.16 0.491 5.0 0.00 5.9 1.7 0.017 1.01 3 H.D. Lucas Laboratory Supervisor/Lead VAB.0001198145 < *> \ Load Oats 7- 2 7-9 TIse Lagged Oats: Lagged La If Screen Analysis Mesh Weight 40 60 80 100 X Drytioe; Static Flow* Color L HETS: Teehnt cian 120 140 200 Pan Av* Microns a t 4* VAB.0001198146 ? Screen Analysis Mesh 40 80 SO -- _0.IJ us"7 too it.<3 * -JL__ o- 3 ,-27/ 33./ *' aRHeNMNiHO anMHMHi 120 lips' S. 22.0 140 H.93 200 1.9S 9.9 MneMHHS .9 Pan o.gy /, 7 Drytlee: ^>p Stsfcic Fleer & /MZ AV(, (Herons; />&. Color L; /tifoo a ^ 7 b / o1/ NETS: *?*?{ / /2j~Sx> Technician: ^ a V-c^O ^.--- .v -iIHiOii^T VAB.0001198147 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730 Phone (601) 369-8111 4 LETTER OF CERT X X I CDM Dates 7/22/91 Product: 5415 VB1A Customer: Attention: United Technologies 511 Hay Street P.0. Box 807 Mt. Airy, NC 27030 Quality Control Manager Railcar No-: ACFX-41167 Order No-: 0000591--000 Date of Shipments 7/19/91 Customer P.O. No.: 050--01309 Prooertv Test Method Volatiles, 7. ABR-1A Bulk Density, GM/CC ABR-2B Brabender Dry Time, Mins . ABR-7 Particle Size, 7- on ABR-3 40 Mesh 200 Mesh Pan Vinyl Chloride Monomer ABGC-26 Inherent Viscosity ABR-10 Hard Particle @ 7Min ABR-12 Contamination, blk/brn METS IR, 7. of Control ABR-5A ABR-13 Oo ft o Analvsis 0.12 0.502 5.0 3.8 1.4 0.019 1 .of 3 4/ 12 111 H.D. Lucas Laboratory Supervisor/Lead VAB.0001198148 A Load Data: Tim Logfed Ship Date: Product:/ 54X1 Lowed In fljr: Silo(s) Gkist Q0<0 HCFX Moisture Contamination 1 *** I 2nd 1 1st 1 2nd f let 1 2nd I 1st 1 ^1 1 ./gl [ I ,<p? 1 I ' o&> I3 1 I Y' I I I 11 2 [ 1t> | 1 ^1 1 T~ 1 Bulk Density 1 .^7 I . I 11 ( .</*? BD t#o/antistat 1 1 1 1 1r T 1 Hard Particle 2nd Viscosity HVCM /. Q6> /^6 Screen Analysis Mesh 40 Weight OH 100 120 140 200 3S7 31* 3. e Pan Dryt lm ^5"/ ) Static Floe: AVf . Microna : /7// Color L: 0 .0$ METS; Technician: VAB.0001198149 % Vnlo Polyman Hiahwov 25f fll|MWwP IMF Adnwdian, Mimmippi 39730-0091 A Diviaion of Post Omea Box 91 Phono (601) 369-8111 Vista ChomicaJ Company 4 LETTER OR CERTIFICATION Date: 6/25/91 Product: 5415 VBIA Customer: Attention: United Technologies 511 Hay Street P.0. Box 807 Mt. Airy, NC 27030 Quality Control Manager Railcar No.: PLWX-44726 Order No.: 0000333-000 Date of Shipment: 6/24/91 Customer P.0. No.: Property Test Method Vo 1 a t i 1 es, X ABR-1A Bulk Density, GM/CC ABR-2B Brabender Dry Time, Mins. ABR-7 Particle Size, 7. on ABR-3 40 Mesh 200 Mesh Pan Vinyl Chloride Monomer Inherent Viscosity ABGC-26 ABR-10 Hard Particle 0 7Min ABR-12 Contamination, blk/brn ABR-5A METS IR, X of Control ABR-13 Analysis 0.21 0.510 5.1 0.00 3.4 1.3 0.028 1.01 1 8/ 2 110 H.D. Lucas Laboratory Supervisor/Lead t VAB.0001198150 ** '-Hf If - T 4 Date: f * * >i i ** *\ > >* *w < -v y Screen Analysis Mesh 40 Meight X q.qQ 0.0 60 60 100 120 140 200 Pan 2o.as~ H2& '7-c)S' ?.3 /. 7/ 0, Q> (0 SSM / / AH Drytiae; sn Static Flow: Color L; a ~Oc(Tl b Ave* Microns / MCTS: t ** Technician: / >-.**#<# H**-**! VAB.0001198151 VUaMynMn ADMionoi VWa Owmicai Company Ar 39730 nUmUrnaSSR (? Date: (r -2>3 ( Product: Customer: Attention: United Technologies 511 Hay Street P. 0. Box 807 Mt. Airy, NC 27030 Quality Control Manager Code No. Trailer No. Order No. Date of Shipment: Customer P.0. No. HMS-XK-21 &oo -0/3.S o VJ Test Method Aaalza.jg Moisture, % ABR-1A * eO 7 Bulk Density, gm/cc 8.405 -/ Brabender Dry Time, Mins. 8.450 -3*& Particle Size, % on 8.300 40 Mesh 200 Mesh a* e 9, 7 Pan Residual VCM, ppm 8.955 Not more than 5.0 PPM Inherent Viscosity 8.600 Hard Particles Q 7 min ABR-12 Contamination, blk/brn ABR-5A METS IR, % of control ABR-13 ^Values property have been determined Statistical Quality Control Program and do not res an actual analysis of a sample from this shipment. Laboratory Supervisor/Lead VAB.0001198152 PVC BULK TRAILBI ANALYSIS A not# 6 Customer Technic -5 / Product Silo___ C9o Trailer Number Time "Z 4*0 0 Order 1ZJ FRONT MOIST Bosom \.......... CONT. Bosom /(, GEL '<A jps BULK DENSITY i. ,Co 1 2. 2. 1 I2* 2. DRY TIME 1. r", o 2. COLOR vise RVCM A1 B * A /-T I [Zo FT I T 11. 1. 1. L- I MIDDLE 1 2. I1 *1 2* '|2. rr | fT. 11 \2. 1. END 2. 1 |2. 1 I2' 1 2. * 1. 2. AN 1 B- 1 L- 1 A* I B- 1 1 I I Particle Size Distribution Scvmii Analysis /O JMsflftSla On notap shafcsr. 40 Rosin plus 1.0 gms. Carti Mash Stas Gross Wt Tars Nat Wt % on Mash Scrsan Analysis 40 4, *0 Mash Sits Gross Wt. Tara Nat Wt H on Mash 40 100 120 140 12 A d 3f.Z- On Rotap shaksr 49 /A flL, A 7/ t z.jr +,7 Rosin plus 1.0 gms. Carti 100 120 140 *90 Glassy Remarks Star 207A RavisaO 1/12/97 Vista Polymors A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 i I CZ&'T I OM Date: 20 June 91 Customer: Attention: United Technologies 511 Hay Street P.0. Box 807 Mt. Airy, NC 27030 Quality Control Manager Product Railcar No. Order No. 5,15 VISTA PLCX-43B65 0000228--000 Date of Shipment: 12 June 91 Customer P.0. No. 050-01215 Property Test Method Volatiles, V. ABR-1A Bulk Density, 6M/CC ABR-2B Brabender Dry Time, Mins. ABR-7 Particle Size, V. on ABR-3 40 Mesh 200 Mesh Pan Vinyl Chloride Monomer ABGC-26 Inherent Viscosity ABR-10 Hard Particle <3 7Min ABR-12 Contamination, blk/brn METS IR, V, of Control ABR-5A ABR-13 O O Analysis . 19 .507 4.9 2.5 1.2 .212 1.02 1 5/8 119 Laboratory Supervisor/Lead i VAB.0001198154 Vista Polyatrs Highway 25 Aberdeen* MS 39730 Load Date : S / Product: j 5415 Time Logged In: /O Logged In By; / Screen Analysis Mesh 40 Weight 0-& 60 /-2 80 100 23- 77 ^7.S 28-& 120 z. /3s? 140 2SL, ^0 200 Drytine: ^ Static Flow: Color L: Myg -0-0* b Avg Microns: METS: Pan Technician: /*? 1 v* ft VAB.0001198155 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 1 I-- ETTER OF CERT I I X 0|SJ Date* 3 June 91 Customer: Attention: United Technologies 511 Hay Street P.O. Box 807 Mt. Airy, NC 27030 Quality Control Manager Product; 5,15 VISTA Railcar No.; GACX-73398 Order No.: 891333-020 Date of Shipment: 31 May 91 Customer P.O. No.: 050-01176 Propertv Test Method Volatiles, 7. Bulk Density, GM/CC ABR-1A ABR-2B Brabender Dry Time, Mins . ABR-7 Particle Size, 7. on ABR-3 40 Mesh 200 Mesh Pan Vinyl Chloride Monomer ABGC-26 Inherent Viscosity ABR-10 Hard Particle 7Min Contamination, blk/brn METS IR, of Control ABR-12 ABR-5A ABR-13 Analvsis 0.12 0.502 5.0 0.00 3.9 1.3 0.030 1.03 2 8/ 29 111 Laboratory Supervisor/Lead VAB.0001198156 0 * ^Nr b# *-< t TT**? ip* ^.1 - - -ilh. T1- .- *, 1 -*. Highway 25 Aberdeen* MS 39730 F*VC RAILCAR ANALYSIS -/?)( Load Date: Time Ship Date: KM___'_ Product 5415 Car No.: Screen Analysis Mesh 40 W*? i gh t X t>.0 Ao Dry t line: 60 .3/ ,L 80 9C. 7 100 /t.9 / 21. f 120 2.20 n.o 140 LX 200 A 13 J. ? Pan /, 3 Static Flow: 0 /7.9 Avg. Microns:: nz^ Color L: f&*>' W a b ASt METS: Technician: % VAB.0001198157 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601} 369-8111 ifi i or\j Date: Customer: Attention 20 May 91 United Technologies 511 Hay Street P.0. Box B07 Mt. Airy, NC 27030 Quality Control Manager Produc t Railcar No. Order No. Date of Shipment: 17 May 91 Customer P.0. No. "" VISTA VIPX-45878 891333-019 050-01126 Propertv Test Method Volatiles, 7. ABR-1A Bulk Density, GM/CC ABR-2B Brabender Dry Time, Mins. ABR-7 Particle Size X on ABR-3 40 Mesh 200 Mesh Pan Vinyl Chloride Monomer Inherent Viscosity Hard Particle @ 7Min Contamination, blk/brn IR* X of Control ABGC-26 ABR-10 ABR-12 ABR-5A ABR-13 Anal y 0.14 0.507 5.1 0.00 3.6 1.3 0.054 1.02 2 4/ 7 117 # VAB.0001198158 Vista Polymers Load Date: Time Logged Highway 25 Aberdeen. MS 39730 1 ! RAILCAR ANALYSIS Product: 5415 Car No.: Screen Analysis Mesh 40 Weight O. & % OP 60 .7 80 100 120 *3*/ J/-7 /7. / 140 200 /- ?8 3-C, Pan /--? Drytime: JL Static Flow: /D Avg. Microns: $ Color L: !OQ 70 a " O-Q'7 b AJ7 , <?2 V, Hi- f METS % Technician: Cj^/- 7 VAB.0001198159 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 LETTER OE CERT X E X CAT X ON Date: 25 Apr. 91 Product: 5415 Customer: Attention: United Technologies 511 Hay Street P.0. Box 807 Mt. Airy, NC 27030 Quality Control Manager Railcar No. : ACFX-41156 Order No. : 891333-018 Date of Shipment: 23 Apr. 91 Customer P.0. No.: 050-01056 Volatiles, % ABR-1A Bulk Density, 6M/CC ABR-2B Brabender Dry Time, Bins. ABR-7 Particle Size, % on ABR-3 40 Mesh 200 Mesh Pan Vinyl Chloride Monomer Inherent Viscosity ABGC-26 ABR-10 Hard Particle @ 7Min i | Contamination, blk/brn METS IR, % of Control ABR-12 ABR-5A ABR-13 0.18 0.505 4.8 0.00 4.2 1.5 0.032 1.01 5 19/ 116 Laboratory Supervisor/Lead VAB.0001198160 Vista Polymers Highway 25 Aberdeen, MS 39780 Load Date : 1 9/ Product: 5415 Time Logged In: Logged Ship Date: Silo(s) Car No. By: Customer: * 06o 1st 2nd 1st 2nd 1st 2nd 1st 2nd Moisture Contamination ? Bulk Density BD wo/antistat J8 >7/ 3z. It t Z2. .*(? /& 3+ Hard Particle Viscosity RVCM Screen Analysis Mesh 40 Weisht Q~GO 60 80 0.20 /6? J3 * 2 100 120 140 /5S/ /OJ>Z 20$ zbo 200 2./o Pan A* Drytime: Static Flow: ^ Color L: /*- & a b Avg. Microns: METS: Technician: VAB.0001198161 Vista Polymen A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 IFIC I ON VIS[\Date: Product: 5415 Customer: Attention: United Technologies 511 Hay Street P.0. Box 807 Mt. Airy, NC 27030 Quality Control Manager Railcar No.: ACFX-41148 Order No.: 891333--017 Date of Shipment: 3-21-91 Customer P.0. No.: 050-00979 Property Test Method Vo 1 a t i 1 es , '/. ABR-1A Bulk Density, GM/CC Brabender Dry Time, Mins. w~ Particle Size, '/. on ABR-2B ABR-7 ABR-3 40 Mesh 200 Mesh Pan Vinyl Chloride Monomer ABGC-26 Inherent Viscosity Hard Particle @ 7Min Con tamination, b1k/brn METS IP, 7. of Control A8R-10 ABR-12 ABR-5A ABR-13 Ana 1vsis 0.11 0.506 4.9 0.00 3.7 1.3 0.038 1.02 3/ 2 117 H.D. Luc as Laboratory Supervisor/Lead VAB.0001198162 Vista Polymers Highway 25 Aberdeen, MS 39730 Load Date: Product: Car No.: 4/H-f . Time Logged In: &ZI 6 & Date: ~ Logged In By: Customer: LLbBxdL ~Tcd^\ Screen Analysis Mesh 40 Weight 0. 00 % p.o 60 .-57 1* ^ Drytime: iia_ 80 /<?. 43 39,^ 100 mi 120 /</ Static Flow: ^ / /& 140 200 Pan 3.3? llL 7.1* 3.7 1,3 J72-JAvg. Microns: Color L: JPDa b fi METS: % Technician: VAB.0001198163 AOMaianef +\ t lipiPw w tot Onto* Boat 71 Atodw Mil.ippi 37730 Pham (601) 3694m A v LETTER OB' CERTIFICATION ,**. * Date: VISTA Product: 5415 Customer: Attention: United Technologies 511 Hay Street P. 0. Box 807 Mt. Airy* NC 27030 Quality Control Manager Code No Trailer No Order No BH8-XK-21 035^2 -CO/ Date of Shipment f Customer P.0. No ^6>T M>, Analysis Moisture, % ABR-1A Bulk Density, gm/cc 8.405 Brabender Dry Time, Mins 6.450 Particle Size, % on 40 Mesh 8.300 &.CO 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Hard Particles 9 7 min 8.955 8.600 ABR-12 Not more than 5.0 PPM / o/. p% JZ Contamination, blk/brn METS IR, X of control ABR-5A ABR-13 / /_/& a determined Statistical Quality Control Program and do not represent an actual analysis of a sample from this shipment. Labors y Supervisor/Lead * VAB.0001198164 4^ * * ** - * r> H A VAB.OOOl 198165 Vista Polyman * A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 h I R* I CC I OM Date: 3-11-91 Product: 5415 VIS1A Customer: Attention: United Technologies 511 Hay Street P.0. Box 807 fit. Airy, NC 27030 Quality Control Manager Railcar No.: UTCX-46570 Order No.: 891333-016 Date of Shipment: 3-8-91 Customer P.0. No.: 050-00940 Proper ty Test Method Vo 1 a t i 1 es , 7. + ABR-1A Bulk Density, GM/CC ABR-2B Brabender Dry Time, Mins. ABR-7 Particle Size, */. on 40 Mesh ABR-3 200 Mesh Pan Vinyl Chloride Monomer ABGC-26 Inherent Viscosity ABR-10 Hard Par tic1e & 7Mi n Con tarnination, b1k/brn ABR-12 ABR-5A METS IP, V. of Control ABR-13 Analysis 0.12 0.498 4.8 0.00 1.1 0.040 1.02 4/ 2 117 if* H . D . Lucas Laboratory Supervisor/Lead + * VAB.0001198166 Vista Polymers 1 . - .X'* -* -44 ^ ''*" * -. <-' l .* -j. \ , f -s-i -V ' k .' ||J V 11 ,*'1 . ' V*1' t - ** 'wr>, v I V * *\ I ' *4 * * .' Highway 25 Aoer deen, MS 39730 Load Date: Time Logged Ship Date: LL 7<-X Product 5415 Car No>: US 7* y V, Logged In By: S i 1o (a): _S3St-L2jL . UTdCustomer: i r^J T~ Ate b a (c 1st , 2nd I 1st I 2nd 1st 2nd Moisture Contamination . f cs> ri Z~- \i 1X Mm | 3l | ,/2-~ j ? "" 2/"'' I cf Bulk Density 1 sfoo __________1. (S9z> 1__________1 BD wo/antistat Hard Particle 1st 2nd Viscosity RVCM Screen Analysis Mesh Weight X 40 a> >o oto 60 80 100 /j Sf< (& Drytime: SS8- Static Flow: 120 4S2 /J-o 140 <</ 200 S- 2- Pan ,3& LL Avg. Microns: Us./ Color L: METS: 9./ b Technician: VAB.0001198167 Tmw r vifftWI A Pivmoo of Vbto Qitmicol Compony Highway 25 Part Oma Box 91 Admlna AMi^ppi 397304091 PIwm (601) 369-6111 + j TOr FROM: DATE: SUBJECT: All Vista PVC Resin Customers Jim Edwards 2/14/91 PVC Resin Particle Size Analysis Vista's Aberdeen PVC Plant Q C Lab has changed the equipment used for particle size analysis. The change is from wire mesh sieves to Electroformed Precision Sieves. ASTM E 11-70 for wire sieves allows 5 to 19 Mm tolerances for openings 200 to 40 mesh respectively. Precision screens offer tolerances 2 Mm for all mesh sizes in that range. This change will not affect our resin's physical properties. There will be a slight change in the reported mesh distributions. The fine and the coarse ends should stay the same or decrease slightly. The middle screens will appear to be more peaked depending on the resin type. Testing has found the wire mesh sieves to be less accurate than the Precision Sieves, allowing oversized resin to pass through to a smaller sieve. The oversized resin slipped through openings made too large by shifting wire mesh. An Experimental Design was recently performed on the resin particle size variation at the Aberdeen Plant. The data showed: 85% of the variance was attributed to the Process 14% of the variance was attributed to the Testing 1% of the variance was attributed to the Sampling The change to Precision Sieves will help reduce the variance attributed to Testing. This will allow better analysis of actua i process variation. If you would like to discuss this change further please call. Sincerely. Jim Edwards Chief Plant Chemist (*30i-;t69-:i8fi7> VAB.0001198168 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 397304)091 Phone (601) 369-8111 I I OISJ * Date: 18 Feb. 91 Product 5415 Customer s Attention United Technologies 511 Hay Street P.0. Box 807 Mt. Airy, NC 27030 Quality Control Manager Railcar No. Order No. UTCX--48050 891333-015 Date of Shipment: 15 Feb. 91 Customer P.0. No.: 050-00880 Property Test Method Volatiles, 7. l Bulk Density, GM/CC ABR-1A ABR-2B Brabender Dry Time, Mins. ABR-7 Particle Size, 7. on ABR-3 40 Mesh 200 Mesh Pan Vinyl Chloride Monomer ABGC-26 Inherent Viscosity ABR-10 Hard Particle @ 7Min ABR-12 Contamination, blk/brn ABR-5A METS IR, 7. of Control ABR-13 Analysis 0.15 0.511 5.5 0.00 3.2 0.8 0.018 1.02 1 4/ 9 117 Laboratory Supervisor/Lead VAB.00011^8169 Vista Polyasrs Highway 2* | |t Absrdssnf MS 39730 itTX Screen Analysis Mesh Weight X p 40 O. *> Drytiae: 60 0.4- 80 JPlA J5^ 100 /fe 3&-/ 120 /0.63 140 3. 7* 9.4 Static Flow: ^ Avg. Microns: Color L: t<%>-&* a AfS b NETS: Technician: VAB.0001198170 Vista Potymare Highway 25 i*r A Division of Vista Chtmical Company Post Omco Box 91 Aderdoon, Mississippi 39730-0091 Phono (601) 369-8111 A ti%t * a IFI I ON VBIA 30 Jan. 91 Products 5415 Customer: Attention s United Technologies 511 Hay Street P.0. Box 807 Mt. Airy, NC 27030 Quality Control lianag er Railcar No UTCX-46483 Order No.: 891333-014 Date of Shipment: 29 Jan. 91 Customer P.Q. No 050-00816 * - * t1 i ,* - Property Volatiles, 7, Bulk Density, GM/CC Brabender Dry Time, Mins Particle Size, V. on 40 Mesh 200 Mesh Pan Vinyl Chloride Monomer Inherent Viscosity Hard Particle @ 7Min Contamination, blk/brn METS IR, 7. of Control Method ABR-1A ABR-2B ABR-7 ABR-3 ABGC-26 ABR-10 ABR-12 ABR-5A ABR-13 Analysis .21 .508 5.0 0.0 4.0 1.2 Oil 1.01 2, I 118 r1 toy. I II f i I * * -------------Bilay P. Sizemore Laboratory Supervisor/Lead VAB.0001198171 Vista Polymers Highway 25 Date: Ship Date: Aberdeen* MS 39730 Screen Analysis Mesh Weight X 40 Sm 00 AO 60 d.*7 80 100 120 JO. 140 200 m ffio Pan AS#' Drjrtiae: Static Flow: 0 Color L: J*0^t Avg Microns: b J^l METS: Technician: VAB.0001198172 YiSvQ rwVyVTvvfS A Division of Vista Chemical Company Highway 25 PostOfnc Box 91 Aberdeen, Mississippi 39730 Phone (601) 369-8111 4 LETTER OE CERTIEIOATION Date: 21 ft Customer: United Technologies 511 Hay Street P. 0. Box 807 Mt. Airy, NC 27030 Attention: Quality Control Manager Date of Shipment: X/ ?J VIS1AProduct: 5415 Code No.: RMS-XK-21 Trailer No. : Order No. : ier P. 0. No. : 0$~O~ Test_Metho4 Moisture, % ABR-1A Bulk Density, gm/cc 8.405 .?? Brabender Dry Time, Mins. 8.450 Particle Size, % on 8.300 40 Mesh 200 Mesh Pan L Residual VCM, ppm 8.955 Not more than 5.0 PPM Inherent Viscosity Hard Particles 7 min 8.600 ABR-12 MIA I Contamination, blk/brn ABR-5A METS IR, % of control ABR-13 * Values for this property have been determined by our Statistical Quality Control Program and do not represent an actual analysis of a sample from this shipment. Laboratory pervisor/Lead VAB.0001198173 4 PVC BULK TRAILER ANALYSIS Dale. /- gA- 5 / Customer Product Silo Technician MOIST CONT. 1 Tty 1 Batumi || Tup | Bottom \'i2 1. / 1 2?Cl' FRONT GEL Trailer Order BULK DENSITY DRY TIME l. iI 1 MIDDLE liber. COLOR vise RVCM - /re i END iI Particle Size Distribution Screen Analysis Mash Size 40 Cross Wt Tare Net Wt H on Mesh & 0O 6L & Screen Analysis Mesh Size Gross Wt Tare Net Wt % on Mesh 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carts 100 120 140 200 Glassy Pan Part. O'? s?.?* /ss( d.7* Mt. Min. On Rotap shaker 49 gms. Resin phis 1.0 gms. Carta Pan (0 100 120 140 200 Glassy Part. Remarks 7y f Star 207A Revised 1/12/87 VAB.0001198174 Vista Polyman A Division of Vista Chemical Company Highway 25 Post Office Box 91 Adordeen, Mississippi 39730-0091 Phone (601) 369-8111 OF IFI X OM Date: 18 Jan. 91 ... VIS1AProduct Customer: Attention: United Technologies 511 Hay Street P.0. Box 807 Mt. Airy, NC 27030 Quality Control Manager Railcar No. Order No. GACX-73386 891333-013 Date of Shipment: 15 Jan. 91 Customer P.0. No. 050-00727 Property Test Method Volatiles, 7. ABR-1A Bulk Density, GM/CC ABR-2B Brabender Dry Time, Mins. ABR-7 Particle Size, 7. on ABR-3 40 Mesh 200 Mesh Pan Vinyl Chloride Monomer ABGC-26 Inherent Viscosity ABR-10 Hard Particle <2 7Min ABR-12 Contamination, blk/brn ABR-5A METS IR, 7m of Control ABR-13 O t in Analysis 0.10 0.506 0.00 3.1 1.1 0.026 1.02 93 5/ 12 120 Laboratory Supervisor/Lead WP r-*n VAB.0001198175 Vista Polymers Highway 25 tj Aberdeen. MS 39730 * RAILCAR ANALYST Load Date: r(3 Time Logged In : Ship Date: Product: 5415 Car No.: * Logged In By: 3 Screen Analysis Mesh 40 Weight % 0' o 60 o-5i Uo 80 129 4 3*?3 100 f*f' I 120 10. o 9 Jit. 1 140 3s C?, if 200 f.Sf 3. / Pan Or S'? /. / Drytime S'O Static Flow: O /Mr? Avg. Microns: Of."? )0&'H a ~ Ob b h METS: /% Technician: 'ii VAB.0001198176 IT"Ifci'k Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 T I CA Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 ^ INJ ^ V' S I s A Date: November 20, 1991 Customer: United Technologies 800 E. Bridge St. Plainwel1, MI 49080 At ten tion Quality Control Manager Ship Date November 19, 1991 Product: 5415 Railcar No.: VIPX 45815 Order No.: 0003664--000 Customer P.0. No.: 10256 P roper ty Volatiles, 7. Bu1k Density, GM/CC Brabender Dry Time, Mins. Particle Size, 7. on 40 Mesh 200 Mesh Pan Vinyl Chloride Monomer Inherent Viscosity Hard Particle @ 7 M i n Con tamination, blk/brn METS IR, 7. of Con t ro1 Test Method ABR-1A ABR-2B ABR-7 ABR-3 ABGC-26 ABR-10 ABR-12 ABR-5A ABR-13 Ana1ysis . 04 5.0 0.0 6.3 1.7 .001 1.02 2 12/4 121 Laboratory SuperVisor/Lead VAB.0001198178 * it I *sr 1 -i^i" r r' 'r r -I Rilywiiii i + 5 ! 1lift Ml v J -C'C ` * *. '^lfL '-' i * Load Date: Time Logged In Ship Date; ;J t-"7 `*i*. Ii '" ''>**\** Product: ** \iMft r*l- 5415 IW^ KH <o Logged In Ckr No.: %+ By: / A rfV 3 / :< / - ^ i' Screen Analysis Mesh <10 Weight X 1t 0.0 to ^ 60 . >% 27. f 100 /&2f 73^ 120 /o-j* 140 27 f ^ 200 3 Drytime ,o Static Plot#: 22 Avg, Microns: Color L: tOLo^ - <r? fL * /./Z, LMETS;: 3 VS'/ / // Pan i h i! Technician: VAB.0001198179 JJ I Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 LETTER OF CE Date: December 19, 1991 Customer: United Technologies 800 E. Bridge St. Plainwell, MI 49080 Attention: Quality Control Manager Date of Shipment: December 18, 1991 I F I CAT I CDrsj VIS1A Product: 5415 Railcar No.: PLCX 43431 Order No.: 0004951-000 Customer P.0. No.: 10307 Propertv Volatiles, 7. Bulk Density, GM/CC Brabender Dry Time, Mins. Particle Size, 7. on 40 Mesh 200 Mesh Pan Vinyl Chloride Monomer Inherent Viscosity Hard Particle <5 7Min Contamination, blk/brn METS IR, 7. of Control Test Method ABR-1A ABR-2B ABR-7 ABR-3 ABGC-26 ABR-10 ABR-12 ABR-5A ABR-13 Ana 1 y sis 0.24 0.484 4.9 0.00 &*4 1.8 0.009 1.03 3 4/7 117 H.D. Lucas Laboratory Supervisor/Lead * VAB.0001198180 Load Date: Lagged Product: Z<tQ 5415* 4 PLCL)( Car Mo.: 4**3/ Screen Analysis Mesh 40 W? i ijh t > O X 60 80 100 120 140 200 Pan /s/<^>>o (o ft 4 :a <*>*( /0.3 ^ 5^ jL Drytime; Static Flow: O t/'3 Avj. Microns Color L: /PO?/ -<? tx /-2-V NETS ; #/T7 L ULB. 2P Technician: VAB.0001198181 Vista Polyman A Division of Vista Chemical Company Highwoy 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 OF CER I I I ON A Date: October 21, 1991 Customer: United Technologies 800 E. Bridge St. Plainwel1, MI 49080 Attention: Quality Control Manager Date of Shipment: October 18, 1991 VIS1AProduct: 5415 Railcar No.: PLWX 44686 Order No.: 0002726-000 Customer P.0. No. 10153 Property Volatiles, 7. Bulk Density, GM/CC Brabender Dry Time, Mins Particle Size, V. on 40 Mesh 200 Mesh Pan Vinyl Chloride Monomer Inherent Viscosity Hard Particle 7Min Contamination, blk/brn METS IR, 7, of Control Test Method ABR-1A ABR-2B ABR-7 ABR-3 ABGC-26 ABR-IO ABR-12 ABR-5A ABR-13 Analysis .03 .494 4.9 0.0 4.1 1.3 .001 1.02 3 6/7 120 Amy E. Bagwell Laboratory Supe rvisor/Lead iSIlBM 4' U t| 't MIM' VAB.0001198182 Vista Polymers Highway 25 Aberdeen M8 39730 RAILCAR ANALYSIS Load Date: 7- Z%-9! Product: 5415 Car No.: Time Logged In: 0100 10 lift A iShip Date: Silo( s ): Logged In By: ^If/ Customer: ~00> Screen Analysis Mesh 40 Weisjht a>jO %f 60 /.e> r Jt-D 80 100 120 140 200 Pan 2 J?o3 Drytime: #3. Static Flow: O //0> 7 Avg. Microns: / Color L: /Oo -o ? a ~Q-(f b A /*? METS: ^3 / /<?a % *I Technician VAB.0001198183 Vista Mywn A Division of Vista Chemical Company Highway 25 tost Office Box 91 Aberdeen, Mississippi 39730*0091 Phone (601) 369-8111 A R IFIC i oisj Date: 9/18/91 VK1A Customer United Technologies 800 E. Bridge St. Plainwell, MI 49080 Product: 5415 Railcar No.: VIPX 45757 Attention: Quality Control Manager Order No 0001653-000 Date of Shipment: 9/17/91 Customer P.0. No 10050 Property Test Method Volatiles, '/. ABR-1A Bulk Density, GM/CC ABR-2B Brabender Dry Time, Mins. ABR-7 Particle Size, V- on ABR-3 40 Mesh 200 Mesh Pan h Vinyl Chloride Monomer ABGC-26 Inherent Viscosity ABR-10 Hard Particle @ 7Min ABR-12 Contamination, blk/brn ABR-5A METS IR, 7. of Control ABR-13 O in Analysis 0.13 0.493 0.00 4.3 1.4 0.001 1.03 4 4/7 119 H.D. Lucas Laboratory Supervisor/Lead 9 * VAB.0001198184 o 41 .y r'ri:'V^">'" ' "ii-iiij w tI Load OMtmr 9 -/r^y/ Ship rtiB tamari tb* 0/00 *':.' Ir . :ii!ili x*rt* m r :{i;; il.,:v;';":-!lj= v ..ij. <*hmrn ,it U ;. ii> :l > Jit- 'Mi WMa * * ftur fir 3rr /to,; u '/A/aJcJM I 1 f ZM I____ Ire ,| 2nd / i^f [ 2M Ire fr U 1r l /s I JHXT^t mT / r L/ // < y ~] 1 I nr rI. l~l /,yyj/~ 7 / /.^/ L BD Mo/aatlatBt 1 L>7 i *r 1 <Z Smrti h&-h -- / --- / - ^. I m v i r VJLmcamitx 7^5/ --f f ffVOf Scroan AnmJLx*m M*nh thtigfiit 40 <s> o X. too ///S c?c?l 3 m Orrta ftilig Flail fifeiop ^ a r f I VAB.0001198185 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730 Phone (601) 369-8111 L-ETTER OF CERTIFICATION Date: 20 August, 1991 Customer: United Technologies BOO E. Bridge St. Plainwell, MI 49080 Produc t Railcar No. Attention: Quality Control Manager Order No. Date of Shipment: 19 August, 91 Customer P.0. No. VISTA VIPX 45795 0000988-000 5949 Property * Test Method Volatiles, 7. ABR-1A Bulk Density, GM/CC ABR-2B Brabender Dry Time, Mins ABR-7 Particle Size , 7. on ABR-3 40 Mesh 200 Mesh Pan Vinyl Chloride Monomer Inherent Viscosity ABGC-26 ABR-10 Hard Particle @ 7Min ABR-12 Contamination , blk/brn METS IR, 7. of Control ABR-5A ABR-13 Ana 1vsis 0.15 0.501 5.0 0.00 3.0 1.1 0.004 1.02 1 5/ 6 119 / XJf m w/ m JAA-AJ'U Amy E. Bagwell Laboratory Supervisor/Lead VAB.0001198186 rm -I n* *' * 4 4r ViBtai Polymmrm fflSfcMjr 28" Load Tim Ship Screen Analysis Mesh 40 Weigh t Q, 00 X 0.0 60 J.O ,42 r/.o 100 120 r-47 22. 0 Jo. 7 ft 4 140 */ 200 t. o Orytine: r.o Static Flow: Avg. Microns: Color L: 166.12- of k A/7 NETS: Pan . r7 Technician: VAB.0001198187 Vista Polymers A Division of Vista Chemicol Company Highway 35 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OF ANALYSIS Date: AtL&O&T 1^1 Customer: United Technologies 000 E. Bridge St. Plainwell, MI 49080 ,,,, V1SIA Product: m Code No.: RMS-XK-21 Trailer No.: T-V74 Attention: Quality Control Manager Order No.: 00012.50-000 Date of Shipment : Au6UT \c\i Customer P.0. No.: 100/3 Propertv Moisture, V. Test Method ABR-1A Analysis ./z. Contamination, blk/brn Hard Particles @ 7 min Bulk Density, gm/cc ABR-5A ABR-12 ABR-2B A .Sot Brabender Dry Time, min. ABR-07 Resin Flow Time, tap/sec. ABR-OB Particle Size, V, on ABR-03 40 mesh Residual VCM, ppm ABGC-26 SI 0 / 76 200 mesh - 3.5 < _5.0___* Pan LA Inherent Viscosity METS IRf V. of control ABR-10 ABR-13 1-02- * /2b **# Values for this property have been determined by our SQC Program and are not tested on truck shipments. ervisor/Le VAB.0001198188 Due Customer Tedtuktan PVCatlLK MCI CONT FRONT J1 J-----------rr--i--------- E middle |i | ij il l ] END *I p| i -I A Order SULK ocnsity COLOR vise RVCM fen&3 L A- PanicJc Size Oismbuiion: Moalt Star Gran Wl. MM Wt. H on Moon Sewn AntlyiM On fltn On Roup H on Moon Remarks 4 VAB.0001198189 VMoMynwn A Divirion of Vista Chemical Company Highway 25 flostOfnco Bax 91 Phono (501) 359-8111 LETTER OF CERTIFICATION A 7/23/91 Customer: United Technologies 800 E. Bridge St. Plainwell, MI 49080 Product 5415 Railcar No. VIPX-45809 Attention: Quality Coritrol Manager Order No. 0000301--000 Date of Shipment: 7/22/91 Customer P.0. No. 3319 Property Test Method Volatiles, X ABR -1A Bulk Density, GM/CC ABR -2B Brabender Dry Time, Mins. ABR -7 Particle Size, % on ABR -3 40 Mesh 200 Mesh Pan Vinyl Chloride Monomer ABGC-26 Inherent Viscosity, ABR--io Hard Particle @ 7Min ABR--12 Contamination, blk/brn ABR--5A METS IR, V. of Control ABR-13 Analysis 0.21 0.508 5.2 0.00 3.1 1.2 0.027 1.02 3 8/ 5 119 H.D. Lucas Laboratory Supervisor/Lead VAB.0001198190 M :n h, Load Date; Tine Logged Date M ^ ' :' y ^ # v '[x "+ >i ,.i |.iIhi. /.'V,oY-. 3.r! sW` M. t //: j Product;) 54X5 Car No.: Logged In By: //hO^< c A 1st [ 2nd I 1st 2nd 1st 2nd 1st 2nd Moisture Contamination Bulk Density BD wo/antistat ,/? a 0 I lr g | .a/ I7 3 / Hard Particle Viscosity RVCM Screen Analysis Mesh Height 40 > >0 % >,0 60 p p- ao ?IS$ 100 /.7d 120 140 P.9Y 200 Pan /,57 <9. (oPl Drytine; Static Flow: Color L; $A Avg. Microns: b METS: Technician: VAB.0001198191 -------------* *HMW Vista Polymers A Division of Vista Chemicol Company Highway 2 Post Office I Aderdeen, Mississippi 39730-0091 Customer: United Technologies 000 E. Bridge St. Plainwell, MI 49000 Code No.: RMS-XK-21 i 1 er No. : /~ >5 0* Attention: Quality Control Manager Order No.: 00006/3 ~0OO Date of Shipment: /7 SclJy ^/ Customer P.0. No.: Propertv Test Method Ana 1vsis Moisture, 7. ABR-iA Con tarnination , b1k/brn ABR-5A + / S' Hard Particles @ 7 min ABR-12 / Bu1k Den sity, gm/cc ABR-2B Brabender Dry Time, min. ABR-07 . S'/S S'. / Resin Flow Time, tap/sec. ABR-00 0 / 0.3 Particle Size , */. on ABR-03 40 mesh 200 mesh Pan 0.0 / & Residual VCM, ppm ABGC-26 < 5.0 # * * fnherent Viscosity ABR-iO 1.02* # # t METS IR, V. of control ABR-i3 /20 * * * * *# Values for this property have been determined by our SQC Program and are not tested on truck shipments. /V, y super VAB.0001198192 w*1r K- A'-n I tt * to*- M "t' ff T .* #, % l*f '** r: *. * PVC BUUC TFUULBF rtfhALYSST fl Ttailtr OONT. k /% r. FRONT 12. 1 [ 1. I [ 2. 1 I 1. j MIDDLE [7 I 1I 2* |1 [ir I |i. I 1 i fi 7 I fl | 12 Order ULK 08KSITY COLOR L \ 00. >40 o-o? l^o vac IRVCM /ew/ PUrtidc Size Oisiribuckm: 14 4 ?.o^P M on Mooli tcroon Anolyolo I*/0 lf-26 >. C ft. a >4 -Min. On Wotop ohofcor 40 to.H S'OO -2 A? /*. 14 3,cft 0.61 MMfl SIm T H on Moon Remarks 1198193 Vista Polymars A Division of Vista Chemicol Company Highway 25 Post Office Box 91 F-- R Adordoon, Mississippi 39730*0091 Phono (601) 369-8111 ifi o^~r i oini A Date: 22 June 9.1 Customer: United Technologies 800 E. Bridge St. Plainwe11, MI 49080 VBIA Product 5415 Railcar No. GACX-73408 Attention: Quality Control Manager Order No. 0000056-000 Date of Shipment: 14 June 91 Customer P.0. No. 3306 mmaIM H ** *a- M frl 1 Property Test Method Volatiles, 7. ** Bulk Density, GM/CC ABR-1A ABR-2B Brabender Dry Time, Mins ABR-7 Particle Size, 7. on ABR-3 40 Mesh 200 Mesh Pan Vinyl Chloride Monomer ABGC-26 Inherent Viscosity ABR-10 Hard Particle @ 7Min ABR-12 Contamination, blk/brn METS IR, 7. of Control ABR-5A ABR** i 3 Analysis 0.13 0.500 4.9 o. oo 3.2 1.3 0.022 1.02 5 6/ 7 119 Laboratory Supervisor/Lead nirrJi t VAB.0001198194 4 nrI -It' ll. ' I #t ' rf' n-* i v ' tjui. . :vMTy '*:=.......... 14 **1*4 ^ /V ^ J ^ 1 1 Hl| I .,1 , .Mx , 11 N| ,. I .mu-1 !***'' .M"lh *x; ( *.v, \ PVC RAILCAR A*l\A.IL3rS XS --A1, Load Date; W~ \? -^Tl Product: I 5415 Car Mo.: ' >f Tine Logged In: lft>o Ship Date: Silo(a): Logged In t 0 *. (o Chatoner: yp 1 1st J 2nd 1 *st 2nd I 1 2nd I 1st Moisture Contamination I /^f Ij i /* f"J i * /j 1r 1 // 1 n r 2 1 T" / 2. 1 /? Bulk Density I ,SV/I [ , OO 1 BD wo/antistat I - -sa#1 Hard Particle 2nd Viscosity RVCM Screen Analysis Mesh 40 Height X & <o 60 80 100 120 140 200 3fa l^D 23 't: 23 3 /S ?O ?. o 3. Drytime: *LJ Static Plow: Avg, Microns: Color L: f0O ^9 b Pan 7S.3 METS: Technician VAB.0001198195 Vista Polymers A Division of Vista Chemical Company I_EE T" Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 , Phone (601) 369-8111 IFI I OM Date: 16 Apr. 91 Customer: United Technologies 800 E. Bridge St. Plainwell, MI 49080 VB1A Product: 5415 RaiIcar No.: UTCX-46440 Attention: Quality Control Manager Order No.: 883959-019 Date of Shipment: 15 Apr. 91 Customer P.0. No.: 35062 Propertv Test Method Volatiles, 7. ABR-1A Bulk Density, 6M/CC ABR-2B Brabender Dry Time, Mins ABR-7 Particle Size, 7. on ABR-3 40 Mesh 200 Mesh Pan Vinyl Chloride Monomer ABGC-26 Inherent Viscosity ABR-10 Hard Particle @ 7Min Contamination, blk/brnf ABR-12 ABR-5A METS IR, 7. of Control ABR-13 Analysis 0.17 0.513 4.9 0.00 3.6 1.2 0.048 1.03 2 5/ 30 121 Laboratory Supervisor/Lead VAB.0001198196 Vista Polymers Highway 25 * Aberdeen! MS 39730 PVC RAILCAR ANALYSX S ZX117 Load Date:. Product: 5415 Car No. : Time Logged : j 8'Ob Logged In By: Date: Screen Analysis Mesh 40 Weight <Q*Qc> % &< O 60 7'/ Drytime: .9 80 100 120 140 200 Pan n.zo IOS O. <B>0 S*. 4 <3* (o t- a Static Flow: O /ff>3 Avg. Microns . n?.g Color L: '0- 3a h /'3S METS: Technician: VAB.0001198197 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730*0091 Phone (601) 369-8111 I I CAT X CJIVI Date: 17 Apr. 91 Customer: United Technologies 800 E. Bridge St. Plainwell, MI 49080 Produc t Railcar No. Attention: Quality Control Manager Order No. Date of Shipment: 16 Apr. 91 Customer P.0. No. VlSlA 5415 VIPX-45901 883959-018 35019 Prooertv Test Method Volatiles, 7. ABR-1A Bulk Density, BM/CC ABR-2B Brabender Dry Time, Mins . ABR-7 Particle Size, 7. on ABR-3 40 Mesh 200 Mesh Pan Vinyl Chloride Monomer ABGC-26 Inherent Viscosity ABR-IO Hard Particle @ 7Min ABR-12 Contamination, blk/brn METS IR, 7. of Control ABR-5A ABR-13 Analysis 0.15 4.8 0.00 2.9 1.1 1.01 1 3/ 7 120 Laboratory Supervisor/Lead VAB.0001198198 Vista Polyasas Highway- 25 \ vT Aberdeen. MS 39730 Load Date: Product: Car No.: Time Logged In: l9dO Logged In By: T(L Ship Date Silo( s) Customer ? 1st 1 2nd I 1st I 2nd I 1st 2nd I 1st I 2nd Moisture Contamination /0O <*& Bulk Density BD wo/antistat i 3 | hr- // r~ /+ s&S1 1 .SIS \r JZ 3 I 1 ~ \T ,2 1 /> 1 . S7<2 1 JL PT~ H9 1 -S76> Hard Particle Viscosity RVCM Screen Analysis Mesh Weight X 40 >, &,) 60 LA : M. Drytime 80 100 120 140 21.1 /3,Z St 200 Pan /. 2 &7 2.1 // Static Flow: a / zf Avg. Microns: Color L: ab METS : L% Technician: VAB.0001198199 Vislo Polymwn A Division of Vista ChoffMcai Company Highway 25 Post Offico Box 91 AdudiMv MmUppi 397300091 Phona (601) 369*6111 * LETTER OF CERTIFICATION -15-91 Customer: United Technologies 800 E. Bridge St. Plainwell, MI 49080 VISIA Product 5415 Railcar No. PLWX-44723 Attention: Quality Control Manager Order No. Date of Shipment: 3-14-91 Customer P.0. No. 34938 Property Test Method Volatiles, 7. ABR-1A Bulk Density, GM/CC ABR-2B Brabender Dry Time, Mins. ABR-7 Particle Size, 7. on ABR-3 40 Mesh 200 Mesh Pan Vinyl Chloride Monomer ABGC-26 Inherent Viscosity ABR-10 Hard Particle @ 7Min Con t amin a tion, b1k/brn ABR-12 ABR-5A METS IR, X of Control ABR-13 Analysis 0.12 0.510 4.9 - 0.00 2.1 1.3 0.997 1.03 2 2/ 2 120 H.D. Lucas Laboratory Supervisor/Lead VAB.0001198200 Vista Polymers Highway 25 Aberdeenf MS 39730 RAILCAR ANALYSIS A Load Date: f Product: Car No.: Time Logged In: Logged In By: Ship Date: Silo(s): Customer i. Moisture Contamination Bulk Density BD wo/antistat Hard Particle stv 2nd 2nd 1st 2nd 1st 2nd J_i_____________ 2- Z a- i . /Z. 2- / SO? 1 .s// Viscosity RVCM Screen Analysis Mesh 40 Weight &,C) X ao 60 j.o 80 jz? 100 120 JS- / /#</ 140 -2- 200 t.e>7 Pan .&</ 3* / AL Drytime = Static Flow: / 9-3 Avg. Microns: ^ Color L: a b 64fc. METS: ^3^0 / /2t>, Q% Technician VAB.0001198201 Vista Polyman A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERT I Aberdeen, Missm^pi 397304)091 Phone (601) 369-8111 I CDM 4 Date: 18 Feb. 91 Customer: United Technologies 800 E. Bridge St. Plainwell, MI 49080 Product: 5415 Railcar No.: GACX-733B9 Attention: Quality Control Manager Order No.: 883959-016 Date of Shipment: 15 Feb. 91 Customer P.0. No.: 34809 Property Test Method Volatiles, 7. ABR-1A Bulk Density, GM/CC ABR-2B Brabender Dry Time, Mins. ABR-7 Particle Size, 7. on ABR-3 40 Mesh 200 Mesh Pan Vinyl Chloride Monomer ABGC-26 Inherent Viscosity ABR-10 Hard Particle @ 7Min ABR-12 Contamination, blk/brn ABR-5A MET5 IR, 7 of Control ABR--13 Analysis 0.12 0.503 5.1 0.00 3.8 1.2 0.044 1.01 1 4/ 117 Laboratory Supervisor/Lead VAB.00011^202 Vista Polymers V!Highway 25 Aberdeen, MS 39730" Load Ship Data: Ar0 m&th&t 1st I 2nd I 1st Moisture Contamination Bulk Density ,// 3 | /o * I 7T | !o L 301 BD wo/antistat Hard Particle Viscosity / 1f RVCM 2nd 2nd 1st 2nd Screen Analysis Mesh 40 Weight &-&U % 60 64 80 J3-3 100 tent 120 140 431 71 200 3-7 Pan L2 Drytime 1 Static Flow: Avg. Microns i it.'? Color L: 100. S3 0 /O b A39 METS: 57/ Technician: VAB.0001198203 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 J* * l t CERT I F I CATE QF YS I S Date: // 9/ .... VIS1A Product Customer: United Technologies 000 E. Bridge St. Plainwell, MI 49000 Code No. Trailer No. RMS--XK--21 Attention: Quality Control Manager Order No. Date of Shipment: /? Customer P.0. No. 3*C?A Proper tv Test Method Analysis Moisture, V. ABR-1A _____ Contamination, blk/brn ABR-5A S' Hard Particles @ 7 min ABR-1 <3 Bulk Density, gm/cc ABR-2B Brabender Dry Time, min ABR-07 .L Resin Flow Time, tap/sec. ABR-OB / Particle Size, 7. on ABR-03 40 mesh 200 mesh Pan Residual VCM, ppm ABGC-26 AO. St if. < 5.0 LL Inherent Viscosity ABR-10 METS IR, V. of control ABR-13 217 %%% %%% Values for this property have been determined by our SQC Program and are not tested on truck shipments. VAB.0001198204 PVC BULK TRAILER ANALYSIS * Hfltp / --/ 7 ^ /_____ Product _________ Trailer Number Y'- Customer /^*/"^_____ Silo ________________________ Time /f) Technician M ^ & Order No. FRONT IMOIST CONT. |Top Bottom Top Bottom GEL % I ( * * i * 4 ft + * * ...... 1 2T BULK DENSITY DRY TIME 1. </ -> COLOR J L/l J. 7^ A = _ 0,64, b - hyf 1. i. 1. l. 1. L= vise MIDDLE 2 i. =A ->n * 1A -> B= 1. 1. 1. 1. L = END 2 2. 1 * "I 1 A- B= RVCM J Particle Size Distribution: Screen Analysis Mesh Size 40 Gross Wt Tare Net Wt % on Mesh 0-60 o. On Screen Analysis Mesh Size Gross Wt Tare Net Wt % on Mesh 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 60 60 100 120 140 200 Glassy Pan Part. 0-2% /?2-t 0-5 '$4'. 24 Z n.z 4*0 2 / 2( // 3.* Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb 60 60 100 120 140 200 s. /./ Glassy Pan Part. Remarks Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 LETTER OF CERTIFICA1 I OfVI Date: 21 Jan. 91 Customer: United Technologies 800 E. Bridge St. Plainwel1, MI 49080 ... VISIAProduct Railcar No. UTCX-46422 Attention: Quality Control Manager Order No. 883959-015 Date of Shipment: 17 Jan. 91 Customer P.0. No. 34692 Property Test Method Volatiles, 7. ABR-1A Bulk Density, GM/CC Brabender Dry Time, Mins ABR-2B * ABR-7 Particle Size, 7. on ABR-3 40 Mesh 200 Mesh Pan Vinyl Chloride Monomer ABGC-26 Inherent Viscosity ABR-10 Hard Particle @ 7Min ABR-12 Contamination, b1k/brn ABR-5A METS IR, 7. of Control ABR-13 Ana1 vs 0.15 0.507 4.9 0.00 2.8 0.8 0.021 1.02 5 3/ 115 Laboratory Supervisor/Lead VAB.0001198206 Vista Polymers \ Highway 25 "T \ Aberdeen. MS 39730 4aU, Load Date : 1-10-11 Product: 5415 : A-L AJJl Time Logged In:O Logged In By: Ship Date: Silo(s) Customer rrruja^ 1st Moisture Contamination -/* i 3 Bulk Density ,&<xo BD wo/antistat Hard Particle ~r n G 2, / 1st ./*> X, ,s*t 1st 1st I Viscosity RVCM i, pij ,Q>} Screen Analysis Mesh Weight 40 Q,CSZ? % O' z? 60 |, \Z> ^ 80 ttM 3>S~W 100 so. n 120 j2o.q 140 3,-LZ T- 3 200 4 Vo D.-i Pan dcfC> 0- Drytime: Hi3 DJIStatic Flow: 0 Avg. Microns Color L: /OP- U2~ a b METS: . Technician 7^k VAB.0001198207 . ....................................................................- "ilH'l'li'. . . . . . . . . . . . . . . . . . . . . . . . . . . . . .. 1 miH ll|lipi1l|nmTVVmmmVnHnViPTllimi||ll|l|p!-ld>4VlliWYVfTTV*W|P*llfT?WIVtmnTmViniftt|PVCniip|||l|l||l<HVV<IMHIVIVnnp?-1 4 `im!HHf1IIWtH'li'flm!lH4!>Uj<nMUh'lr>4ffl|rtt'imHtnrit1!W'ti|FMititimMi'1|i'm'. . . . . . . . . . . . > 'iiimup,HiP'+iii-,-r,Hip-' P'vlH'r' II V< .-. i i'|M-- Pl*r I rP I ......................... I ............ npi.ii 'i-P'i`r|Miiir,>h<<prpp|>iPt'kr ipmi.p-uMi I 4 I I I I 1 I I iI I I I r 1 I i i I I i iI I I I I I I 4 VAB.0001198208 Vista Fblymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OF ANALYSIS A Date: January 2* 1992 Customer: Vulcan Plastics 207 Burham Athens* AL 35611 Attention: Billy Turner Ship Date: December 30* 1991 VIS1AProduct: 5385 Railcar No.: VIPX 45747 Order No.: 0005156--004- Property Moisture* */ Bulk Density* gm/cc Particle Size* V* on 40 Mesh 200 Mesh Pan Residual VCM* ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis 0.11 0.562 0.00 5.4 1 .6 0.009 0.93 Amy E.^Bafgwell Laboratory Sup VAB.0001198209 ..i.i Vista Polymers Highway 25 Aberdeen, MS 39730 Load Date: Product Car No Time Logged In: /"73 0 M Ship Date Silo(s): Logged In By: Custome Screen Analysis Mesh 40 Weight % Drytime: 60 t-lt P*h 80 31.7 100 /STo7 &>./ 120 J&te !Vb 140 200 Pan Of* Static Flow: ^ / Avg. Microns: I&&Q Color L: a b #7/ Technician: VAB.0001198210 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601)369-8111 -f i-- =--| r pr T r'AXF" riR AIM AI V ^ T c? Date: January 2? 1992 Customer: Vulcan Plastics 207 Burham Athens* AL 35611 Attention: Billy Turner Ship Date: December 30* 1991 --VIS1AProduct Railcar No. VIPX 45891 Order No. 0005156-003 Property Moisture, */. Bulk Density, gm/cc Particle Size, V* on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis 0.04 0.00 4.7 1 .4 0.001 0.93 Bagwel1 tory Supervisor/Lead VAB.0001198211 Vista Polymers Highway 25 Aberdeen, MS 39730 Load Date: /?" / 9/ Product: Car No.: V ?9/ Time Logged In: Ship Date : _m$6 Silo(s): Logged In By: Customer: Nc `Tjiehtl-- Moisture Contamination Bulk Density Fluff Hard Particle 2nd v5^f 1 6^--- 2nd 1st 2nd 2nd I * ^ ^-- /o 7 .<57* | 0 3- ^3, 1 <57/ Viscosity RVCM ,ooi Mesh/Glassies Screen Analysis Mesh Weight % 40 co 0.0 60 J*L 7 Drytime: 80 & 100 I&.SI 120 /%/ 140 ^.3 200 233 Pan Static Flow: & / 7.C& Avg. Microns: 1*7 Color L: a b f* ^ Technician VAB.0001198212 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 ANALYSIS T Date: December 30, 1991 Customer: Vulcan Plastics 207 Burham Athens, AL 35611 Attention: Billy Turner Ship Date: December 27, 1991 -VISIAProduc t Railcar No. GACX 73412 Order No.: 0005156-000 Property Moisture, '/. Bulk Density, gm/cc Particle Size, 7. on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis 0.13 0.570 0.00 3.6 1.2 0.047 0.94 my t. uuag Laborator VAB.0001198213 Vista Polymers Highway 25 Aberdeen, MS 39730 Screen Analysis Mesh 40 Weight % 0,,0 60 h/7 2,3 80 /7. 04 SI.3 100 2.7.3 120 f.^3 ILA 140 27Z7.? 200 /,7* S.i Pan /. Drytime: Static Flow: o i t-z- Avg. Microns: Hs.o Color L; /oo.lf a " b / 7^ Technician: /V'T'S VAB.0001198214 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601)369-8111 CERT I F7 I E OF ANALYSIS December 30, 1991 Customer: Vulcan Plastics 207 Burham Athens, AL 35611 Attention: Billy Turner Ship Date: December 27, 1991 VISTAProduct: 5385 Railcar No.: VIPX 45277 Order No.: 0005156-001 Property Moisture, X Bulk Density, gm/cc Particle Size, 7. on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis 0.05 0.592 0.00 6.3 1.5 0.009 0.90 Bagwe11 Laboratory Supervisor/Lead VAB.0001198215 + Vista Polymers Highway 25 Aberdeen MS 39730 Kr V ^ rt/Y _1_ JLiV^/^n X OXo *s Load Date: Product: 5385 Car No.: ff27? Time Logged In: JX Sh ip Date: l"Z-/Z-~7 Silo(s): Logged In By: Custome r: tip Ty&fr Moisture Contamination Bulk Density Fluff Hard Particle Viscosity RVCM 40 Mesh/Glassies Screen Analysis Mesh Weight 40 & % d-D 60 80 100 Igjfe? }3.?^ 3 120 140 200 Pan > &JS f~ Drytime: Hz6 Static Flow: a Avg. Microns: /45T? Color L: b LSI Technician: VAB.0001198216 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERT I F=- I OF ANALYSIS Date: December 30, 1991 Customer: Vulcan Plastics 207 Burham Athens, AL 35611 Attention: Billy Turner Ship Date: December 27, 1991 VKIA Product: 5385 Railcar No.: ACFX 41182 Order No.: 0005156--002 Property Moisture, 7. Bulk Density, gm/cc Particle Size, 7. on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis . 12 0.0 3.4 1.0 . 137 .94 Supervisor/Lead VAB.0001198217 Load Pater I ^"'2-( Time Logged Ship Date: Product: No.: <*v//z Moisture *St 2nd I 1st Znd 1st Znd 1st 2nd 1 ! I1 c2-- #1 ^oL' Contamination Hm hlBuiJc Density^" 1 f n^tBD ua/ant is tat ^ 1 X 1 Hard Particle Viscosity RVCM 456 Screen Analysis Mesh Weight 40 <1 X 60 Q3e> J/O 80 100 fSt^TA ss:$ 120 Prytine Hfi Static Flow: O L 140 t572f 200 Pan L70 d 5"0 fr ^Zf.ttb Aw. Hlcrona: Color L; /^* ^7 */9 tr / 2r * f l|lf - + V-ir*- - Technician -- .wTM i i Ittl \ * VAB.0001198218 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CD EE F? T" X R" I CATE CDF" Aberdeen, Mississippi 39730-0091 Phone (601) 369-811 1 XS 4 Date: December 4, 1991 Customer: Vulcan Plastics 207 Burharn Athens, AL 3561 Attention: Billy Turner Ship Date: November 27, 1991 VISTAProduct: 5385 Railcar No.: VIPX 45921 Order No.: 0004107-003 Property Moisture, 7. Bulk Density, gm/cc Particle Size, 7. on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analvsis .09 .526 0.0 10.2 2.1 .275 .93 my j Laboratory Supervisor/Lead r VAB.0001198219 Vista Polymers Highway 25 Aberdeen, MS 39730 A Load Date Product Car No Time Logged In: /qQQ Ship Date: 1 ( 1t7 k si lo(s): Logged In By: 7 7/1 Customer: AJp 7??^ Moisture Contamination Bulk Density Fluff Hard Particle 1st 2nd Jf-kt 2nd 1st I 2nd 1 | .A? | 1st I 2nd 1 JF .370 1 Lgg. UiTkS 1 T7 .57* Viscosity RVCM Mesh/Glassi Screen Analysis Mesh 40 Weight % 60 80 100 120 140 200 Pan <5r> /rtf# /y;ao 7.1* -5T// /go /S78 10.9- p.i Drytime: -- Static Flow: ^ // Avg. Microns: /y-l.c Color L: a 6-fC? b /.&5 Technician: VAB.0001198220 Visto Polymers A Division of Visto Chemical Company Highway 25 Post Office Box 91 CERT I F I CATE OF Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 11 / (4 V'S X S Date: November 27, 1991 Customer: Vulcan Plastics 207 Burham Athens, AL 35611 Attention: Billy Turner Ship Date: November 26, 1991 Product: 5385 Railcar No.: UTCX 46452 Order No.: 0004107--001 Property Moisture, 7. Bulk Density, gm/cc Particle Size, 7. on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis .12 .549 0.0 8.9 0.5 .274 .94 Laboratory VAB.0001198221 Vista Polymers Highway 25 Aberdeen, MS 39730 Ft, A. X LCAR ANALYSTS &Ll A Load Date: Product: Car No ... Time Logged In : Logged In By: Ship Date: Silo(s): Customer: ulC4U*J> Moisture Contamination 1st 2nd tip Bulk Density ___ Fluff Hard Particle Viscosity RVCM Mesh/Glassi .371lS <5^ 7H 9 ziL 1st 2nd 57+ 2nd 1st 2nd / Screen Analysis Mesh Weight % 40 4 OP P.O 60 0.8U LI 80 100 120 140 200 f 7.<*h *rf6 27.L 2L.Z /?./ t.f Drytime: Static Flow: 6 L Avg. Microns Color L: f**^^ a o,oA b / Pan Technician: FlKfHPt- VAB.0001198222 Vista Polymers A Division of Vista Chemical Company I Highway 25 Post Office Box 91 X CZdt n Aberdeen, Phone (601) V" s i November 27, 1991 Customer: Vulcan Plastics 207 Burham Athens, AL 35611 Attention: Billy Turner Ship Date: November 26, 1991 Product: 5385 Railcar No-: UTCX 46575 Order No.: 0004107-000 Property Moisture, 7. Bulk Density, gm/cc rticle Size, V. on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis 02 0.0 16.0 4.5 150 Laboratory rvisor "in M ^ I ,1 I p I p Hfi* " VAB.0001198223 \ Vista Polymers Highway 25 Aberdeen, MS 39730 Screen Analysis Mesh Weight 40 4, OO % 60 * a/ 80 /A / 100 /** 120 140 /<Hf" pcf? 200 Pan geo -26" AS*0 tfsS Drytime: //jfe-*Static Flow: Avg. Microns: iss.i Color L: jQO.SZS a b Technician; VAB.0001198224 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 f Phone (601) 369-8111 (^ CERT I X CATE OF ANALYSIS Date: November 19, 1991 Customer: Vulcan Plastics 207 Burham Athens, AL 35611 Attention: Billy Turner Ship Date: November 15, 1991 Product: 5385 Railcar No.: PLCX 43738 Order No.: 0003698-002 Property Moisture, */. Bulk Density, gm/cc Particle Size, on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis .02 . 574 0.0 18.3 2.4 .003 .93 my Laboratory rvisor/Lead VAB.0001198225 p Vista Pol Hlginftf 25 AberdMOf MB 39730 Load Date : /! ^ Product:) 5385 43 73f Ti Ship Date: Logged in.* n66 Silo(s): Logged In By: 7 7, Cuatoaer: a fjo nutitt c_ Screen Analysis Hesh Weight 40 c 60 A 6*7 100 ?./ 2/,/ ft i Drytiae 57 Static Flow: Color L: 120 140 200 ?./S" 2/-1 /f-3 Pan Avg. Microns: /*38M- b Technician VAB.0001198226 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OF ANALYSIS A Date: November 19, 1991 Customer: Vulcan Plastics 207 Burham Athens, AL 35611 Attention: Billy Turner Ship Date: November 15, 1991 Product: 5385 Railcar No.: VIPX 45711 Order No.: 000369B-001 Propertv Moisture, V. Bulk Density, gm/cc Particle Size, 7. on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Ana1vsis . 14 . 547 0.0 16.0 2.7 .260 .93 Laboratory Supervisor/Lead VAB.0001198227 Vista Pol Jl- Highway' ZB Aberdeen, M8 39730 H, / Load Data: // ~/J.rfL Product: Logged Logged In Bjr: Ship Date: Silo(s) ^JT ?// Moisture Contaaination Bulk Density Hard Particle 1st 2nd 1st 2nd 1st I 2nd | 1st 2nd . e> / 1 gI I , /</ 1 1 / z-- S(7) e B 53? Viscosity RVCM 40 Mesh/Glassies ftcO Screen Analysis Mesh 40 Weight *p LL 2- 8.7 100 120 /W2- /it. 2 <Dk>' 140 33.7 Pan 7.78 f-33 /Q,.o 371 Dryt 1m Static Flow: Color L: 99-7/ a Avg. Microns h Technician: VAB.0001198228 - Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 4 V A CERT X F7 X CC T EC OF ANALYSIS Date: December 13, 1991 Customer: Vulcan Plastics 207 Burham Athens, AL 35611 Attention: Billy Turner Shi p 10, 1991 VKIAProduct: 5385 Railcar No.: VIPX 45805 Order No.: 0004691-000 Propertv Moisture, V. Bulk Density, gm/cc Particle Size, 7. on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 AB6C-26 ABR-10 Analysis 0.14 0.584 0.00 8.7 1.9 0.93 my it/ Bagwell Laboratory Supervisor VAB.0001198229 Vista Polymers Highway 25 Aberdeen, MS 39730 Load Date: Time Ship Date : Product: 5385 I n: /4taa Silo(s): Car No.: fa ~~ Screen Analysis Mesh Weight 40 Q< 0 & % 0^0 60 . Za 80 100 120 140 200 /-,!? 7. / 4. 34 29,/ -2s^.0 /*3 f.7 Drytime: ,7.7Static Flow: 0 Avg. Microns: Color L: f&OtZO a 'J* b Uf Pan . 93 /. 9 Technician: rgMd* VAB.0001198230 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-6111 CERTIFICATE OF ANALYSIS Date: December 13, 1991 Customer: Vulcan Plastics 207 Burham Athens, AL 35611 Attention: Billy Turner Ship Date: December 10, 1991 VKIA Product: 5385 Railcar No.: ACFX 41146 Order No.: 0004691-001 Property Moisture, V. Bulk Density, gm/cc Particle Size, 7. on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis 0.15 0.580 0.00 9.2 2.6 0.142 0.90 Amy EL/ Bagwell Laboratory rvisor/Lead VAB.0001198231 Vista Polymers Highway 25 Aberdeen, MS 3973Q ^ F*VO RAILCAR ANALYSIS Screen Analysis Mesh 40 Weight 0*oo % 0*o 60 . // , 2L- 80 7.*2- 100 /r.s'j J/. O 120 /3, /? -Z7J 140 7/ AA /5T / 200 7.z Pan A -7/ -2. 4 Drytime: __________ Static Flow: 0f 0 Avg. Microns: /^t Color L: J06* 3 a "< 2-7 b Technician VAB.0001198232 * ~y Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 1 1 \A CERTIFICATE OF ^ ^ L_ V S X S Date December 4, 1991 Customer: Vulcan Plastics 207 Burham Athens, AL 35611 Attention: Billy Turner Ship Date: November 27, 1991 Produc t Railcar No.: ACFX 41181 Order No.: 0004107-002 Propertv Moisture, V. Bulk Density, gm/cc Particle Size, 7. on 40 Mesh 200 Mesh ran Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analvsis .04 0.0 9.4 2.0 . 110 .94 Laboratory Supervisor/Lead VAB.0001198233 * * ,41 '# Vista Polymers Highway 25 * 'll Aberdeen MS 39730 A 4 Load Date: //- **?/ Product: 5385 Car No.: f//% / Time Logged In: D?# Ship Date: ) (\yi h Silo(s): Logged In By: L2& Customer Ato Moisture Contamination I Bulk Density Fluff Hard Particle 2nd 2nd 1st | 2nd 1st 2nd j.Cif- cL k 71 f 1 /o Viscosity RVCM Mesh/Glassies no Screen Analysis Mesh 40 Weight % Ok o 60 #33 0.? 80 /0/SD 20.0 100 /4-2Z 120 140 /2.2Z- 2.3Z ti.n 200 4. 7d q.4 Pan /o.2. 2.0 Drytime: Static Flow: {0 /f Avg. Microns: laris' Color L: (*> U a b /`tf Technician VAB.0001198234 rr- 0-1 -_^1| Vista Polymers Highway 25 Aberdeen, MS 39730 rv m m m ~~ - a. -ma u u w *. & A Load Date: Product: 5385 Car No.: ^ Time Logged In: Logged In By: Ship Date: Silo(s): Customer: Screen Analysis Mesh 40 60 80 100 120 140 200 Weight ________ ________ ________ ________ ________ ________ ________ % Pan Drytime Static Flow: _____(______ Avg. Microns: Color L: Technician: i'pii VAB.0001198235 * * * 0 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730*0091 Phone (601) 369-8111 LETTER OF CERTIFICATION Date: 2 S' // ^ ^ Customer Vulcan Plastics 207 Burham Athens, AL 356 Attention: Billy Turner Ship Date: zS ///. 91 VISIA Product: 5385 Trailer No: Order No0 0 0 Propertv Moisture, 7. Bulk Density, gm/cc Particle Size, 7. on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-iA ABR-2A ABR-3 Analysis 0. 0 ABGC-26 ABR--10 Not more than 8.5 PPM This material was pro duced to yield an inherent viscosity in the range of .90 to .95. VAB.0001198236 4 A Date. Customer Technician PVC BULK TRAILER ANALYSIS Silo </77. jr Trailer Number Time )!2 0 T~XU Particle Size Distribution: Screen Analysis /0 Mesh Size 40 Gross Wt Tare Net Wt H on Mesh 0. 4 O 09 Screen Analysis v V Mesh Size Gross Wt Tare Net Wt H on Mesh 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 gins. Carb 60 80 100 120 140 200 Glassy Pan Part. All 2.^ Min LML 2/. 2^ /2.U 2*7 /A U Z_Z Ml A On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 /,i Glassy Pan Part. Remarks wpmilN J 4 M n ICI Htt VAB.0001198237 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 AfdVs J f Customer: Vulcan Plastics 207 Burham Athens, AL 35611 Attention: Billy Turner Ship Date: A/4V* 2/ Aberdeen, Mississippi 39730-0091 Phone (601) 369-811 1 / A i i ce* X OM Product: VIS1A Trailer No: J" Order No.: COO 5 792-0 Property Moisture, 7. Bulk Density, gm/cc Particle Size, V. on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC--26 ABR-10 Analysis <?. O 2^ 2 Not more than 8.5 PPM This material was pro duced to yield an inherent viscosity in the range of .90 to .95. oratory ........mm * VAB.0001198238 -ii.. PVC BULK TRAILER ANALYSIS Date. 11" Customer Technician ' ? I_________ Product S3 L)uIcAk$_______ Silo__ (r 7^--------- ________________________________________ Trailer Number Order No. A Particle Size Distribution: Screen Analysis_____ Ui.Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb Mesh Size 40 60 80 100 120 140 200 Glassy Pan Part. Gross Wt. Tare Net Wt. % on Mesh 0'O O . ZO t^o /4,,(. tf )3. it- 7. (.4 f.70 ).Q o, o /& 2?, J z.6. r /r. j 9. 2.0 Screen Analysis . Mesh Size Gross Wt. 40 Min. On Rotan shaker 49 amt. Resin olus 1.0 amt. Carb Pan 60 80 100 120 140 200 Glassy Part. Tare Net Wt. % on Mesh Remarks Wff *4n HP VAB.0001198239 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 1 1 LETTER OF CEIF^T I F I I OM A Date: AJ Customers Vulcan Plastic 207 Burham Athens, AL Attention: Billy Turner Ship Date: 2-C AJJU* VISIA Product: 53S5 Trailer No: Order No.: 0 00 3 f f Z - OO / Property Moisture, */. Bulk Density, gm/cc Particle Size, 7. on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 Analysis OP . r?2. 0^. ABGC--26 ABR--10 Not more than 8.5 PPM This material was pro duced to yield an inherent viscosity in the range of .90 to .95. VAB.0001198240 PVC BULK TRAILER ANALYSIS * iw H'Z 3'? /_________ Prndnp* S' S f __________ Trailer Number__ZlZ Customer )/u.! ______ Silo___ 6 $ $ Time __________ Technician 'n1<id_______________ _______________________ Order No. Particle Size Distribution: Screen Analysis /o Mesh Size 40 Gross Wt. Tare Net Wt. H on Mesh <>* l. Screen Analysis * H V Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 Remarks Min On Rotap shaker. 49 gins. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. .01 ,1 Min. 60 7.3/ /3.1Z 17-* jr.y 7. Sj ./f.Z- S'.// JC. 2- /./S' 2.,3 On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Pan 80 100 120 140 200 Glassy Part. --* e A in mHm VAB.0001198241 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601)369-8111 * LETTER OF C El FR "T X fr^ X CAT I ON * Date: 2.3 AfdU* 9/ Customer: Vulcan Plastics 207 Burham Athens, AL 356 Attention: Billy Turner Ship Date: -2^ VrfV. 9/ VBIA Product: 5385 Trailer No: Order No.: Coo Property Moisture, 7. Bulk Density, gm/cc Particle Size, X on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-IO Analvsis - > r/7 o. 0 h z,o Not more than 8.5 PPM This material was pro duced to yield an inherent viscosity in the range of .90 to .95. ratory Supervi*br/Lead VAB.0001198242 PVC BULK TRAILER ANALYSIS A Date IhZX'li Customer */ AjJ Product -S' 3 ^ ^ Silo___ Lt Technician MOIST Bottom i ** CONT. Bottom i 4 V * GEL FRONT I Trailer Number r Time 0 TTO Order OO0 2*3*) 2O0G BULK DENSITY I . r/ 7 DRY TIME I S. o COLOR vise L =/Ofi.lL RVCM a = ~/r B = / C6 \ L MIDDLE A= END II L= Particle Size Distribution: Screen Analysis_______JMOin On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb Mesh Size 40 60 80 100 120 140 200 Glassy Pan Part. Gross Wt. Tare Net Wt. % on Mesh o, 0& 9-7o /snt to 1. X 2\-4- tf.AO 1*00 2<o Screen Analysis Min. On Rotap shaker 49 gms. Resin plus Mesh Size 40 60 80 100 120 1.0 gms. Carb Pan 140 200 Glassy Part. Gross Wt. _________ _________ _________ _________ _________ _________ _________ Tare _________ _________ _________ _________ _________ _________ Net Wt. _________ _________ ________ ________ _________ _________ _________ 4% on Mesh _________ _________ Remarks m-.-a 4* n r<r? VAB.0001198243 Vista Polymers A Division of Vista Chemical Company CERT X R" I Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 OF ANALYSIS A Date: November 19, 1991 Customer: Vulcan Plastics 207 Burham A t hen s, AL 35611 Attention Bi11y Turner Ship Date November 15, 1991 Product: 5385 VISTA Railcar No.: VIPX 45910 Order No.: 0003698-000 Property Moisture, V. Bulk Density, gm/cc Particle Size, 7. on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 * ABGC-26 ABR-10 O o Analysis . 15 .576 11.0 2.4 1.984 .93 Laboratory Supervisor/Lead VAB.0001198244 >!* Vista Pol Highway 25 Aberdeen MS 39730 A PVC RAX LCAR ANALYS X S Load Date: / Q '/S'-9/ Product; Car Ho. Tine Logged o/oo Logged In By: Ship Date; Silo(s): Cuetoner Moisture Contaaination Bulk Density Fluff Hard Particle 1st 2nd 1st 2nd I 1st I 2nd [ 1st 1,c3 ~Wl 1 %t7 1| | 1 % .S%3 \s68 2nd Viscosity RVCM Mesh/Glass /.in- Screen Analysis Mesh 40 Weight 0^0 60 4/g o3 60 //s? 100 IMS 120 li&t xti 140 200 O Drytine: S^> Static Flow: Avg. Microns: Color L : /*>// At) I b Pan Technician: VAB.0001198245 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 LETTER OF CERTIFICATION A Date: November 19, 1991 Customer: Vulcan Plastics 207 Burham Athens, AL 35611 Attention: Billy Turner Ship Date: November 13, 1991 Product: 5385 VB1A RAILCAR No.: PLWX 44461 Order No.: 0008000--001 Property Moisture, 7. Bulk Density, gm/cc Particle Size, 7. on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis .13 .580 0.0 10.1 2.4 .256 .93 VAB.0001198246 y Viatm Poly--tb Highway 25 Abcrdetn> MS 39730 Load Ship Date: /0~*23''c?/ Product 5385 Cmr Logged togged In By: Silo(s) Gusto Moisture Contaaination Bulk Density Fluff Hard Particle A 1^ CB 1st I 2nd | 1st I 2nd 1 1st I 2nd 1 1st .of 1______ J 1 T2^1 !* 1 | tzsT [ .nr I_______ 1 .r/*-1 ."7* I .S~?6 , IJ 1 /aT I | /*r [ , }1_ 1~ 1 J&e I sra 1_______ .r?(* 1 S'7' 1 1 JT77 2nd Viscosity RVCM Mesh/Glass Screen Analysis Mesh 40 Weight .o*> 60 80 100 120 140 200 Pan n .2-2, //.o3 /s-9* //.s-y l. 93 SZa S A 21 22. / 27f 23.3 /3. J /*. / Drytiee: Static Floe: Color L: ~.ol b Avg, Microns: Technician VAB.0001198247 K r *4 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A I__ETTER OF CERT I I I Of\J Date: November 19, 1991 Customer: Vulcan Plastics 207 Burham Athens, AL 35611 Attention: Billy Turner Ship Date: November 13, 1991 Produc t VfclA RAILCAR No. VIPX 45870 Order No.: 0008000-000 Property Moisture, V. Bulk Density, gm/cc Particle Size, 7. on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis .05 0.0 7.6 1.9 1.964 .93 A my E. era g4el 1 0 Laboratory Sup ervisor/Lead VAB.0001198248 in Vista Pol Highway 25 Aberdeen, MS 39730 "Nt / Load Date: Tiae gad Ship Date; Product: Car No. Logged In By: Silo(s): Oustoner: ode**-' - DOO 1st 2nd I 1st 2nd f 1st 2nd 1st 2nd Moisture Contaaination Bulk Density I ,o5J I /s\ 39 \S7^ I Fluff I .of 11 I . g> ^ i?n --11 sZ. sg f 1 Hard Particle Viscosity RVCM 40 Mesh/Glassies Screen Analysis Mesh 40 Weight 60 ff .3 so,n 100 S 120 /S7 }Z2JZ> I4 140 13. 200 Pan . 7-4 /f Drytiae: Static Plow Avg. Microns Color L: /QO'O b /'6>7 Technician: VAB.0001198249 , rr Ha Vh<p Oiwwtcd Company nwV>-P--w--fot foal Offic* Bob 91 39730 Phom MOD 3694111 A Dt Customers Vulcan Plastics 207 Burham Athens, AL 35611 Attention* Billy Turner Date of Bhi pment I |sr i CAT I OIM Product* VIS1A Trai1er No.t7=27 e> Lot No.i rder No.t s&coz&g- 0O& Property Test Method Volatiles, % Bulk Density, GM/CC Brabender Dry Time, Mins Particle Size, % on 40 Mesh 200 Mesh Pan Vinyl Chloride Monomer Inherent Viscosity 0.950 0.410 0.450 0.300 0.955 0. 600 Laboratory Supervisor/Lead VAB.0001198250 Customer Technicia PVC BULK TRAILER ANALYSIS 4 Particle Size Distribution: Screen Analysis Mesh Size 40 Gross Wt Tare Net Wt 4 H on Mesh Screen Analysis Mesh Size Gross Wt. Tare Net Wt % on Mesh 40 Remarks Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 60 100 120 140 200 Glassy Pan Part. /S?3o Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Pan 60 80 100 120 140 200 Glassy Part. Star 207A Revised 1/12/97 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 ( Sk Date: January 2* 199E Customer: Vulcan Plastics 207 Burham Athens* AL 35611 Attention: Billy Turner Ship Date: December 30* 1991 --VISlAProduct Railcar No. ACFX 41155 Order No. 0005156-005 Property Moisture* % Bulk Density* gm/cc Particle Size* V* on 40 Mesh 200 Mesh Pan Residual VCM* ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Ana1vsis 0.04 0.00 10.9 2.8 0.93 Laboratory Supervisor/Lead VAB.0001198252 Vista Polymers Highway 25 Aberdeen MS 39730 a Load Date: Time Ship RAX LCAR ANALYSIS Product: In: ALT o 5385 Car No.: In By: Screen Analysis Mesh Weight X 40 0, Qo ________X , 0/0 60 ** Drytime: ^3 80 100 120 140 200 Pan fi'iC Lto Mo 2M. m. Static Flow: ^ / /ft? Avg. Microns: /rs. # Color L: ab Tech nician: 7ft 0 VAB.0001198253 Vbfto MjiMfi VMa Ommical Company mjam-m--n-ro*c9 Pbrf Oflk l<w 91 39730 PhoM (Ml) in369-4 A OF CERT* I X ION Data i Customer: Vulcan Plastics 207 Burham Athens, AL 35611 Attentions Billy Turner Data of 8h i pmant Products VIS1A Trailer No.i Lot Nok 0rd.r No.. 00OO2&&-00t Property Test Method Analysis Volatiles, Y. 8.950 Bulk Density, 6M/CC 8.410 Brabender Dry Time,Mins. 8.450 Particle Size, 7. on 8.300 40 Mesh 200 Mesh Pan Vinyl Chloride Monomer 8.955 Inherent Viscosity 8.600 Not more than 8.5 PPM This material was produced to yield an inherent viscosity in the ran of . W to VAB.0001198254 Customer Technic PVC BULK TRAILER ANALYSIS A Particle Size Distribution: Screen Analysis Me*h Size Gross Wt Tare Nat Wt H on Mash Screen Analysis 40 0,0 Mash Size Gross Wt. Taro Net Wt H on Mash 40 Min On Rotap shaker. 49 gins. Resin plus 1.0 gms. Carto 60 80 100 120 140 200 ffltfty Pan Part. <?,/? Q-3 /d.M fe/rZ n.s$ l\,5 3.3? f.az Min. On Rotap shaksr 49 gms. Rsain plus 1.0 gms. Carta 60 80 100 120 140 200 Pan Glassy Part. Remarks VAD.0001198255 Vida Poiyman ADMiionaf Vida CtiamicQi Company Highway 25 Rod Ofnc* Bon 91 MniHDoi 39730 Phono ( )601 369-8111 LETTER 01=- CERTIFICATION Datti (o-(& ~*?l Customer: Vulcan Plastics 207 Burham Athens, AL 35611 Attention: Billy Turner Date of Shi pment: ^ Trailer No Lot No: Order No,: {>OOO A Property Test Method Analysis Volatiles, X 8.950 Bulk Density, 6M/CC 8.410 Brabender Dry Time, Mins. 8.450 Particle Size, X on B. 300 40 Mesh *h 200 Mesh Pan Vinyl Chloride Monomer Inherent Viscosity 8.600 z~. p.o Not more than B. 5 PPM This material was produced to yield an inherent viscosity in the r e of to Laboratory 8uper7isor7/Li ead VAB.0001198256 w PVC BULK TRAILER ANALYSIS A Date Customer \/^ C-cA ^ Product Technicia MOIST Bottom i J3 CON'T. Bottom GEL 1 Trailer Number. Time ^ ^ Order No. BULK DENSITY DRY TIME COLOR L FRONT I 2. A = 0./O = /.o II I L- vise RVCM 0/ MIDDLE A= END \i B= Particle Size Distribution Screw) Analysis Mash Size 40 Gross Wt Tare Net Wt H on Mesh 6,, OO 6 Screen Analysis Mesh Size Gross Wt. Tare Net Wt H on Mesh 40 Min On Rotsp shaker. 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Gtassy Pan Part. e.a~ o //.# 2**4- Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Pan Glassy Part. Remarks Star 207A Revised 1/12/87 tvp rWffiw* A DMriofi of Ptm (toil 369-OTI Date: Customer: Vulcan Plastics 207 Burham Athens, AL 35611 Attention: Billy Turner Date of Shipment: ^lf I 1CATION Product: Trailer No.: Lot No.: Order No.: VISTA ^O'P^ Property Test Method Analysis Volatiles, % 8.950 Bulk Density, 6M/CC 8.410 Brabender Dry Time,Mins. 8.450 Particle Size, % on 8.300 40 Mesh 200 Mesh Pan Vinyl Chloride Monomer 8.955 Inherent Viscosity 8.600 Not more than 8.5 PPM This material was produced to yield an Inherent viscosity in the ranae of to Laboratory Super isor/Lead VAB.0001198258 Hate ^ PVC BULK TRAILER ANALYSIS _______ Product ^ <3&d Trailer Number T-SP 4 Particle Size Distribution: Screen Analyeta Mesh Slza 40 Groaa Wt Tara Nat Wt. _______ &6Q H on Maah Scraan Analysis ______ Maah Slza Oroaa Wt. Tara Nat Wt. H on Maah 40 _____ Min On Rotap shaker. 49 gms. Raain phis 1.0 gma. Cart* 100 120 140 Qtaaay Pan Part. *.o /'*> /ffrti 6S& 3.7<e Ice? UfaS" {3-Q _Min. On Rotap shaker 49 gma. Raain plua 1.0 gma. Carb Pan 00 90 100 120 140 200 (llaaay Part. Remarks i 1 4-------------- iiU|*ii|l MjV: fNIHMliPMlim1- VAB.0001198259 II r-. - Vista Polymers A Division of Vista Chemical Compony Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730*0091 Phone (601) 369*8111 IFIC x orvi Date 20 June 91 Customers Vulcan Plastics 207 Burham Athens, AL 35611 Attentions Billy Turner Date of Shipments 11 June 91 Products 53B5 VISIA RAILCAR No.s UTCX-46444 Order No.s 0000158-005 Property Moisture, 7. Bulk Density, gm/cc Particle Size, 7. on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis .03 0.0 5.7 1.9 .070 .92 Laboratory Supervisor/Lead h VAB.0001198260 Vista Polymers Highway & Aberdeen. MS 39730 * Load Pate: &Product: 5385 Car No.: %TCX Time Logged In: ^ Logged In By: /1 Ship Date: Silo(s): Customer: 7HGfaL Moisture Contamination Bulk Density Fluff Hard Particle I 1st 2nd 1st I 2nd 1 *03 ? /? .S5*> _________ !(c> j \.5& | 1st I 2nd .*3 \ > I .SX3 I I 1st 7 \'/o I .&*f- 2nd Viscosity RVCM Mesh/Glassi Screen Analysis Mesh Weight 40 A % 60 80 100 120 140 > 37 52- &0J3 200 Pan if Drytime: Static Flow: Color L: n#> a _ /Avg. Microns: b /.&? Technician: a i b VAB.0001198261 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 IF" I CAT I OM *' Date: 17 June 91 Customer: Vulcan Plastics 207 Burham Athens, AL 35611 Attention: Billy Turner Date of Shipment: 10 June 91 Product: 5385 RAILCAR No.: UTCX-46402 Order No.: 0000158--004 Propertv Moisture, "/. Bulk Density, gm/cc Particle Size, V. on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis .12 0.0 7.6 2.6 .368 .93 Laboratory Supervisor/Lead s i VAB.0001198262 Vista Polymers Highway 25 Aberdeen MS 39730 A Ship Date: Time ! U40 2_ Screen Analysis Mesh 40 Weight % OvO 60 80 100 120 140 200 Pan 10.7? /r.zs' /Z.37 4.^7 3.71 /.Zi Z Z/# 6 JO* ZM Drytime: Static Plow a / f-S'" Avg. Microns Color L: lQ0> 07 a b A 4(7 Technician: VAB.0001198263 Yisto Polynw* A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 . : \ + LETTER OF CERTIFICATIQNV. Date: 19 June 91 Customer: Vulcan Plastics 207 Burham Athens, AL 35611 Attention: Billy Turner Date of Shipment: 7 June 91 Product: 5385 RAILCAR No.; GACX-73382 Order No.: 0000158-002 ProDertv Moisture, 7. Bulk Density, gm/cc Particle Size, 7. on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-IO ftlillYEi? 0.11 0.572 0.00 9.4 2.8 0.190 0.93 Laboratory Supervisor/Lead VAB.0001198264 Vista Polymers Highway 25 G Aberdeen MS 39730 Load Date: Product: 5385 Car No Time Logged In: Q&S0D Logged In By: Ship Date: Silo(s): Customer Moisture Contamination Bulk Density Fluff Hard Particle 2nd 2nd 1st 2nd rfe? /2- Lr72-| Z2_ Sx~ .f7 7 2nd r?o Viscosity RVCM Mesh/Glassi Screen Analysis Mesh 40 Weight % 0.0 Drytime: 60 0.03 J. 80 r.?/? 100 /J.SI Z7.L 120 If. VC J/.f- 140 ?, 0-* ILL 200 9.7> Pan t,40 Static Flow: 0 / Avg. Microns Z^J Color L: a fa 4 Technician: VAB.0001198265 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 OF CERTIFICATION Date: 19 June 91 Customer: Vulcan Plastics 207 Burham Athens, AL 3561 Attention: Billy Turner Date of Shipment: 6 June 91 Product VKIA RAILCAR No. VIPX-45907 Order No.: 0000158-001 PrBPtrty Moisture, 7. Bulk Density, gm/cc Particle Size, 7. on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-IO Analysis 0.03 0.580 0.00 5.9 2.0 0.065 0.94 Laboratory Supervisor/Lead i VAB.0001198266 Vista Polymers r^\ Highway 25 Aberdeen. MS 39730 Load Date: Time Logged In l/fWRAI L C A R, ANALYS IS Product: 5385 Car No .:Jj_^P7 04&b Logged In By: Ship Date: Silo(s): Customer: 1st 2nd 1st 2nd I 1st 2nd 1st Moisture g>31 q^ _________ . _____Contamination 1 7 7V- ___ .O/ 1 V 1 . Y7 Bulk Density 1 1 usr?y 1 Fluff X) 0 _________1 Hard Particle 2nd Viscosity RVCM Mesh/Glassi Screen Analysis Mesh 40 Weight X f> P Drytime: 60 80 (& 30 3 100 120 2-o~ 7 140 200 /0. 2s 3. 9 Pan JL Static Flow a /. Q&'^>< Avg. Microns Color L: a 0.&y Technician * VAB.0001198267 Vista Polymers A Division of Vista Chemical Company 25 Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 II x arvi Date: 13 June 91 Customer: Vulcan Plastics 207 Burham Athens, AL 35611 Attention: Billy Turner Date of Shipment: 10 June 91 Product: 5385 VB1A RAILCAR No.: UTCX-46510 Order No.: 0000158-004 Property Moisture, X Bulk Density, gm/cc Particle Size, X on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis 0.20 0.544 0.00 7.0 2.9 0.230 0.92 Laboratory Supervisor/Lead i VAB.0001198268 Vista Polymers Highway 25 Aberdeen^ MS 39730 Load Date: Product: Car No Time Logged In: Logged In By: Ship Date: Silo(s) Customer: Screen Analysis Mesh Weight 40 ________ 60 80 100 ________ ________ ________ 120 ______ X 140 200 ________ ________ Pan Drytime: Static Flow: Color L: a L Avg. Microns b Technician: % VAB.0001198269 Vista Polymers Highway 25 Aberdeenv MS 39730 RAILCAR ANALYSIS * Load Date: S - Product: 5385 Car No. : Time Logged In: C3 Logged In By: / ,/ Ship Date: Silo(s): Customer: f& Moisture Contamination A 1st I 2nd CA I 1st I 2nd <^CB J) 1st 2nd 1 <^B J) I 1st 2nd Bulk Density Fluff Hard Particle Sr\s.. ?j Ei' A' 1= i: si uj J Ir Viscosity RVCM Mesh/Glassi | Screen Analysis Mesh 40 60 80 100 120 140 200 Pan Weight % Drytime: Static Flow: Color L: a L Avg. Microns: b Technician: l*T 1 VAB.0001198270 Vista Polymers Highway 25 Aberdeen* MS 39730 RAILCAR ANALYSIS Load Date: T~ Product: 5385 Car No.: Time Logged In: Logged In By: >3L Ship Date: Silo(s )'._f Customer /yvo 2-3 S Moisture Contamination ,/? S6 2nd 2nd 2nd JLO 2nd Bulk Density Fluff Hard Particle .57? i Viscosity RVCM Mesh/Glassies Screen Analysis Mesh 40 Weight o.o'b % Q.Q 60 80 100 120 140 200 Pan id-ft %21 3hk %L2 S.LL 2 IMA Z3_ Drytime: Static Flow: o /// ^ Avg. M icrons Color L: ,z/*Sl a b //> Technician: r do + E s VAB.0001198271 VUo PolyiMH AOMaionof Villa Qwmteial Company rapiww OcK* foot Ofnca ton 91 Abwdaan. Mimmppi 39730 Pham (601) 369-8111 CERTIFI x ovm Data i Customers Vulcan Plastics 207 Burham Athens, AL 35611 Attentioni Billy Turner Date of Shipments ^^^7/ Products Trailer No.i Lot No.i Order No. s VISTA Property Test Method Analysis Volatiles, 7. 8.950 Bulk Density, GM/CC 8.410 Brabender Dry Time, Mins. 8.450 Particle Size, V. on 8.300 40 Mesh 200 Mesh Pan Vinyl Chloride Monomer 8.955 Inherent Viscosity 8.600 Not more than 8.5 PPM This material was produced to yield an inherent viscosity in the range of to -5L_. Laboratory Supervisor/Lead VAB.0001198272 Date b Customer TWImlriM. ft tt-jT-S PVC BULK TRAILS) ANALYSIS Product Silo L12. Trailer Number. Time Order No. * Particle Size Distribution: Screen Anatyala Meeh Size Qroee Wt. Tare Net Wt. H on Meeh Screen Analysis 40 MmK Sin Qroee Wt. Tare Net Wt. % on Meeh Remarks 40 Min On Rotap shaker. 49 gme. Realn plus 1.0 gme. Carto 100 120 140 200 GUassy Pan Part. ok L Min. 90 ML Zl.L /6.7/ /. .rjr 2(- n.i On Rotap shaker 49 gme. Realn phis 1.0 gme. Carb 100 120 140 200 isk u Pan Qlaeay Part. 20TA 1/12/07 ffin unr ii ii UHtfN *** i -t * AB.0001198273 K 1 YUoMyiMfi ADMiionof VWq CkwMal Compony nijnwOlr Fb* Omc* Box 91 Afcwinn, Mmmippi 39730 PIiom (601) 349-8111 Dates Customers Vulcan Plastics 207 Burham Athens, AL 35611 Attentioni Billy Turnsr Date of Shipmenti >**2*^/ CERTIFI X OIM Products VIS1A Trai1er no. Lot No.i rd.r No. i 000?t$ytf'--00t> Property Test Method Analysis Volatiles, X Bulk Density, 8M/CC Brabender Dry Time, Mins Particle Size, % on 40 Mesh 200 Mesh Pan Vinyl Chloride Monomer Inherent Viscosity 8.950 8.410 8.450 8.300 8.955 8.600 .*7 .<572- Not more than 8.5 PPM This material was produced to yield an inherent viscosity in the range of "0 to j95 Laboratory Supervissoorr/Lead | 1 -- -W-*! -- VAB.0001198274 PVC BULK TRAILER ANALYSIS Customer Technician FRONT MOIST CON'T. I2E Bottom | Top l t&7\ 0 m i * t * 1 Bottom GEL I 2. 2. 2. 1 I. i. Trailer Num Order No BULK DENSITY I DRY TIME I 2. 2. 1. I COLOR vise ~99r2- ify' - /2-7 L 4 MIDDLE 2. i END 2. 2. B I II I L 2. 2. 2. 2 B Particle Size Distribution: ScrMn Analyst* Math Slat Gross Wt. f Tart Nat Wt. H on Mash Scrssn Analysis 40 && Mash Stzs Gross Wt. Tara Nat Wt. H on Mash 40 Min On Rotap shaksr. 40 gins. Basin plus 1.0 gms. Carb 100 120 140 200 Glassy Pan Part. fo.&t m Min. On Rotap shaksr 40 gms. Rasln plus 1.0 gms. Carb 100 120 140 a. 8/ j&: Glassy Pan Remarks Star 297A m.n |i i Pij *F1V 1/12/07 F -ta- j* " %. --p a - tt* OH1 VAB.0001198275 II H LJ Date: 30 May 91 Customer: Vulcan Plastics 207 Burham Athens, AL 3561 Attention: Billy Turner Date of Shipment: 2B May 91 Product: 5385 VISIA RAILCAR No-: UTCX-46566 Order No.: 006125-281 Property Moisture, 7. Bulk Density, gm/cc Particle Size, 7- on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-IO Ana Ivsis 0.07 0.570 0.00 7.5 2.4 0.92 Laboratory Supervisor/Lead VAB.0001198276 Vista Polymers Highway 25 Aberdeen* MS 39730 * Load Date: S'~ 2L. ~ RAILCAR ANALYSIS P XTCX / Product: 5385 Car No.: 4(. s' U. Time Logged In: Ship Date : 2%. Silo(s): Logged In By: (el 1 Customer Moisture Contamination Bulk Density A CA I 1st I 2nd 1 1st 2nd 1 .oC 1________ I -2*. -- 1 /Sd 1 to fo 1 1 CB I 1st 2nd .o? I /? 1 /*sT\ B 1st I 2nd .<oi ~s> I //J> _________ II 11 Fluff Hard Particle Viscosity RVCM Mesh/Glassi Screen Analysis Mesh 40 Weight % 0*00 0.0 Drytime: 60 Q.so $* (p 80 100 /b.zs /5J0 2P*6> Static Flow: 120 140 /J 2 200 ^2 Pan //S' Avg. Microns: /3-0 Color L: a ^V7 b Arp_ Technician: nr* . t VAB.0001198277 Vista Polymers 1 A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phono (601) 369-8111 LETTER OF CERT I f=" X C^T I OfVJ Date: 31 May 91 Customer: Vulcan Plastics 207 Burham Athens, AL 35611 Attention: Billy Turner Date of Shipment: 30 May 91 Products 53B5 VKt\ RAILCAR No-: PLCX-43944 Order No-: 806125-288 Property Moisture, 7. Bulk Density, gm/cc Particle Size, X on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR--3 ABGC-26 ABR-10 Analysis 0.10 0.575 0-00 6.6 1.8 0-*7 0.5J3 H.D. Lucas Laboratory Supervisor/Lead VAB.0001198278 -iti if ^'7 r Vista Polymers Highway 25 Aberdeen* MS 39730 RAILCAR ANALYSX S Load Pate : ^*7^ Product: 5385 Car No.: Time Logged In: Ship Date: Silo(s) Logged In By: LO& l/UlCA/J Customer: 8o(ot2S- A 1st 1 2nd CA 1st 1 2nd 1 CB I 1st I 2nd I 1st B 2nd Moisture Contamination 1 JO 1 2- Bulk Density Fluff _ L sgo .*9 1I .5f?o , O </|________ 1 "V 1 /? ,;0 .57 > $ * _________ i Hard Particle Viscosity RVCM 1 . n.3 LZ&7 Mesh/Glassi Screen Analysis Mesh 40 Weight % M> 0-0 Drytime: 60 L 80 is.sL 3LL- 100 /X7/ 120 140 Jp.ZS S.<t3 Ah- /e-9 200 Static Flow: O / n. Avg. Microns Pan a.*? Color L: a P-O*/ b Technician: C*0 a VAB.0001198*279 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601} 369-8111 -f LETTER OF CERT I F=" I CAT I OM Date: 31 May 91 Customer: Vulcan Plastics 207 Burham Athens, AL 3561 Attention: Billy Turner Date of Shipment: 29 May 91 Product: 5385 VIS1A RAILCAR No.: PLWX-44372 Order No.: 806125-280 Property Moisture, V. Bulk Density, gm/cc Particle Size, X on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis 0.13 0.00 8.9 2.2 0.174 0.94 H.D. Lucas Laboratory Supervisor/Lead VAB.0001198280 Vista Polymers Highway 25 Aberdeen MS 39730 Load Date: '2?-?/ Product: 5385 Car No.: plw'k A Time Logged In: //& <^> Ship Date: ^ Silo(s) Ao ate-fal Logged In By: : Vuju+-> Customer 3Q&/25- Screen Analysis Mesh 40 Weight 0. oo % 0. 0 60 2.7 80 jiM z, 7 100 /?~C3 2r. / 120 //>.n 2/. <T 140 /J.2- 200 s.? Pan Drytime: r.o Static Flow: 0/7.? Avg. Microns: at?.? Color L: 9f. a ~>/0 b / $2. Technician: VAB.0001198281 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 * Date: 30 May 91 Customer: Vulcan Plastics 207 Burham Athens, AL 3561 Attention: Billy Turner Date of Shipment: 28 May 91 I OM Product RAILCAR No. VISTA 5383 ACFX-41172 Order No.: 806125-282 Property Moisture, 7. Bulk Density, gm/cc Particle Size, 7. on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis 0.12 0.00 6.4 1 .6 0.94 Laboratory Supervisor/Lead VAB.0001198282 Vista Polymers Highway 25 Aberdeen! MS 39v 730 Load Date: Time Logged Ship Date: Product: ACfXMALYSIS 5385 Car No. 4/J 7 6/0 0 Logged Silo(s): Ctf. t ?7 Customer Moisture Contamination Bulk Density Fluff I 1st I 2nd | 1st 1 2nd 1 ,/o 1 ~L of 1 \t 1 \/x~ . U*d / | /x~ 1 SS21 I 1st \./G 2nd ^1 f3 stpI I 1st 1 2nd \./z 1 13 1 14 1 SX31 Hard Particle Viscosity RVCM Mesh/Glassies Screen Analysis Mesh 40 Weight x $ -<pO O'O 60 /P2_ 2.0 80 30-0 100 120 140 /3,9V 2&3Z- 21. f 20 3 //Y 200 Pan 0,f< Drytime: Static Plow: O / %./ Avg. Microns : /64~- Color L: /&0-fT a v.07 b / 4-? Technician: % VAB.0001198283 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Adardeen, Mississippi 39730-0091 Phone (501) 369-8111 IFICA A X OM Date: 29 May 91 Customer: Vulcan Plastics 207 Burham Athens, AL 35611 Attention; Billy Turner Date of Shipment: 24 May 91 Product: 5385 VB1A RAILCAR No.: VIPX-45842 Order No.: 006125-279 Property Moisture, V. Bulk Density, gm/cc Particle Size, V. on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR--2A ABR-3 ABGC-26 ABR-10 Analysis 0.03 0.566 0.00 8.1 1.9 0.93 Laboratory Supervisor/Lead VAB.0001198284 Vista Polyfliers Highway 25 Aberdeenv MS 39730 X LCAR ANALYSIS Load Date: Lgy Time Logged Product: 5385 Car No.: l. ogged In By: /77. /~ Ship Date: Silofs): 677-^v>-^>74 Customer: Moisture Contamination Bulk Density Fluff Hard Particle S% o 1st 2nd ________ 1st 2nd ^I / 2-- ..sHg'S v S~82-- 5 /S~~\ L,5lt> Viscosity RVCM Mesh/Glassi Screen Analysis Mesh 40 Weight qO X > *66 60 0 LX 80 jl(-/ 7 100 /XJ/ R2B 120 140 -2L 200 Pan O^L IS* / L3L Drytime: Static Flow: & / /Q* V Avg. Microns Color L: j>0 a ' O-Q ^b / Technician: N 4 VAB.0001198285 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 fe I F=* I C X ON Date: 24 Apr. 91 Customer: Vulcan Plastics 207 Burham Athens, AL 35611 Attention: Billy Turner Date of Shipment: 22 Apr. 91 RAILCAR No.: PLCX-46B69 Order No.: 806125-277 Property Moisture, 7. Bulk Density, gm/cc Particle Size, Y. on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR--10 -0 o Anal vs 0.05 0.589 0.00 5.6 0.100 0.93 Laboratory Supervisor/Lead VAB.0001198286 Vista Polymers rS t Highway 25 Aberdeen. MS 39730 h RAILCAR ANALYSIS Plcx Load Date: (-f ^ I ? f Product: 5385 Car No. : MC? $h 9 Time Logged In: 1 (& & O Ship Date : 2^ Silo(s): Logged By: Customer: Moisture Contamination Bulk Density 1 Fluff Hard Particle 1 1st 2nd 1 1st 2nd J> i .03 1 ~fT~ | 1 1st I 2nd I 1st 1 2nd | .0c^ 1________ 7 ,Q3 1 S' 1 Lsaff .S?o ________ 1 Viscosity RVCM Mesh/Glassi Screen Analysis Mesh 40 Weight % <9-0 Drytime: 60 J.1<S 80 !%&. 100 120 W a. o 140 zZ 200 Static Plow: e> / *5 Avg. Microns: Color L: /*0.0*7 a o.ol b !-G7 Pan 0_3O *.C> Technician: VAB.0001198287 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATION Date: 24 Apr. 91 Customer: Vulcan Plastics 207 Burham Athens, AL 35611 Attention: Billy Turner Date of Shipment: 22 Apr. 91 Product VIS1A RAILCAR No. PLCX-446B6 Order No.: 806125-276 Property Moisture, */. Bulk Density, gm/cc Particle Size, 7. on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 0.12 0.571 0.00 4.0 1.5 0.92 Laboratory Supervisor/Lead VAB.0001198288 Vista Polywers Highway 25 ^r s Aberdeen, MS 39730 A "4 flusX Screen Analysis Mesh 40 Weight Drytime 60 80 100 120 140 200 Pan Q.Z<? / 9e 0.74 ) 4.0 /.S' Static Flow: 0 /*?.Q Microns: Color L: 6? 7 a ti.ob b Technician: ^CtO VAB.0001198289 Vwto MyMn ADMakmof vtHQ UMica company mt A*a^1n--w--u--T- **}Kw PM OfRw Bok 91 39730 Phon (601I) 364994111 CERTIFI z ovm Date! Customer Vulcan Plastics 207 Burham Athens, AL 35611 Attentions Billy Turner Date of Shipments it Product:fy Trai1er No.: -rZu0 Lot No.s Order No 8 't Property Test Method Analysis Volatiles, 7. 6.950 Bulk Density, GM/CC 6.410 Brabender Dry Time,Mins. 8.450 Particle Size, V, on 6.300 40 Mesh 200 Mesh Pan Vinyl Chloride Monomer 8.955 Inherent Viscosity 8.600 Not more than 8.5 PPM This material was produced to yield an inherent viscosity in the rjgnge of 9^ to * Laboratory Supervisor/Lead VAB.0001198290 PVC BULK TRAILER ANALYSIS A Purticlc Si/c Distribution Scrson Analysis Mash Sin Gross Wl Taro Not Wt H on Mosh Scroon Analysis 40 >*& Mosh Sirs Gross Wt. Taro Not Wt H on Mosh Remarks 40 On Rotap shahsr. 40 gats. Rosin phis 1.0 pm. Carto 60 100 120 140 200 Glassy Pan Part. {(it . 3t( 2^ (X.C* On Rotap shafcor 40 gots. Rosm phis 1.0 gms. Carto Pan 100 120 140 200 Glassy Part. Star 207A Rosiaod 1/12/07 wv'- - IhlpSl nlhfjm ill 4A1 Vista Mj/iMfi ADMstanof MB UMBhI UiBpBIJr fijn1-w---w--- OaCw fat Ofnc* Box 91 Abwdawy Mmmmpyi 39730 PfcoM (dOl) 3A9-BT11 LETTER OF CERTIFICATION Data i f~/S''<U Customer Vulcan Plastics 207 Burham Athens. AL Attentions Billy Turner Date of Shipments Products Trailer No.s Lot No.s Order No.s Property Test Method Analysis Volatiles, 7. 8.950 Bulk Density, 8M/CC 8.410 Brabender Dry Time, Mins. 8.450 Particle Size, % on B.300 40 Mesh 200 Mesh Pan Vinyl Chloride Monomer 8.955 Inherent Viscosity 8.600 __ '~}~L_ __ __________ Not more than 8.5 PPM This material was produced to yield an Inherent viscosity in the range of to s 7cT . ____ ~ rylte3rry><*1 Labor at or y Sup ervisor /Lead VAB.0001198292 PVC BULK TRAILER ANALYSIS Date Customer Product Trailer Number. Time jff-y-g Order MOIST Bmom I CONT. Btwran GEL BULK DENSITY I DRY TIME I COLOR L* FRONT M1 1 1 > V1 if li | i 1 2* \- 11 I l. I i 11 It 1 MIDDLE I1 i 4 u1 i I I ow* * I i m11 A- 11 1 T.--------- ---------------- i. 11. I1 I END \- 0 A vise RVCM Particle Size Disiribuiion Scroan Analysis Mash Stea 40 Gross Wt Taro Nat Wt H on Mssli O* *>0 Scrosn Analysis Mash Size Gross Wt. Taro Nat Wt H on Masfi 40 On Rotap shakar. 40 gins. Rasm pkis 1.0 gms. Csrb ISO 120 140 200 Glassy Pan Part. UVjJZiL- U* 3.2 iS.4 to.l ~7. o Min. On Rotap sfiafcar .40 gms. Rasin plus t.O gms. CsTO 100 120 140 200 o.fs L2_ Glassy Pan Part. Remarks Star 207A Ravisad 1/12/07 1 II IMBilURi-- If'IP- - - - - - - - - - - - - - tfUSM 4r Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 X F I CA X OM * Date: 22 Apr. 91 Customer: Vulcan PIa sties 207 Burham Athens, AL 35611 Attentions Billy Turner Date of Shipment: 18 Apr. 91 Product: 5385 VISTA RAILCAR No.: VIPX-45870 Order No.: 806125-275 Propertv Moisture, 7. Bulk Density, gm/cc Particle Size, 7. on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analvsis 0.08 0.586 0.00 4.9 1.4 0.340 0.93 VAB.0001198294 Vista Polymers High* Aberdeen MS 39730 Load Date: Product: 5385 Car No.: Time Logged In: Ship Date :JL Silo( s ): Logged In By Customer & Moisture Contamination fv 1 1st 1 2nd . 3e V \ Bulk Density Fluff Hard Particle 1 I <ToR\ 1 /^B J 1st J 2nd 1st 1 2nd ^D ^ 1___ / <97 1 Ji " /O -rsV 1 1 i*J I 1st I 2nd 1 -p 1 1j 1 y~ 1 -stVi I 1 Viscosity RVCM Mesh/Glassi Screen Analysis Mesh Weight 40 v>BV % 60 73 80 100 120 140 200 Pan Ml IL 4? /.f Drytime: Static Flow: D. / ^ Avg. Microns Color L: !P&\0 ty* & -- &\ b Technician: VAB.0001198295 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A LETTER OF CERT I F I C^T I OIM Date: 17 Apr. 91 Customer: Vulcan Plastics 207 Burham Athens, AL 35611 Attention: Billy Turner Date of Shipment: 16 Apr. 91 VIS1AProduct: 53B5 RAILCAR No.: VIPX-45809 Order No.: 806125-274 Property Moisture, 7. Bulk Density, gm/cc Particle Size, 7. on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis 0.16 0.581 0.00 7.3 1.7 0.066 0.94 Laboratory Supervisor/Lead * VAB.0001198296 Vista Polymers T*Hig 25 Aberdeen, MS 39730 XXXXRAILCAR ANALYSIS Load Date: Product: 5385 Car No.: Time Logged In: JA.Ship Date : Silo(s): Logged In By: Customer (JO Moisture Contamination i 12nd 1st 2nd 1st 2nd 1st 2nd ./z Bulk Density Fluff Hard Particle Viscosity RVCM Mesh/Glassies Screen Analysis Mesh 40 Weight % o- Drytime: 60 !-^c> 3.C 80 is-,?? <s\9* s 100 (3-3! 24-U 120 140 2o,o //-2 200 5-tS" Pan L3. Static Flow: O /S^y Avg. Microns: v ^4- S Color L: a b I* Technician: VAB.0001198297 VbtoMpNMn AOtvWowof _____ VUb Cjiamied Company Hlghjnf25 RmI Offic* Boh 91 AbedM* MMstai39730 phof* |40D 369-irii ) LETTER OF CERTIFICATION Datat *? / Customers Vulcan Plastics 207 Burhain Athens, AL 35611 Attention! Billy Turnar Data of Shipment! y/ - /7 ? J VBIA^Products Trai1er No.i -r-'2-f$'> Lot No.s Order No.s 9>*5i5'7g ~ a*/ Property Test Method Analysis Volatiles, 7. 6.950 Bulk Density, Gh/CC 8.410 Brabender Dry Time, Mins. 8.450 Particle Size, % on 8.300 40 Mesh 200 Mesh Pan Vinyl Chloride Monomer 8.955 Inherent Viscosity 8.600 ____ Not more than B.5 PPM This material was produced to yield an inherent viscosity in the range of to . " Laborat VAB.0001198298 Customer Technician /? y / PVC BULK TRAILER ANALYSIS Product Particle Size Distribution Screen Analysis Mesh Size Gross Wt Tare Net Wt % on Mesh Screen Analysis Mesh Size Gross Wt. Tare Net Wt H on Mesh Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb Glassy Pan Part. 40 60 100 120 140 200 ^_ 40 o. 7,2_ -a*i ml. MJJL- >0.->? S21 J-C9 3v? 1L LSo Min. On Retap shaker 49 gms. Resin plus 1.0 gms. Carb Pan 60 100 120 140 200 Glasay Part. Remarks Star 207A Revised 1/12/87 ttMMapsavnfnsuM HUHBUN-nWOta ADMatonof Vhla Chornied Company Abardamy Mmmippi 39730 Phon* (601) 3694111 LETTER OF CERTIFICATION Dates f*7 ? ^ Customeri Vulcan Plastics 207 Burham Athens, AL 35611 Attentioni Billy Turner Date of Shipments 4L^/J,L / VISTA Products s5~7 8^S Trailer No.! ~f~. X Lot No.i Order No. t 9GLS^T'P} -0 02-- Property Test Method Analysis Volatiles, % 8.950 Bulk Density, 0M/CC 0.410 Brabender Dry Time, Mins. 8.430 Particle Size, 3C on 8.300 40 Mesh 200 Mesh Pan Vinyl Chloride Monomer Inherent Viscosity 8.955 8.600 AJJ)_ ^S79 __^57_/_ __Q.'JL.__ ______ 2* Not more than 8.5 PPM This material was produced to yield an inherent viscosity in the range of to ______________________________________________ Laboratory 8upervisor/Lead VAB.0001198300 Customer PVC BULK TRAILER ANALYSIS Particle Si/.c Distribution: Screen Analysis Mesh Size 40 Gross Wt Tare Net Wt H on Mesh D &.*o Screen Analysis Mesh Size Gross Wt Tare Net Wt H on Mesh 40 Min On Rotap shaker. 40 gms. Resin plus 1.0 ams. Carb 60 80 100 120 140 200 Glassy Pan Part. JJui ~S.fl. ~J.eS Jii 2?J 214 Ml 22. 2.S Min. On Rotap shaker 49 gms. Resin plus 1.0 aim. Carb 100 120 140 200 Pan Glassy Part. Remarks Star 207A Revised 1/12/87 --- i min 98301 { Vista Polymen A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730*0091 Phone (601) 359-8111 IF I CA x orvi -f Date: 15 Apr. 91 Customer: Vulcan Plastic Burham Athens, AL 35611 Attention: Billy Turner Date of Shipment: 12 Apr. 91 Product: 5385 VISIA RAILCAR No.: GACX-73389 Order No.: 806125-272 Propertv Moisture, 7. Bulk Density, gm/cc Particle Size, X on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis 0.08 0.578 0.00 11.2 2.2 0.070 0.94 Bi 1 emore Laboratory Supervisor/Lead VAB.000110S3O2 Vista Polymers Highway 2 A Aberdeen. MS 39730 RAX L OAR ANALYSTS Load Date Time JJLShip Date: 12, Product: In: 0l3& 5385 9/ Car No Screen Analysis Mesh 40 Weight 0,5 o % O,& 60 Cl`3 0 U- 80 iAl_ 100 /&/* 120 . 77 140 7.9/ /4~p 200 &L2 U-3l Pan JJA 3 Drytime: Static Flow: & / /Oi.'Q Avg. Microns: / H Color L: !6 0* H# a Dt O'l' b Technician: VAB.0001198303 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 AdenJeen, Mississippi 39730-0091 Phono (601) 369-8111 OF I ON Date: 15 Apr. 91 Customer: Vulcan Plastics 207 Burham Athens, AL 35611 Attention: Billy Turner Date of Shipment: 11 Apr. 91 Produc t: RAILCAR No.: VIPX-45910 Order No.: 806125-271 Proper tv Moisture, 7. Bulk Density, gm/cc Particle Size, V. on 40 Mesh 200 Mesh > Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis 0.13 0.00 5.6 1.8 0.047 0.93 H.D. Lucas Laboratory Supervisor/Lead VAB.0001198304 Vista Polymers Highway 25 Aberdeen* MS 39730 Load Date: Cr-^t I RAILCAR ANALYSIS Producti 5385 Car No.: i/ /y 7 Time Logged In: l&cf Logged In By: Ship Date Silo( s ): Customer: 4 I A I CA Moisture Contamination 1 1st I 2nd | , f0 \ 1M 17 1 I 1st I 2nd | ,q \ 1 _5L 1 17 1 CB 1st I 2nd is 1 Bulk Density Fluff Hard Particle Viscosity 1 | J y^ | / / RVCM 40 Mesh/Glassies \.S7f\ II 11 1 <s.ns 1 H 11 11 B 1st 2nd , n't- ...ii . ?o Screen Analysis Mesh 40 Weight % o.o 60 80 22- [Ml 37,k 100 Ml 5U 120 /4.P Drytime: S.D Static Flow: 0 ftf.0 140 200 Pan Xfz .if a , ISf-9 Avg. Microns Color L: /0&- </o a OOl b J^2. Technician: VAB.0001198305 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Offiice Box 91 TI Adsnksn, Mississippi 39730-0091 Phone (601) 369-8111 4 X I ON Date: 12 Apr. 91 Customer: Vulcan Fla sties 207 Burham Athens, AL 35611 Attention: Billy Turner Date of Shipment: 12 Apr. 91 VIS1AProduct: 5385 RAILCAR No.: VIPX-45Q20 Order No.: 806125-270 Propertv Moisture, V. Bulk Density, gm/cc Particle Size, 7. on 40 Mesh 200 Mesh Pan Residua 1 VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analvsis 0.21 0.591 0.00 5.2 1.6 0.705 0.94 Bi lJKy P. re Laboratory Supervisor/Lead VAB.0001198306 Vista Polymers Highway 25 Aberdeeni MS 39730 A RAILCAR ANALYSIS Load Date : M Product 5385 Car No ... Time Logged In: D ^ V^O Logged In By: Ship Date: 21 Silo ( s ): k 7L1l77 L<& Customer o Screen Analysis Mesh 40 Weight % 0.0 Drytime: 60 40 . + 80 10.5 3 <0.9 100 120 ?. 3-3 140 8^ 200 -1.55 S"-l_ Pan 1*t Static !Flow: o Avff. Microns: `2 Color L : 1 CD. 2 ^ a O'Qj b / Technician: &S VAB.0001198307 1 I- Vista Polymen A Division of Vista Chemical Company Highway 25 Post Office Box 91 Adenfeen, Mississippi 39730-0091 Phone (601) 369-8111 A LETTER OF CERT I F I CAT I ON Date: 3-19-91 Customer: Vulcan Plastics 207 Burham A t hen s , AL 3 5611 Attention: Billy Turner Date of Shipment: 3-18-91 Product: 5385 VISIA RAILCAR No.: VIPX-45856 Order No.: 806125-269 Property Moisture, 7. Bulk Density, gm/cc Particle Size, 7. on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis 0.14 0.556 0.00 9.x 1.9 0.351 0.93 Laboratory Supervisor/Lead VAB.0001198308 Vista Polymers 4 Highway 25 Aberdtent NS 39730 PVC RATLCAR ANALYSTS 4 Screen Analysis Mesh 40 Weight % O'C? Drytime: 60 80 100 120 140 200 Pan Static Plow: S'?.0 9./ LA /<&Y:Avg, Microns Color L<` ^ft ^'OO b Technician: w fBPgilWF'P' VAB.0001198309 V Vista Polyman 25 Adetdeen, Mississippi 39730-0091 A Division of e Box 91 Phone (601) 369-8111 Vista Chemical Company &F? QF IF I I OM Date: 3-19-91 Customer: Vulcan Plastics 207 Burham Athens, AL 35611 Attention: Billy Turner Date of Shipment: 3-18-91 Produc t: RAILCAR No.: UTCX-46499 Order No.: 806125-268 Proper ty Moisture, V. Bulk Density, gm/cc Particle Size, V. on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis 0.16 0.548 0.00 4.0 1.6 0.500 0.91 H. D. Lucas VAB.0001198310 Vista Polymers Highway 25 Aberdeen MS 39730 4 PVC RAILCAR ANALYSIS v UTZ-X Load Date:3-It, -?/ Product: 5385 Car No 4L4 97 Tine Logged In: /76 ^ Ship Date: 3 Silo(s): In By: Customer Vio W\GrHV\ Moisture Contamination Bulk Density Fluff Hard Particle A 1 CA 1 1st 2nd I^ 31 iO I 1st 1 -09 13 I ! *> 2nd 1 ('<CB ' 1st I 2nd 1 ,08 1 f\ /S' 1 1 fb \ I1st 2nd y'O 1J | /P 1 1 I Viscosity RVCM Mesh/Glassi soO Screen Analysis Mesh 40 Weight % a. o 60 O. SO 80 100 120 1^,4 / So.S> 140 3.!3l (,2 200 I^S 4.0 Pan /L Drytime: Static Flow: # / ^ P Avg, Microns: * ^ Color L: a b /,9g Technician: VAB.0001198311 Vista Polyman A Division of Vista Chemical Company Highway 25 Peat Office Box 91 Aberdeen, Mississippi 39730-0091 ' Phone |601) 369-6111 IFI C^"T X a IVI Date: 3-19-91 Customer: Vulcan Plastics 207 Burham Athens, AL 35611 Attention: Billy Turner Date of Shipment: 3-18--91 Produc t RAILCAR No.: PLWX-44673 Order No.: 806125-267 Property Moisture, 7. Bulk Density, gm/cc Particle Size, 7. on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis 0.14 0.577 0.00 6.5 1.5 0.605 0.94 Laboratory Supervisor/Lead VAB.0001198312 Vista Polyners Highway 25 Aberdeen, MS 39730 Load Date: Tine Ship Date: PVC RAILCAR ANALYSIS PLlJY Product: 5385 Car No.: 4 Screen Analysis Mesh 40 60 80 100 Weight % Drytime: Static Flow Color L: a 120 140 200 L Avg. Microns: b Pan Technician: K. VAB.0001198313 I!.. * Vislo Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 I Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 * A i oi\j Date: 3-15-91 Customer: Vulcan Plastics 207 Burham Athens, AL 35611 Attention: Billy Turner Date of Shipment: 3-14-91 Product: 5385 RAILCAR No.: PLWX-44717 Order No.: 806125-266 Proper tv Moisture, 7. Bulk Density, gm/cc Particle Size, 7. on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 o'O o Analvsis 0.564 0. OO 3.7 1.7 O . 012 0.92 i H.D. Lucas Laboratory Supervisor/Lead mrnrnmmmm VAB.0001198314 Vista Polymers Highway 25 Aberdeen9 MS 39730 j4 RAILCAR ANALYSIS Load Date : , ? --/3 Product: Car No. : ^^*7/ 7 Time Logged In: sO Ship Date \-2>' /4~^9/ Silo(s): Logged In By: Customer Moisture Contamination 2nd 2nd 1st 2nd Bulk Density Fluff Hard Particle Viscosity RVCM 11 <$~2P 1 , #/2. Mesh/Glassies 11 Screen Analysis Mesh Weight 40 0.0 V % O.0D Drytime: 60 0 80 Lk ,0 100 Mi2 120 LLL 140 43- ZOO Static Flow: 0 / ^\b Avg. Microns Color L: / 00, a b 2nd Pan lX- Technician: A.A. 4* VAB.0001198315 Vista Polymers A Division of Vista Chemicol Company 14 Adsidssn, .Mississippi 39730-0091 Phono (601) 369-6111 LETTER OF- CERT I F I CAT I ON Date: 3-13-91 Customer: Vulcan Plastics 207 Burham Athens, AL Attention: Billy Turner Date of Shipment: 3-12-91 Product: 5385 VKIA RAILCAR No.: UTCX-46511 Order No.: 806125-265 Propertv Moisture, V. Bulk Density, gm/cc Particle Size, 7. on 40 Mesh 200 Mesh Residua1 VCM, ppm Inheren t Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis 0.06 0.00 6.0 1.6 0.93 H.D. Lucas Laboratory Supervisor/Lead VAB.0001198316 1 Vista Polymers Highway 25 Aberdeen, MS 39730 3Load Date: Time Logged In:. Ship Date: Product: 5385 Car No.: Logged In By: U. Y 44^7/ Moisture Contamination 2nd CA 1 st 2nd Bulk Density Fluff Hard Particle Viscosity RVCM JL 40 Mesh/Glassies Screen Analysis * Mesh 40 Weight fit &0 % 6-so Drytime: Static Flow: Color L: Microns: Technician VAB.0001198317 ^ I aJ^rwMV^,*gJ-iW K* ^ 1^,1 +-*1***X 1 . '"-L J r P* ""h ..'Vb . .< V' ' h -' | ."-n"'1* \ \ w'-'^r > './..V1'." ^ ` ^'r 'V' i-^wk -1-iTiP# bn | Mh *+ ^-n'ki fr i ' I i-* tj|#r ^ *' h *'' :` '< ' "' ' I- 1>ti 'l'-\i''-*, j- **'!'- 4-'-:ph',^l ' 11 "J |.\'Lt ''"V, V h '*% - 1/ ' ''l-,h-` 1 -H . '" V ''V-i V-J' VL + 1`lI' ' \ 1- V'h ^VV.^Vb '"h ^'' *VfcV -*r>, '^ji, \vv,1 ^ _.'. \ V1 i,-i ^ v.itwi \ ^ '* V|^V 1 V'V V-* V*,-*%"I \ r Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-009) Phone (601) 369-8111 OF 3-14-91 Customer: Vulcan Plastic 207 Burham Athens, AL Attention: Billy Turner Date of Shipment: 3-12-91 X OKI Product: 5385 VBft RAILCAR No.: PLWX-446B0 Order No.: 806125-264 Pr9Per^Y Moisture, 7. Bulk Density, gm/cc Particle Size, 7. on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analvsis 0.11 0.585 0.00 6.6 1.5 0.227 0.93 H.D. Lucas Laboratory Supervisor/Lead u VAB.0001198318 Vista Polymers Highway 25 Aberdeen* MS 39730 4 Load Date: J7/- *7/ Product: 5385 Car No.: Time Logged In: Ship Date ~^/ Silo(s): Logged In By: Customer: Screen Analysis Mesh 40 Weight X hiOtf 0 -DP 60 AW Z3 80 iZJt .Vi-V 100 'LS'd 120 140 200 Drytime: n(oStatic Plow: o Avg. Microns Color L: a b L2l Pan L Technician: 2> S VAB.0001198319 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 LETTER OE CERTIEIOAT ION A Date: 8 Feb. 91 Customer: Vulcan Plastics 207 Durham Athens, AL 35611 Attention: Billy Turner Date of Shipment: 6 Feb. 91 Product: 5385 RAILCAR No.: VIPX-45785 Order No.: 806125-263 Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity ABR-1A ABR-2A ABR- 3 ABGC-26 ABR-10 0.08 0.580 0.00 7.7 2.0 0.169 0.93 y P. Laboratory Supervisor/Lead * VAB.0001198320 Vista Polymers A " V.T Highway 25 i Aberdeen, MS 39730 / RAILCAR ANALYSIS Load Date: Tine Logged Ship Date: *7/ Product 5385 Car No.: Silo(s): Logged In By: Customer I/iaI ~Plasht Moisture Contamination Bulk Density Fluff Hard Particle 1st 2nd 1st I 2nd , a r1 /7S~ 1st I 2nd JL.- 2? ! 1st I <*>7 A- -U 2nd Viscosity RVCM Mesh/Glassies Screen Analysis Mesh 40 Weight % 0 xO 0 60 80 100 120 140 200 i2L /Z,7^3 /f-3? AM Uh~~ lLl Pan Drytime: Static Flow: Q / &*l Avg. Microns: Color L: ab Technician: * * i VAB.0001198321 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A I-- ETTER CD CERTIFICATION Date: 5 Feb* 91 Customer: Attention: Vulcan Plastics 207 Burham Athens, AL 35611 v Billy Turner Date of Shipment: 4 Feb. 91 Product: 5385 VIS1A RAILCAR No.: ACFX-41150 Order No.: 806125-261 Propertv Moisture, 7. Bulk Density, gm/cc Particle Size, 7. on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analvsis 0.10 0.00 7.7 2.1 0.206 0.93 Laboratory Supervisor/Lead VAB.0001198322 Vista Polyaars Highway 26 Abardaan, MS 397$0 3 k HAILCAR ANALYSX S Load Date: Product: 5385 ? Car N 4//so Time Logged In: /3c>c> -tJzL Ship Date Silo(s): Logged In By: Uf, Customer: /TO 1st 2nd 2nd 1st 2nd j 1 1 i Moisture Contamination Bulk Density Fluff ______________ V l^ l \r57t> 1 I fad _________________________________________________________ I 1 ,j57? | .a*? 7 n ________________________________________________________ 1 I , /o ( "9 ,5i<f Hard Particle Viscosity -- 1 04Q 1 RVCM Mesh/Glassi 2nd Screen Analysis Mesh 40 Weight X 0.0 Drytime: 60 3.? 80 /i-3? 33.2 100 2'f.o 120 /0.2a. /9.<jC 140 ^73-? )0. -y 200 2:2 Pan 2./ Static Flow: 0 / Avg. Microns: I C"? .-Q Color L: !0o~o4 a O./C h /-CfC Technician: / ^?j VAB.0001198323 *. * -y. Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A I-- ETTER OF* CERTIFICATION Date 5 Feb. 91 Customer: Vulcan Plastics 207 Burham Athens, AL 35611 Attention: Billy Turner Date of Shipment: 4 Feb. 91 Product: 5385 VISIA RAILCAR No.: ACFX-53140 Order No.: 806125-262 Propertv Moisture, '/, Bulk Density, gm/cc Particle Size, 7. on 40 Mesh 200 Mesh Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis 0.11 0.00 7.4 2.4 0.248 0.93 Laboratory Supervisor/Lead VAB.0001198324 Vista Polyapa Highway 25 Abrdn MS 39730 >. P Load Date * RAILCAR ANALYSIS lz-P Product: 5385 Car No*: SCFX 3/<& Time Logged In: Logged In By: Ship Date Silo(s): Customer /V 0 1 Moisture Contamination Bulk Density Fluff Hard Particle 55 1st I 2nd 1 !Q> 1 .S'? 7 1 ( CA) 1st 1 2nd | 4 &> 1T ,S79 1 1st 1 2nd / // / F 1 1 L ssr I (fgjj 1st I 2nd , i1 k1 .sig 1 1 Viscosity RVCM Mesh/Glassies Screen Analysis Mesh 40 Weight % Q*i> Drytime: 60 80 100 120 140 200 Pan mo // 24 & l'/8 2.9-V 23 A a / /. & Static Flow: <Z> ^ Avg. Microns: I Cf< Color L: /GG*/>~ a b A* Technician: VAB.0001198325 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 4 LETTER OF- CERT I F" I CAT I ON Date: 4 Feb 91 Customer: Vulcan Plastics 207 iBurham Athens, AL 3561 Attention: Billy*Turner Date of Shipment: 1 Feb. 91 Product RAILCAR No. Order No.: B06125-260 Propertv Moisture, 7. Bulk Density, gm/cc Particle Size, 7. on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-iA ABR-2A ABR-3 ABGC-26 ABR-10 Analysis 0.03 0.577 0.00 6.0 1.7 0.192 0.92 Laboratory Supervisor/Lead it^ii ii-r1 VAB.0001198326 Vista PoXyaars KZii. fir* Highway 25 / A AMrdMHi NS 39730 RAILCAR ANALYSIS Load Date So Product 5385 Car No.: Time Logged In: OS O Logged In By: Ship Date: Silo(s): GS1 Customer cr at Moisture Contamination Bulk Density Fluff Hard Particle 2nd 2nd ,03, ______ , Q (o I ^ S? S' yg iS'fllr <^74\ 2nd , oJS'j Y i US7J\ 1st t d6 A /7 2nd Viscosity RVCM Mesh/Glassi Screen Analysis Mesh 40 Weight QC> % C>-o c) 60 80 100 120 140 200 Pan 3/e 2-/.J Drytime: Static Flow: Avg. Microns: /&7 Color L: ab Technician: MVHtHirtH-fwm VAB.0001198327 4 HHmHUHiWMPhi' MHIIMir(ii|lr-IIPHIPI'H "HlHUHP'it-IHiimiH1' lUMPPHf'- :.hi m- "iiiHirm- :n''ril>l''PU'iMEIPiM''i||iHini*VtHniltfMrmTm'''i'fVmM''HP)i|r*f|fVV|VniVVVIIVffVIVTflVVni|^VfnriinVVVfflP'M1tflf0V|VVVf|||^^ 1 !''hlllHVn4ltfftflVffVl|ff1l<h||t1|fHhPHIPW<l|iPV!!fV1IIMHpU>VU)ltHI|IPMpPfHi`' 'mM*ftMIHP'tnttHMt1TPPnMP'l'P*pMtHMP*'r'|nfPtf}tttfirfEiiH'|Hlflpfi|'tlPM!PlH4prHi'P-'t"P-'PlHPNl<HI|IH''>MJi-iljMiENm''|H. ..i|ii,r . 1 -i-- i" - -kf^m -mi.. - m- - w rP- hIi-'m.......in. -; m i- IIH'^MP i'll. H i I I I I I I J I I I I I I I I ! i I I I I I I 4 VAB.0001198328 Vista Polymers To: Mark Manion Highway 25 P. 0. Box 91 Aberdeen, MS 39730 Date Fax Sent: 8/30/91 OFFGRADE RAILCARS Railcar No.: VIPX 45703 . UmOrrJLLoad Date: 8/08/91 Customer Product: Pond Resin Ship Date: iO fafa State: Test A CA CB B 4 Moisture Contamination, Blk. Contamination, Brn. Bulk Density, gm/cc % on 40 Mesh % thru 140 Mesh % on Pan L Color b Color Inherent Viscosity RVCM .43 1000+ 1000 + .480 0.9 15.7 5.3 69.70 6.28 0.863 0.003 .31 1000+ 1000+ .440 3.4 14.5 5.8 74.11 6.20 0.879 0.198 .32 1000+ 1000 + .427 3.4 14.8 5.4 73.54 6.30 0.878 0.002 .37 1000 + 1000 + .467 0.8 15.4 6.2 71.25 6.09 0.871 0.001 J. Richard Williams Quality Control Supervisor VAB.0001198329 .L Vista Polymers Highway 25 Aberdeen MS 39730 iT Load Date Time Logged Ship Date: Product 4S1o3 *2^4l Logged In By: Silo(s): 4>?jr Customer: Moisture Contamination / M / Bulk Density Color ML" Color MaM Color "b" Static Flow Viscosity RVCM Screen Analysis . L9. 70 D. 70 L.2.P O' H.U .9&2> 60.3 .44 o 74. U $% (q (p C>. 2.0 2- Mesh Weight % 40 0.<79 0.4 60 1.13 80 /0. 27,2. 100 II.39 23.? . 32. / .4&n 73-SV O.^tf X 113. f 002* 120 7c.fl At.4 140 7.3/ ?4.U .37 / .4 (*7 7/.2S* (o Qty I / /c.s . 77/ .oof 200 S. 2-1 70.9 Pan Weight CA % /. 70 3- I.S9 3- 2- II. s4 33.1 n.4 33-n '> & J9.3 (e.fO 729 4.27 <?. 7 2.9? jr. f Weight % l.bl 3.4 1.1*3 /6. So II. ss' 70.3S' 23.1 JC.S- /3.3 4. 72. 9.4 Weight % _q.4 of 1.49 3.0 It.4 7 22-4 12.1304.3 iQ. 2 b '-20.2. (e.lol J3-4 4.3$ 3.10 4.2 Technician: VAB.0001198330 Vista Polymers To: Mark Manion Highway 25 P. 0. Box 91 Aberdeen, MS 39730 Date Fax Sent: 11/18/91 4 OFFGRADE RAILCARS Railcar No.: ACFX 41163 Load Date: 11/14/91 Customer: : flJlzoWProduct: Debox Ship Date State: fir Test A CA CB B Moisture Contamination, Blk. Contamination, Brn. Bulk Density, gm/cc % on 40 Mesh % thru 140 Mesh % on Pan L Color b Color Inherent Viscosity (Top) Inherent Viscosity (Bot) RVCM .22 50 100 .415 0.0 36.4 8.9 99.17 1.76 0.813 0.809 0.219 .04 100 250 .554 0.0 29.6 6.4 99.35 1.87 0.868 0.886 0.069 . 22 55 200 .402 0.0 38.5 9.7 98.30 2.24 0.807 0.779 0.081 .08 100 500 .543 0.0 24.1* 5.4 99.33 1.99 0.868 0.877 0.073 J. Richard Williams Quality Control Supervisor VAB.0001198331 Vista Polymers Highway 25 Aberdeen MS 39730 Load Date 7/ Product Car No.: Time Logged In:. Igoo Logged In By: Co Ufl(*3 Ship Date: Silo( s ) : (oS^ Customer: Moisture Contamination It* / Z SO . 2 2- SS~/ 6 0 oT /*/ SO0 Bulk Density Color If V If Color ft M Color ff . V/jr Q. // Static Flow Viscosity * /o.L '877 RVCM Screen Analysis .on^b Mesh Weight % 40 0.0 Q. Weight CA % QiO 0 Weight % p-qQ o ,0 60 . os" 80 7/7 1J M 21 V* J.gS' ll.2 100 ZiZ. l. 2. *l.7f J3A 7 17.7 120 140 200 Pan 7-7jt fy.it/ L 2 !6 .S S 2L1 ff.il BA. list ?.zt tiL to . Y h&z. /g-yz. /y.y/i 2o.7 JgJ 51.8 7.7 Weight % L p .o i_ L2iL //v51? 22. F /^7 ,g.P Technician: VAB.0001198332 Vista Polymers t Highway 25 P. 0. Box 91 Aberdeen, MS 39730 To: Mark Manion Date Fax Sent: 10/19/91 OFFGRADE RAILCARS Railcar No.: VIPX 45765 Load Date: 10/09/91 Customer: Product: Debox Idhl Ship Date: i/ State: Test A CA CB B Moisture Contamination, Blk. Contamination, Brn. Bulk Density, gm/cc % on 40 Mesh % thru 140 Mesh % on Pan L Color b Color Inherent Viscosity (Top) Inherent Viscosity (Bot) RVCM .12 22 30 .530 0.0 28.2 6.0 100.03 1.34 0.933 0.953 0.025 .08 25 20 .530 0.0 28.9 5.7 100.03 1.28 0.939 0.938 0.036 .03 98 47 .556 0.8 9.8 1.8 99.01 0.79 0.829 0.915 2.689 .15 42 29 .586 0.0 12.2 2.1 99.72 1.23 0.918 0.894 0.001 J. Richard Williams Quality Control Supervisor H t* LOW m VAB.0001198333 Vista Polymers Highway 25 Aberdeent MS 39730 RAILCAR ANALYSI OFFGRADE Load Time Logged Ship Date: Product lr>-R3g( Car No.: L Silo(s ) : Logged In By: &&A 23. Customer 4 Screen Analysis Mesh We i gh t X 40 >. &0 /5L 60 O -AT /> 2 80 100 /Z> 120 140 1(13 IML 2^9-. 93.9 200 99. a Pan 38 Weigh t CA % 0. 00 0. )($ 63 <tk 3,1 lh 111* l& *f-7 lib 0 We i gh t CB % <0.V*2~ *-8 -L5. /9.0O We i gh t % 0. te> no 6, 6,0 f.9. u.r2 99.8 239 ]1 3.0 o.*2 18 Ms /57 ap to. I 31 Technician: ( VAB.0001198334 ^feMI ra^4.- iikju .. Vista Polymers To: Mark Manion Highway 25 P. O. Box 91 Aberdeen, MS 39730 Data Pax Sant: 5/29/91 OFFGRADE RAILCARS Railcar No*: GACX 73385 Load Date: 4/29/91 : lAJOf&Yd Customer Product: 5415 Ship Date: // State: Test CA CB Moisture Contamination, Blk* Contamination, Brn Bulk Density, gm/cc 7 Minute Hard Particle % on 40 Mesh X thru 140 Mesh X on Pan L Color b Color Inherent Viscosity RVCM .15 2 6 .523 50 0'0 4.9 1.3 100.61 1.51 1.038 0.021 .16 2 7 .510 50 .14 1 9 .523 3 .19 2 11 '516 50 Composite Result J. Richard Williams Quality Control Supervisor VAB.0001198335 Vista Polymers Highway 25 Aberdeen< MS 39730 TP\T C RAILCAR ANALYSIS 4 Load Date: Tine Logged Ship Date: Product: 5415 Car No.: Logged In By: Silo(s): Custoner: bio "j3eA^S Analysis Mesh 40 Weiffht >'> X Oo 60 O./S G>. 80 17.0<f SvC / 100 ti>.W 33 n. 120 q.JlO 140 ?/ 200 i-2f Pan O. ") Drytiae: Static Flow: y /! Avg. Microns: ICS. ^ Color L: loo,cr 0-oi b < S { METS: 7X Technician: 7X- JifS VAB.0001198336 FROM:UISTA 1 TO:LAB NOU 7, 1991 2M7PM 479 P.01 VISTA POLYMERS b A DIVISION OF VISTA CHEMICAL COMPAm 0071321 000043S3501 VISTA CHEMICAL COMPANY P. O. BOX 71321 CHICAGO 60694 GUST# SSS3713 WEXFORD P 0 BOX INTERNATIONAL 520 MENDHAM 07945 30604 0002555000 ii/OS/91 O PAGE HAW KPLASTICS COOSA PINES SIDING COOSA PINES 3S044 i 12314 NET DUE IN 30 DAYS -0000000 000255"000 FOB ORGIN FRT PPD RAIL 0002255-000 0/00/00 1 g GRADE/DEBOX RESlNiAi) RESR# 10S15 VIPX 45814 175,400. 00 LB THIS REPLACES ORDER 1BS5 WHICH DID NOT SHIP. be!shtolAN6ED from *19 T0 * 18 0N N0V 5- per JIM THIS IS NOW OFF CUSTOMER HOLD. PLEASE SHIP THIS . 190000 33,326. 00 REQUEST DATE PROMISE DATE 91/11/16 91/11/06 #**#*#############*#*### i ACKNOWLEDGEMENT * ##*## # * i .i m T ip** 33,326.00 VAB.0001198337 FRDM ' UISTR 1 LOADING ORDER DATE PREPARED HfrF W\ 1+t i I I I WW'HM ORDER NO.: SHIP DATE: CUSTOMER SPECIAL INSTRUCTIONS TD:LflB Aberdeen Chemical Plant NDU 7, 1991 2:48PM 8478 P.02 VIDIM /* 4 PH 1 * WM <11 11 II I PRODUa TYPE PRODUCT FROM YARD LOADING AUTHORIZED SIGNATURE LOADED/SAMPLED BY APPROVED BY TIME/DATE TIME/DATE COMMENTS: * 1111'1`fI'lTi | iiem mini FWlflH T^lil^e||i iiniiwwr mi tup......in > irrmr f w> >> '> i n tmimrii n BP^WF 'e U1 I YARD OPERATOR SHIPPING INSPECTION n CAR/FRAILER INSPECTED BY* * m> * i*ii ti l dMi mt+s+miM TIME/DATE: - PRODUCT LAST CONTAINED: APPROVAL FOR LOADING: RAILCAR INSNCTION COMPARTMENT W**P PRODUCT IN CAR DOMELIDS WALKWAYS HANDWHEELS CAPS LOCKING ARMS CAP HOLDERS/LOCKS PUNCTURES mmrnMmmM I- o.lc, ip ph 1 PPoM*m CB B CAR/TRAILER APPROVED YES NO GENERAL APPEARANCE - GOOD / FAIR / POOR *4- H111 I TRAILER INSPECTION TIRES TRAILER BODY CONDITION i I DOME LIDS (INCLUDING GASKETS) HOSES (IF USED) UNLOADING/SAMPLE VALVES mtm*\ e. LANDING GEAR (UOlLEY LEGS) DUST CAPS (U/L LINE CAP) MUD FLAPS WINTERIZATION NEED TO WASH O YES NO COMMENTS VI2-29-X5 Rv. 7/90 I IP*" I p1,p "N" * |I W VAB.0001198338 TRANSMISSION CONFIRMATION REPORT No.=000125 DATE/TIME DURATION TRANSMITTER C FROM) OCT 28i 1991 3:47PM 40s UISTA QC LAB-ABERDEEN 601 369 3642 RECEIUER CTO) PAGES XMITTED PAGES ERRORED 02 RESULT OK COMM. MODE G3 RESOLUTION NORMAL 2015436820 * 11 * VAB.0001198339 55-0000349 I 1 I R UCK LINES, INC *ir' 'SSGfrY * TP-: 6>2D *f ht-k* .0001198340 Vista Polymers Highway 25 P.0.Box 91 From u)'M Date: Aberdeen, MS 39730 To saX. 4 Comments: Number of pages excluding cover -- VAB.0001198341 ' *|H O I K^VMfhH'Mnmn tpur.BL.a. i. Vista Polymers To: Mark Manion Highway 25 P. 0. Box 91 Aberdeen, MS 39730 Date Fax Sent: 9/03/91 OFFORADE RAILCARS Railcar No: VIPX 45814 Load Date : 8/16&27/91 Customer: l L Product: Debox Ship Date State: Test A CA CB B Moisture Contamination, Blk. Contamination, Brn. Bulk Density, gn/cc % on 40 Mesh % thru 140 Mesh % on Pan L Color b Color Inherent Viscosity (Top) Inherent Viscosity (Bot) RVCM 02 2 146 .553 0.0 19.2 2.6 99.16 1.75 0.662 0.011 .08 2 139 .553 0.0 15.7 2.1 99.29 1.71 0.659 0.019 .08 3 183 .543 0.0 20.4 5.3 100.28 1.50 0.759 0.925 0.368 .04 3 120 .573 0.2 11.6 2.3 99.51 1.33 0.746 0.837 0.015 Compartment A & CA contain 5265 offgrade. There were no top IV samples J. Richard Williams Quality Control Supervisor VAB.0001198342 O Vista Polymers Highway 2 5 Aberdeen* MS 39730 OAaaQcI 73 [LCAR A j_ o 4 Load Date : $~/L "9/ Time Logged In: Product : l&gBftY Car No.: 45$/4 Logged In By: M&. Ship Date: Silo(s) : Customer: Moisture Contamination Bulk Density Color "L" Color "a" Color "b" Static Flow Viscosity RVCM Screen Analysis Mesh 40 Weight 0*0o % . oA ^ J!4(p . oZ 2 'IS? .553. 99. / .53. 1 99.29 c*7'S' /. '75 >. 70 1 /7/ .of S UfJ 1 0<f 3 / Iko .*73. /CO.Zf o./L /'J?Q__________1 94.5! C. f?9 1.33 1 1 1 C. <o Z. . o // /to Tops 60 80 o. QJh AlCA 100 S.'JS /7-Sr tf. c9 /J-tl 2(p. 2- AA t/zifo Pan 8.9.9 jL11 UtJe. 2-U Weight CA % COO O.o SL , oG Shi s.i5 /0.3 to .o 8 30-2- UL tas<f b. 8o /. 0 o^ [ Weight % 0-0 / 0*0 3\ to L. 2. Weight 0.0% X SL JSk /0 n.zz aa.4 /QZf 9S4 19.1 H.4? 24/o Ip. l/o 5.\ S.o</ V LL> 9-3 / /< . 23 Technician: VAB.0001198343 Vista Polymers To: Mark Manion Highway 25 P. 0. Box 91 Aberdeen, MS 39730 Date Fax Sent: 9/25/91 A 0FF6RADE RAILCARS Railcar No.: ACFX 41166 Load Date: 9/21/91 Customer: Product: Debox Ship Date: State: Test A CA CB B Moisture Contamination, Blk. Contamination, Brn. Bulk Density, gm/cc X on 40 Mesh X thru 140 Mesh X on Pan L Color b Color Inherent Viscosity (Top) Inherent Viscosity (Bot) RVCM .06 5 66 .544 0.0 10.0 2.5 100.02 1.49 0.885 0.927 0.038 .04 9 75 .518 0.0 4.9 1.8 99.43 1.39 0.971 0.963 0.062 .09 6 88 .548 0.0 9.6 2.4 100.02 1.47 0.868 0.964 0.006 .05 65 45 .521 0.0 4.8 1.4 98.99 1.28 0.893 0.928 0.095 J. Richard Williams Quality Control Supervisor VAB.0001198344 Vista Pc/lyifce Highway 25 Aberdeen, MS 39730 RAX LOAR ANALYSXS 4 Load Date: Product: Car No.: Time Logged In: Logged In By: Ship Date: Silo(s): Customer Moisture Contamination Bulk Density Color ML" Color "a" Color "b" Static Flow Viscosity RVCM Screen Analysis Mesh 40 60 80 100 0 Weight D-0 O ,(fV Ml ((/. $ z % 0.0 __J_ 23. 23jg 120 140 200 Pan S-7S /.3J ?.r 3.S' Weight CA % Weight vDO n % O.oo ............ O.0& .So g>.o &3T 13.90 317 221 JSS , 92 S2J- 21_ 13 cv//46t> lSS UM 3-ft /ll J2J3 M3 RS 7.2. 2SL 0 Weight .00 % DfV 121 3.70 M3_ .7o n.u -M- 3A -MIL Technician VAB.0001198345 Vista Polymers To: Mark Manion Highway 25 P. 0. Box 91 Aberdeen, MS 39730 Date Fax Sent: 10/02/91 A OFFGRADE RAILCARS Railcar No.: ACFX 41136 Load Date: 9/28 : (A)(Ia Customer Product: Debox Ship Date: 10 _________________ State: Test A CA CB B Moisture Contamination, Blk. Contamination, Brn. Bulk Density, gm/cc X on 40 Mesh X thru 140 Mesh X on Pan L Color b Color Inherent Viscosity (Top) Inherent Viscosity (Bot) RVCM, ppm .05 3 44 .574 0.0 8.00 1.5 99.41 1.36 0.802 0.938 1.067 .09 6 99 .571 0.0 11.0 2.4 99.28 1.52 0.925 0.920 0.440 .07 56 500 .547 0.2 7.7 1.8 98.38 1.19 0.869 0.883 0.096 .06 4 47 .556 0.2 12.1 2.4 99.12 1.27 0.900 0.856 0.196 J. Richard Williams Quality Control Supervisor VAB.0001198346 -Vita Polymers Highway 25 RAI L.UAK OFFGRADE Aberdeeni MS 39730 / Load Date: 7- 9f Product: Car No.: 9//so Time Logged In: Logged In Bv: Ship Date: S\aS> Moisture Contamination Bulk Density Color "L" C o,lor au M Silo( s ) : C t! 6/L- Customer 1^ ~,<xr 3 /*/</ ,7if 1 CA CB B *7 _i 1 ^ / ff L^7 1 . 7 ^ / Soo .sm , t> ^ > HI SSI, w.38 99-14 Color f i ft Static Flow Viscosity RVCM I I 1.37 o 'in \ 0 ' tjr]1 0 ' %] 1 c? /?,3 1 Tr<e /. 93$ T. 125/ fz 0 1 r ft?/ - *13 I <rr I /, z7 J e. -H-O | >.>?& | 6. /9<i 1 Screen Analysis Mesh We i gh t '/*u/ 40 O-QC O'O 60 0l 80 list 23n LOO tC-ttr 3X. 3 120 /3/-T 140 iL L227 2 200 Pan 3.3? XK. /, 5 Weigh t % o coo -S7 D/c? _LJ_ lPi_ aa.c. as.o /I,S3 33.-L 6, <33 I3J Lj,Z$ JJI SX 24_ Wei gh t CB % Weigh t y /o <9-1 nj6 }3Q &Qr) 211 3,(p S It-3 2A3 LX /m /i. z z. 9 [6-H Qn 2H Technician: oo f-j rs VAB.0001198347 Vista Polymers To: Mark Manion Highway 25 P. O. Box 91 Aberdeen, MS 39730 Date Fax Sent: 9/24/91 4 OFFGRADE RAILCARS Railcar No.: ACFX 52783 Load Date: 9/04/91 Customer: Product: POND Ship Date: State: Test A CA CB B Moisture Contamination, Blk. Contamination, Brn. Bulk Density, gm/cc % on 40 Mesh % thru 140 Mesh % on Pan L Color b Color Inherent Viscosity RVCM .51 1000+ 1000 + .481 8.1 13.6 6.1 76.98 6.21 0.898 0.365 .42 1000 + 1000 + .486 9.7 12.1 5.5 76.66 6.30 0.904 0.434 .45 1000 + 1000+ .471 1.3 17.9 7.5 74.46 5.88 0.896 0.272 .46 1000+ 1000+ .459 0.3 23.7 10.0 75.35 6.38 0.875 0.266 J. Richard Williams Quality Control Supervisor VAB.0001198348 t Load Date: f Time Logged In: Product: \&M Car No* Logged In By: Screen Analysis Mesh 40 Weight % 4-0 l 11 60 i>.7 I3S" 80 &L3_ 100 9. /z- 1L*_ 120 <*8 2. 140 jj JU4_ 200 Pan 3.OS' 7'S' C.t Weight CA % Weight CB % imc 7-3o PU JJT 17 UlL- <233. LL7 n,t Ml 3 3 ^ 3.7</ 2? LC S. L3 3- If /ICQ /0?3 g.gr s.?r sin s.7l 13 23.2 2I.S L1 1 Weight % . /-? ,3 t.ni 2.3 i. ?s /t. lo.z? zo.G /0X! /S'. / L.n >J. 7 f.H Technician: MWMMIW VAB.0001198349 i ip ip--jp ^mui ! i i -v, Vista Polymers Highway 25 / Aberdeen, MS 39730 Load Date : %' // Product: P<s$*X i///x Car No.: V'9d/ Time Logged In: . /3 11/31 Ship Date Silo(s): Logged In By: 6>f?/& bgZ. Customer Moisture Contamination Bulk Density Color "L" Color "a" Color "b" Static Flow Viscosity RVCM Screen Analysis Mesh Weight % 40 0. (*> <X0 Weight % 0.6& 0*0 /. 0^6? . 2$2~ *2. /o-o ICV.Q7 ajo .04~ . 6o(p o.ctf' LSS ,723 fats ,7?Ar^ .9/A T. 2Sf O/O 60 80 100 &2g0.6 G*. f3.S r 7.<f f.9-3^ */M/ 00 17X 120 140 T 2(.2 200 Pan gs* (.96 36 7.27 </.2$ oft p.o Weight CB % 0.00 0.0 <1*1 0.6> fe>.30 /0(7 fQSa 2o> s*ro 9.70 2.7 Weight % 0.tX> o. O 0. 0.4- lp.2o 3o.f- IdLt* 6.-33 l2.9 Technician: w - in ipr. Ip VAB.0001198350 r To: Mark Manion Date Fax Sent: 8/26/91 OFFGRADE RAILCARS Railcar No.: PLWX 44283 Load Date: i 8/17/ Customer / Test Product: Debox Ship Date: ) State: A CA CB B Moisture Contamination, Blk. Contamination, Brn. Bulk Density, gm/cc % on 40 Mesh % thru 140 Mesh % on Pan L Color b Color i Inherent Viscosity (Top) Inherent Viscosity (Bot) RVCM .48 52 65 .454 0.0 34.5 8.1 99.10 1.70 0.777 0.898 0.051 . 14 65 75 .457 0.0 12.7 3.0 98.85 1.82 0,778 0.776 0.033 .45 70 59 .457 0.0 34.6 6.2 98.79 1.99 0.865 0.146 .47 65 80 .482 0.4 23.6 4.9 98.78 1.91 0.896 0,111 Waiting on yard to obtain samples. J. Richard Williams Quality Control Supervisor VAB.0001198351 Vista Polymers Highway 25 Aberdeen, MS 39730 A Load Date : / Product: Car No.: Time Logged In: 03J* Logged In By: Ship Date: Silo(s): 4 // it2- Customer: Screen Analysis Mesh 40 Weight 0.0 % 0.0 60 M - Weight % f7 C.O Weight % (9^0 Weight % JA ij .3 LA . 90 L 80 -5. </Q iO 100 >3 /3 7 120 ?// MJ. 140 /o&i 31.7 200 Pan I7.Q /J-2sf /ZS\ 37-0 ! 3.0 Cff3 /33 //3i> 33.7 1<b3'l 3>. I 3&.H L 'cA~ 7.23. )>3L c^t 3 ? 33 . a?? lALL y.9 Technician: VAB.0001198352 Vista Polymers To: Mark Manion Highway 25 P. 0. Box 91 Aberdeen, MS 39730 Date Fax Sent: 6/28/91 OFFGRADE RAILCARS Railcar No.: PLCX 46853 Product: Debox Test A CA CB B Moisture Contamination, Blk. Contamination, Brn. Bulk Density, gm/cc % on 40 Mesh % thru 140 Mesh % on Pan L Color b Color Inherent Viscosity (Top) Inherent Viscosity (Bot) RVCM . 23 2 10 .584 0.0 8.6 1.9 99.94 1.39 0.682 0.933 0.203 .19 2000 2000 .560 0.0 23.3 4.8 98.57 1.60 0.824 0.854 0.039 .26 50 500 .560 0.0 10.3 2.1 99.83 1.63 0.633 0.938 0.224 .03 20 100 .578 0.0 11.2 2.4 97.91 2.00 0.678 0.604 0.072 J. Richard Williams Quality Control Supervisor VAB.0001198353 Vista Polymers Highway 25 Aberdeen* MS 39730 RAILCAR ANALYSIS A Load Date : 'ZS-lt Product ;|pa*l Car No.: Time Logged In : { Logged In By: Ship Date: Silo(s): Customer: Vs ,*f f\ A 1 CA CB BI Moisture Contamination . 73 ' /v . /. <eoo * 2oo7}i~ (5_^ , FF<?K<zu11 .03 ^ y /^- 1 Bulk Density -3~7g Color "L" Color "a" ___.99'S7 -07 7 1 A32-_ 1 47.9/ f f('/M /m jF W 11 Color "b" | j'j<j | | 0.0 2-or> Static Flow. T 1 1 0 /S.O | 0i/0.4~ | Of 7.4- Viscosity RyCM 7 LZZ.] ?33> | r 3//J <gs4- | r<ll/ 7J? | , 203 1 - 03? 1 . 2J+- T Z>~)$//,, &o4-----------------,>7Z Screen Analysis i1 Mesh 40 60 80 100 120 140 200 Pan Weight % S>.Q QV /*>f A3-7 7 30- o<2.? 7'S iu. 3 A2 Weight o./z /p./S" fhZS /o.JL? 9.33 J.yA a c/d 4-S Weight O oo CB x O *0o 0.13 3 f.si IL12 /v. y/ /3-U =n o? 7. 7 7?^ /< 6 ^0? Ls2_ !31 3J_ Weight x >O0 //</ JJ/3 1.0 3^3 / *i I Technician: i 11| 4m DPtjlHfipnnp-Drra------ '' p'-JtVflkfl#. in -i- VAB.0001198354 Vista Polymers To: Mark Manion Highway 25 P. O. Box 91 Aberdeen, MS 39730 Date Fax Sent: 8/14/91 OFFGRADE RAILCARS Railcar No.: VIPX 45732 Load Date 8/10/ Customer: Product: Pond Ship Date: Test A CA CB B Moisture Contamination, Blk. Contamination, Brn. Bulk Density, gm/cc X on 40 Mesh X thru 140 Mesh X on Pan L Color b Color Inherent Viscosity RVCM .30 1000+ 1000+ .408 0.5 11.0 3.8 74.11 6.12 0.862 0.001 .30 1000+ 1000 + .409 0.4 10.7 3.7 73.81 6.12 0.859 0.024 .32 1000+ 1000+ .413 06 10.6 3.7 73.37 6.00 0.861 0.084 .32 1000+ 1000+ .480 11.2 8.5 3.2 74.01 6.10 0.853 0.040 J. Richard Williams Quality Control Supervisor VAB.0001198355 Vista Polymers Highway 25 Aberdeen, MS 39730 PVC RAILCAR ANALYSIS 2+9/Load Date: Product: Car No Time Logged In: Logged In By: Ship Date: Silo(s) : Custome A Moisture Contamination Bulk Density Color "L" Color "a" Color "b" Static Flow Viscosity ,3o /oco */ooo~* /0QC~f ^ /OOP 7*U) o.n to. 12, / //otO 73.#/ OJL LOZ 1 7/olJ /O0 /ooo-r\ /* .*HZ V/0 `73. 3 7 (o. co RVCM Screen Analysis . <>/ <P t4~- e>4> Mesh Weight % 40 0,2*1 0, 60 oo 4. Q. 80 I3.3S- 100 /A.3.1/ 2+ 7 120 /t.'lZAO. J 140 te.So A3o 200 3.S4 712. Pan LA? Weight AJI CA X OA a.fi *z 13. 21 ( 2C! 3 20.7 <*32 !2.<t 23. Weight oof % __Qje_ /if 2.8 !3. it 27. 4 12-89 /C.22, 3.43 LjL O .L3. 3. 7 Weight % 11.2. 2.SC <20. 12.18 2Z.9 /7.2. 4.73 207 Technician: VAB.0001198356 Vista Polyaers To: Mark Hanlon Highway 25 P. O. Box 91 Aberdeen, MS 39730 Date Fax Sent: 5/29/91 OFFGRADE RAILCARS Railcar No.: ACFX 52783 Load Date: 5/24/91 Customer: Product: POND Ship Date: State: Test A CA CB B Moisture Contamination, Blk. Contamination, Brn. Bulk Density, gm/cc % on 40 Mesh % thru 140 Mesh % on Pan L Color b Color Inherent Viscosity RVCM .88 1000. 1000+ .442 2.3 15.1 5.4 82.67 7.15 0.865 0.021 00 o .32 1000+ 1000. .445 11.6 3.9 80.31 6.79 0.836 0.019 .83 1000+ 1000+ .453 0.4 18.1 6.9 84.47 7.08 0.814 0.025 92 1000+ 1000+ .456 0.3 10.6 3.5 74.71 5.33 0.816 0.115 J. Richard Williams Quality Control Supervisor VAB.0001198357 *m Vista Polymers Highway 25 Aberdeen, MS 39730 a Load Time Logged In: Product I DG Logged In By: Ship Date: Silo(s): Customer: Moisture Contamination Bulk Density Color If V If Color ft it *A ... JPS> CA 3P~ I CB \ -S3 | 1B -f A J 1/pocT* /tool* 1 /OO^f ' /OdX> f- J /0&Ol~ * /&6G / \ Spoor f /aaaf 1 . ^ .33 vCsf^^ 7*7/ Color ti Static Flow Viscosity /^>o v' 7 A? I sVo /1^ J? RVCM Screen Analysis Mesh Weight X 40 A/3 *?. J 60 J". 80 100 120 fO'*f P/.J 140 200 ? 7 Pan <2 Weight CA X Weight CB X / Weight X :? PS- 7 // 7 ;a6>o JP-8 ? 7 J.? ^). A 7 /3 ll.g /&'> b 2/3 / f- ^ S.&o- 3-V7 /S-8 //'7 6? &.~W -L. M7 iP.L3 ^Li_ J 7.^ 7-31 I *73 3S Technician: X VAB.0001198358 Vista Polymers To: Mark Manion Highway 25 P. O. Box 91 Aberdeen, MS 39730 Date Fax Sent: 7/10/91 OFFGRADE RAILCARS Railcar No.: ACFX 41149 Load Date: 7/05/91 Customer Product: Debox Ship Date WSL State Test A CA CB B Moisture Contamination, Blk. Contamination, Brn. Bulk Density, gm/cc X on 40 Mesh X thru 140 Mesh X on Pan L Color b Color Inherent Viscosity (Top) Inherent Viscosity (Bot) RVCM .03 500 soo .570 0.1 13.8 2.9 98.57 0.98 0.867 0.870 0.052 .03 500 500 .564 0.1 10.6 2.2 98.30 1.19 0.759 0.752 0.177 .12 29 33 .621 0.0 16.5 2.6 99.16 1.35 0.795 0.805 0.185 .04 199 400 .594 0.2 8.9 1.7 99.18 1.19 0.904 0.893 0.021 J. Richard Williams Quality Control Supervisor VAB.0001198359 Vista Polymers Highway 25 Aberdeeni MS 39730 PVC RAX LCAR ANALYSIS ORRGRALE Load Date : 7-S'- Product: Car Time Logged In: // *3 Q Logged In By: A ii A.. * * :_zeiLl-ZlI ,X-___ Ship Date: Silo(s) : Customer: Moisture Contamination Bulk Density Color ft Color "a" Color "b" Static Flow Viscosity RVCM Screen Analysis 'Up Mesh / 40 Weight % a/ .03 .570 78.57 c.98 / 8.9 0.47 / &.0 ,#/ 60 80 A. M2 .75? 100 IP'/ <* / o.99 / 9.0 .7&r 120 79.70 140 /9? /-too 99.H A 38 .m 200 Pan f. {0.9 P.9 Weight a t>3 CA % e>. I 0.& {<?&- /9.ro /38/ P76p 5 f5 (7.9 tfr9t> 5.4- l/o 2.7- Weight CB % dL OO Cl 6 >. fO 0.8 /Cs>J /a at /&PJ7 {52 f. 30 9.<P Weight % O AaCe 0 (6&h 9(7 /`tfC' 982 7925 7/3 L7 Technician: fpzr+f&t- VAB.0001198360 ca VAB.0001198361 Vista Polymers To: Fayetta Tasby Highway 25 P. 0. Box 91 Aberdeen MS 39730 Date Fax Sent: 4/15/91 OFFGRADE RAILCARS Railcar No.: UTCX 46427 Load Date: 4/11/91 Customer: ___ _____________ Product: Debox Ship Date: _______________ State: ____ Test A CA CB B Moisture Contamination, Blk. Contamination, Brn. Bulk Density, gm/cc X on 40 Mesh X thru 140 Mesh X on Pan L Color b Color Inherent Viscosity (Top) Inherent Viscosity (Bot) RVCM .14 60 150 .535 0.0 8.1 2.5 99.28 1.97 0.785 0.774 0.086 .12 40 200 .536 0.0 33.8 11.5 99.26 1.44 0.783 0.774 0.110 .06 15 57 .534 0.0 5.4 1.5 99.26 1.44 0.779 0.979 0.193 .12 100 1000 .535 0.0 9.9 1.6 99.61 1.61 0.779 0.950 0.192 J. Richard Williams Quality Control Supervisor VAB.0001198362 Vista Polymers Highway 25 Aberdeen, MS 39730 Load Pate: ^ w// *7*7 Produc t: fte Car No. : Time Logged In: /##& Logged In By: Ship Date: Silo( si :***-*//- ,>- 7TM JP* Customer: Moisture Contamination Bulk Density Color "L" Color "a" Color "b" Static Flow Viscosity r.// > t /5~D ifo / ^oo J 11 7 7 z fi 0.3Z 99.2 U c.y3 1 1 A9 7 1 7 ir.n 1 _____ 0 //Lo 1 0 k________ /T'Tlr?I , /2~ /,? ft/no iT3 </ sjr 97. S) 1 /o' A 0.07 I / b ! g> ///.^ 1 0 //<5>,? 1 I RVCM Screen Analysis Mesh Weight % 40 4>o2' t>`0 60 80 100 120 aa.,P 2b / 200 Pan Il4L 2, Weight Q.CfO A? 7-/^ 22>f? //i ? CA % 0.0 13. f /& /7.Y iU US' Weight 0"DC> % 3-3 atM3 12.0t> 13-70 77? tit qU.O 21M IS.7 3^9 L. Weight X 0-0 d1 12,72 ft-72 ( ?1 7 3LT 213 s.m Jo,$~ yyy 13 Jl Technician: VAB.0001198363 Vista Polymers To: Mark Manion Highway 25 P. 0. Box 91 Aberdeen, MS 39730 Date Fax Sent: 5/20/91 OFFGRADE RAILCARS Railcar No.: ACFX 41179 Load Date: 5/16/91 Customer: Product: Debox Shin Date: State: Test A CA CB B oto Moisture Contamination, Blk. Contamination, Brn. Bulk Density, gm/cc X on 40 Mesh X thru 140 Mesh X on Pan L Color b Color Inherent Viscosity (Top) Inherent Viscosity (Bot) RVCM 5 12 .543 0.0 12.0 2.3 99.41 1.32 0.752 0.751 0.242 .09 5 10 .558 0.0 2.8 1.4 99.38 1.35 0.730 0.758 0.300 .13 7 76 .566 0.0 6.0 1.6 99.40 2.11 0.960 0.970 0.065 .17 12 250 .576 0.3 9.5 2.0 99.54 1.73 0.913 0.904 0.760 J. Richard Williams Quality Control Supervisor VAB.0001198364 Vista Polymers Highway 25 Aberdeen* MS 39730 A Load Date: o Product: J Car No Time Logged In: CL?o O Logged In By: Ship Date: Silo(s): Customer: /v\o Moisture Contamination Bulk Density Color "L" Color "a" Color "b" Static Flow Viscosity BVCM Screen Analys A 1 ,01 I L /3 i.st. ~ o /?. L~ , /J7 . ^2. , ,732. CA . o T ^ | oS~ i ,sr o ' 7.3 |,7sS . 30Q | ,730 CB B .13 t 1 / 7 /7 / -2_ /^(S"<> .stf. rifr vf o Q*T 57Ti 0 / 7 t/ <S7L cm. $9 [ 31 1,7? \ ns* /. 7D7 . Q(s>5, 1 ,?tt> . (fO /^J7 Mesh Weight % 40 Q.6 0 0.0 60 .50 -M 80 too 120 140 200 Pan 1.3? 12-<f? /V.40 ?-y3 N.7 3S. o -I&? Li54_ 3.3 Weight 0.0'O Q3X // IS7I % O.'o M- v4t),2. 2hZ_ 1 6,6 7.3V i/6 . 7<? * J-Y Weight CB % 0 Jb Weight % ,/j j.03 nor }</?& 3W 30.0 l.t/0 m.oo /2.CV 3>.g 3%.D XS.3 (91 [6. $ V 3/.? 3,2Z MAL jo 0- 3.7/ ns ~?.S 3it> Technician: Cci FS VAB.0001198365 Vista Polymers To: Mark Manion Highway 25 P. 0. Box 91 Aberdeen. MS 39730 Date Fax Sent: 5/01/91 OFFGRADE RAILCARS i Railcar No.: PLWX 44723 Load Date: 4/19/91 Product: 5415 Ship Date: Test Moisture Contamination. Blk. Contamination. Brn. Bulk Density, gm/cc X on 40 Mesh X thru 140 Mesh X on Pan L Color b Color Inherent Viscosity RVCM o o A CA CB B .14 3 1000 .497 11 2 1000 .506 .13 5 100 493 .14 2 95 .492 6.0 1.8 100.42 1.55 1.012 0.001 Composite Result J. Richard Williams Quality Control Supervisor VAB.0001198366 Vista Polymers Highway 25 Load Date: Time Aberdeen, MS 39730 Screen Analysis Mesh 40 Weight 0*0 O 60 U U. 80 9/So 100 JMl 37.2 120 22L )$,U . 140 Ml LAL 200 X01 Pan JO ,8 =Drytime Ml Static Flow: Avg. Microns: Color L: /DP. aO this MCTS: Technician: VAB.0001198367 Vista Polymers Highway 25 AbtrdMDt MS 39730 RAILCAR ANALYSIS A Load Date: Time Screen Analysis Mesh 40 Weight % 60 L 80 AM 100 UUlL 120 1M. if.o 140 lo U 200 AC. 7 Pan 6.4f Dry time: Static Flow: Avg. Microns: I7&.0 Color L: /( a ob WETS: M Technician: VAB.0001198368 i i-j*+ 11 nn^ i l-T^.... B___C.,3E. ,1_ * Vista Polymers To: Fayetta Tasby Highway 25 P. O. Box 91 Aberdeen, MS 39730 Date Fax Sent: 11/16/90 OFFGRADE RAILCARS Railcar No.: UTCX 46548 Load Date: 11/11/90 Customer: Test Product: Pond Ship Date: State.: GA A CA CB B Moisture Contamination, Blk. Contamination, Brn. Bulk Density, gm/cc % on 40 Mesh % thru 140 Mesh X on Pan L Color b Color Inherent Viscosity RVCM .24 1000+ 1000. .425 0.1 21.0 7.2 80.63 6.38 0.866 .247 .21 1000+ 1000+ .442 0.1 24.5 8.7 81.25 6.31 0.802 41.741 .21 1000+ 1000+ 445 0.2 19.8 6.3 77.57 7.57 0.805 22.206 .23 1000 + 1000+ .459 0.1 13.4 0.6 78.55 7.38 0.855 21.83 J. Richard Williams Quality Control Supervisor VAB.0001198369 Vista Polymers Highway 25 Aberdeen! MS 39730 Load Date : It'll'?6 Product Car : 4-CS~4f Time Logged In : /i&Q Logged In By: Ship Date: Silo(s): Customer: Moisture Contamination /do & a 600 Bulk Density Color "L It Color "a ft 7/? Color "b" Static Flow Viscosity 1 RVCM \ I --* - Screen Analysis A. 3? 0 / IT66 * f w /0_ M / 6-3f 9.'s*7 j //<S2T ? / n.7 \ * 4/-1+1 32. Z*6 Mesh 0 weignt % 40 j 60 80 100 120 140 -/ ^ A Jf fT. S3 7,/s J /t-f 2-0* ? Zg.f /?,Z 9.38 T 3/ 3/ 200 Pan 7J.S 7* 2 Weight CA % 0.03 0J {71 t?3 ! 2.3cl 7^0 <fc39 /7.7 /Z& /STS SS 1 Weight CB % C.0<( Cl Weight % J>-( 0.3Z. 70 O.ls M/ 0'.a /0-SZ> /4-60 7/42t.O 36. 0 /7~3 (q.33 {fb Po/7 CtL UZ5 3/7 A3-5 6-S> />. 3! Technician: VAB.0001198370 Vista Polymers To: Fayetta Tasby Highway 25 P. O. Box 91 Aberdeen, MS 39730 Date Fax Sent: 2/01/91 OFFGRADE RAILCARS Railcar No.: VIPX 45766 Load Date: 12/28/90 Customer: Product: 5385 Ship ate: 1 U________ State: (ml Test A CA CB B Moisture Contamination, Blk. Contamination, Brn. Bulk Density, gm/cc X on 40 Mesh X thru 140 Mesh X on Pan L Color b Color Inherent Viscosity RVCM .20 4 16 .559 0.0 -- 11.2 .35 * 4 12 .530 .21 6 12 .568 100.32 1.24 0.932 .267 -- Composite .25 4 14 .553 * Original moisture check was .58. The .35 was after cleaning out bottom tubes. J. Richard Williams Quality Control Supervisor VAB.0001198371 Vista Polymers Highway 25 Aberdeen, MS 39730 Load Date: Product: Car No Time Logged In: Logged In By: Ship Date: Silo(s ) : Customer: Moisture C o n t am i nation A 1st 2nd 13 HJO Bulk Density Fluff Hard Particle 1st i- i i CB 1st 2nd B 1st 2nd }\rekv rrrtf Viscosity RVCM 40 Mesh/Glassies Screen Analysis Mesh 40 60 80 100 120 140 200 Pan Weight % Drytime Static Flow: _____/______ Avg. Microns: Color L: Technician: VAB.0001198372 , Vista Polymers Highway 25 Aberdeen, MS 39730 A Load Date: Product: 5385 Car No Time Logged In: Logged In By: Ship Date: Silo(s): Customer Screen Analysis Mesh 40 Weight 0O> - % 60 .30 80 --/--*------ 1/---- 100 MJf 120 \S,2L 30.% 140 71C. 200 Pan ty.xr f.os' 3,f Drytime: V.9 Static Flow: E*>/?P Avg. Micirons: /</?, Color L : /fro,a b A A Y* Technician Op 4- VAB.0001198373 jHrfutmntiiifiMi 4 iiqiifftfHnrnitffvwfivvtvvivtvftvpvfvtntfiMiiiffmtfttinivfpmmmipftwivlH-41 !MNiiflttnnfflFiii|fl^|iHiirtfliipimiiiiM''MitiitH|iPiMiwi>fmiHHi*imvwMMr -:imin!tttttiippiiiiFii'iiii'pip*ppmiiH'!ii|H"Mrni'M'PiPfii|iiiitfftflniiiP'piiiHiHiiiimim"i'Hpiiiji<hriii'|'r!'i::L-ji4Mi'H''i>..t'iH"' h- -im-j M*^*i it !..... -nr..-,. |[^inn| !("' ''HI'1 :a-.'PS -l*i|i| ....... [AJ&ObGr&A'/fJ MGLb! *\ m m \ l f I. I .1 pr ,1 I I I I I r r 1 i l i | I i i i i i r i i i i i i i i i i i i i l 4 VAB.0001198374 j Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730*0091 Phone (601) 369-81 1 1 OF ANALYSIS * Date: ///^/^/ Customer: Woodgrain Mouldin P. 0. Box 7380 Waco, TX 76710 Attention: Richard Burge Date of Shipment Inc Property Moisture, 7. Bulk Density, gm/cc Particle Size, V. on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC--26 ABR--10 VIS1A Product: 5265 Order No. : Q004&*\ ~DOO Trailer No.: 5 b: /9^2r Analysis /)6 f 0 >D (p - I ___^C> Not more than 8.5 PPM This material was produced to yield an inherent vis cosity in the range of 0.62 to 0.70. tlJ aborat^yry Super^isjar/Lead VAB.0001198375 4 O O A. O) o <D a CO c/> c 9 cx E CL /N * VAB.0001198376 *' n MUM Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 I F I CA Aberdeen, Mississippi 39730-0091 Phone (501) 369-8111 A * YS I S Date: f2~ 12'4 I Customer: Woodgrain Mouldings, Inc P. 0. Box 7300 Waco, TX 76710 Attention: Richard Burge Date of Shipment: Property Moisture, 7. Bulk Density, gm/cc Particle Size, 7. on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC--26 ABR-10 VKIA Product: 5265 Order No. : OOO t/OS'l-DO 6 Trailer No.: T'SIC, Lor Mo : Analysis o'? 431 r>. o M. Not more than 0.5 PPM This material was produced to yield an inherent vis cosity in the range of 0.62 to 0.70. Sup^rv^ sor/Lead VAB.0001198377 i ^ g o o> # O) o * > 01198378 * , -* Vista Polymers A Division of Vista Chemicol Company Highway 25 Post Office Box 91 CERTIFICATE OF Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 1 1 XS * Dates //'2 6""^/ Customer: Woodgrain Mouldings, Inc P. 0. Box 7300 Waco, TX 76710 Attention: Richard Burge Date of Shipment: //- 22-^/ ;Lor AJo. \ OLftT-fT Product: 5265 Order No.: Q ^ Trailer No.: Qj &OO Property Moisture, 7. Bulk Density, gm/cc Particle Size, V. on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis 08 Q- O k>. I 2.0 Not more than 8.5 PPM This material was produced to yield an i nherent viscosity in the range of 0.62 to 0.70. Laborator Super at /Lead VAB.0001198379 rt i I 1* i II f h1 k: 1p O CL oCO 8 r i i* Ei i ' 1 4 Mi A O) o \o OL CO w c > CL o s a cc *)* w\ iiiftu.i in. wiii --H III MMUM - 3 VAB.0001198380 t- * * Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OK Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 l VS X S Date: //- Customer: Woodgrain Mouldings* Inc P. 0. Box 7380 Waco, TX 76710 Attention: Richard Burge Date of Shipment: VISIA Product: 3265 Order No.: &o3J-ooo 1er No. 7^ ?J>3 Property Moisture* 7. Bulk Density, gm/cc Particle Size, X on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 Analysis 4>C> glQ* & ABGC-26 ABR-10 Not more than 8.5 PPM This material was produced to yield an inherent vis cosity in the range of 0.62 to 0.70. Laboratory Supervisor/Lead VAB.0001198381 Date. /A ra -9 / Customer Technician___ ,/ PVC BULK TRAILER ANALYSIS Product Silo Trailer Number Time Order No. h Particle Size Distribution: Screen Analysis Mesh Size 40 Min On fflotap shaker. 49 gins. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. Gross Wt. Tare Net Wt. % on Mesh Screen Analysis <*.> -"S /fO (e-IZ. /WO /-a~ 0 7 Jp. n t A tg M______J=^ 3 ? /3-P 39 / / olo* (a -------------------Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb a Mesh Size Gross Wt. 40 80 _________ _____ Glassy Pan Part. 100 120 140 200 Tare _________ ______ Net Wt. _________ ______ H on Mesh _________ _____ Remarks Star 207A Revised 1/12/87 VAB.0001198382 Vista Polymers A Division of Vista Chemical Compony Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-6111 LETTER OB' CERTIFICATION Date: . 24, mi Customer: WOODORAIN MOULDINGS, INC P. 0. Pox 7380 Waco, TX 76710 Attention: Richard Burge Date of Shipment: ^4/ M*?/ VISIA Product: 5265 Trailer No.: % iftq Order No.: OOQn^^CO! Moisture , % Bulk Density, gm/cc Particle Sise, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity ABR-1A 8.410 8.300 .on 8.955 8.600 LLl __________ Not more than 8.5 PPM This material was produced to yield an inherent viscosity in the range of 0.62 to to 0.68. I l t t fi I 1 fc+ i I r * * m r e. tP* *1 L l f \ t%4 r ir f V * t1t p I it k- or/Lead WMPii* f iWhi VAB.0001198383 PVCNLX 2 FRONT ll. I MIDDLE [71 i. [ 2. 1 11. 1 11 12 I |i. I (2. j ULK OCNSITY humic Slxe Oixiributiufi: I3oO A COLOR VBC IRVCM 42.7i o.<e>7 L* Tam MM Remiriift g'-Q-S' Zif_ /3/&i> S-S'/ 4 VAB.0001198384 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730*0091 Phone (601) 369-0111 A LETTER OF CERTIFICATION Date: Customer: W00DGRAIN MOULDINGS, INC. P. 0. Pox 7380 Waco, TX 76710 Attention: Richard Burse Date of Shipment: /v VK1A Product: 5265 Trailer No. : 7^ Order No. : &0O 4 Moisture, % Bulk Density, gm/cc Particle Size, X on 40 Mesh 200 Mesh Pan Residual VCM, PPm Inherent Viscosity Test Method ABR-1A 8.410 8.300 8.955 8.600 Not more than 8.5 PPM This material was produced to yield an inherent viscosity in the range of 0.62 to to 0.68. atory Supervisor/Lead VAB.0001198385 PVC BULK TRMLBT ANALYSIS Date. - /1 Cuatemcr I FRONT i iiNiim SBo Z i" MOIST CONT GEL iraB--c--r Tbne Order BULK DENSITY DRY TIME , rn I 0 WiT- COLOR 71.14} B - /* vise RVCM MIDDLE 11 di l * 1B 111 B * B 2m B- | V | 11. I It. I i. i. i. L - I I END A I B- 1 Particle Size Distribution: Screen Anaiyets _______Mki On Rotay enter. 49 gen. Reein pkn 1.0 gen. Cut Mesh Size 40 Grose Wt. Tore Net Wt. 44 on Mesh > +0 e>*> Screen Analysis Mesh Size Wt Tore Net Wt. H on Meeh 40 100 120 140 03& 8.60 6.S 1r+* 4,,4' ?/gr &7r --#i_c/ /<i>,c yM' s t.W 9- /.- lain. On Retag shaker 40 gen. Reeki pkn t.O gets. Card Glassy Ran hart. 00 00 100 120 140 200 Remarks Star 207A Revised t/12/a7 VAB.0001198386 * rt ss i PVC BULK.TRAILBrANALYSIS r" o / /-- __ '7T_ {// f-- A Particle Size DiMribuiion: 8ww Awlyfli On HofQ 40 1.0 qoml Cob Mooli StBO Grow Wt. Tom 40 ________ ------------ 60 _____ ------- 120 140 H on Mooli Q*00__ Sentii Anolyolo ,,, / Min. On Rotap ihofcar 40 mol Room pfeo 1*0 ma. Carto Mooh Stao Tom Not 1 40 00 00 100 120 140 , 200 4 Remarks k Star 207A 1/12/07 4-WW1 . ...T Mf 4 198387 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 A LETTER OF CERTIFICATION Date: Customer: WOODGRAIN MOULDINGS, INC. P. 0. pox 7380 Waco, TX 76710 Attention: Richard Burse Date of Shipment: VIS1A Product: 5265 Trailer No.: ^& Order No. : 000/397-60 / Property Moisture, % * Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity TsstJfefehgd ABR-1A 8.410 8.300 8.955 8.600 Not more than 6.5 PPM This material was produced to yield an inherent viscosity in the range of 0.62 to to 0.68. t Laboratory Supervisor/Lead VAB.0001198388 r iw. PVC BULK TRAILER ANALYSIS _________ Product ~A6>S_________ Tnlar Nnmic U)e*4*iVA t / SUo___________________________________ Tlnw. OS'-/S'- 03= vc* A Particle Size Distribution: Scraan Analysis Mash Slza 40 Gross Wt. _____ Tara Nat Wt. H on Mash Scraan Analysis Min On Rotap shsfcar. 49 gms. Rasin plus 1.0 gms. Cab 00 SO 100 120 140 200 Glassy Pan Part. >.(<> ?.<*> I3(e (Wo ffto Cl /& &'?,! r7*& p^tfc ft# __Min. On Rotap shafcar 40 gms. Rasin phis 1.0 gms. Cart) d.5& /^ Glassy Mash Slza 40 00 00 100 120 140 200 Gross Wt. _________ _________ _________ _____ Nat Wt. H on Mash Remarks i t Star 207A Ravisad 1/12/87 VAB.0001198389 Vista PotyiMo A Division of Vista Chemical Company Highway 25 Post Office Bax 91 Aberdeen, Mississippi 39730*0091 Phone (601) 369*8111 A LETTER OB' CERT IFI CAT I ON Customer: WOODGRAIN MOULDINGS, INC. P. 0. Pox 7380 Waco, TX 76710 Attention: Richard Burge Date of Shipment: 5*<25'? I VISlA Product: 5265 Trailer No.: 7-^25- Order No. : OOO /Z?7-0OO Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity ABR-1A 8.410 8.300 8.955 8.600 Not more than 6.5 PPM This material was produced to yield an inherent viscosity in the range of 0.62 to to 0.68. Laboratory Supervisor/Lead r VAB.0001198390 Vido BolyMdi Attrition of Virto Granted Compony rnyrWW ftv Pod Omco Box 91 Abnrd--y, Mitsmippi 39730 Phono (Ml) 369-8TI1 LETTER OB' CERTIFICATION A Date: 7/3o/9( Customer: W00DGHAIN MOULDINGS. INC. P. 0. Box 7380 Waco, TX 76710 Attention: Richard Burge VKIA Product: 5265 Trailer No.: 7" $o Order No. : QQOO (s>SS -O OO Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity ABR-1A 8.410 8.300 Analysis . /o o. o 9S 8.955 8.600 Not more than 8.5 PPM This material was produced to yield an inherent viscosity in the range of 0.62 to to 0.68. Laboratory Supervisor/Lead VAB.0001198391 Date Customer Technician lAJD pvc bulk Trailer analysis Product l*T2 &> 1 WHET A MOIST B(iHnn CONT. Stiftmi GEL Order BULK DENSITY <pGC&6?5? COLOR vise RVCM FRONT TT I MIDDLE 12. 1 iI END ia 1I 11 ( 1 y^pe 111 1. |1 ml* o j 11 11 11 i 11. i. jI i^ * II *i* i L- j1 % 11 i. 11 -- e I 1 '1 Particle Size Distribution Screen Analysis Mash Sica Gross Wt Tare Net Wt % on Mesh Screen Analysis 40 30 Mesh Slae Gross Wt. Tare Net Wt H on Mesh 40 On fletap shaker. 46 gat. Resin plus 1.0 Cart 60 100 120 140 Qlmy Pan Part. -* * 4 -pH 4?. f Z. O. Z /?^ 3?:i Min. On Rotap shaker 4t gate. Resin plus 1.0 *7*/ Carb 100 120 140 Gteosy 1TM Remarks VAB.0001198392 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A LE TTER OF CERTIFICATION Date: Customer: WOODGRAIN MOULDINGS, INC. P. 0. Box 7380 Waco, TX 76710 Attention: Richard Burge Date of Shipment: P/^Jp/ Product: 5265 Trailer No. : 7^- $/C Order No. : 900 Property Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A 8.410 8.300 Aoaly?is 8.955 8.600 i Not more than 8.5 PPM This material was produced to yield an inherent viscosity in the range of 0.62 to to 0.68. Laboratory Supervisor/Lead VAB.0001198393 * X Customer Technician PVC BULK TRAILER ANALYSIS A Particle Size Distribution: Screen Analysis Mesh Size 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 60 60 100 120 140 200 Glassy Pan Part. Gross Wt. -- ---* -- ^ ---- -- -- Tare Net Wt. H on Mesh +* 0.6 (Cl*H /S73 6* S' fa* S*>-t //*t 673X (fo &BL& /0.X J?.S Screen Analysis Mesh Size Gross Wt. 40 ___ Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carta Pan 60 60 100 120 140 200 Glassy Part. Tsre Net Wt. H on Mosh Remarks_____ Star 207A Revised 1/12/a7 VAB.0001198394 VblaUyiMn A Division of Vista Chomied Company Highway 25 Post Offico Box 91 Abordaon, Mississippi 39730 Phono (601) 369-8111 A' 4 LETTER OB' CERTIFICATION Date: rfu.f. ?/ Customer: W00DGRAIN MOULDINGS, INC. P. 0. Box 7380 Waco, TX 76710 Attention: Richard Burge Date of Shipment: rftto, VISIA Product: 5265 Trailer No. : 7- jU3 Order No. : OOO//&0-00O Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity 8.955 8.600 Not more than 8.5 PPM This material was produced to yield an inherent viscosity in the range of 0.62 to to 0.68. * VAB.0001198395 Cu*toner Technician n Panicle Size Distribution Screen Aneiysis Meet* SUe arose Wt. Tere r Net Wt H on Meen Screen AnSyw* 4C OiOfi 0. 0 MeenSlie Oroee Wi. Tire Net Wl. H on Meen On flotep sinker- 100 120 jj t 2~ Mm. f On t*o enefcm 40 2./, 100 120 Remarks 1M 140 /V. * xjT. i^ 140 epi PVC BULK TRAILER ANALYSIS rw. 7-8"?/_______ Product L~__________ Trailer Namber-- Particle Size Distribution: Screen Analysis Mesh Size 40 Gross Wt. Tare Net Wt. H on Mesh C.oo O.Co Screen Analysis Mesh Size Gross Wt. Tare Net Wt. H on Mash 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 pm. Carto 60 00 100 120 140 200 Glassy Pan Part. 0-/Z B-Z 4.29 P.f ?(, /9- 37 // SS 494 /7.S 3S.2 23./ 9.S /.2e ___ Min. On Rotap shaker 40 gms. Resin plus 1.0 gms. Carto Pan 60 100 120 140 Glassy Part. Remarks Vista Mywn A Division of Vista Chamical Company Highway 25 fait Omes Boat 91 Afcsrdxn. MiaMppi 39730 faoiM (601) 369*8111 LETTER OB' CERTIFICATION . 7-<5/-9/ Date Customer: WOODGRAIN MOULDINGS, INC P. 0. Box 7380 Waco, TX 76710 Attention: Richard Burge Date of Shipment: \o\ Product: 5265 Trailer No. : *7*" Order No. : 0O0O1> *2" Property Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A 8.410 8.300 .// .s4*r 9.S 8.955 8.600 Not more than 8.5 PPM This material was produced to yield an inherent viscosity in the range of 0.62 to to 0.68. Laboratory Supervisor/Lead VAB.0001198398 Vista Potymafs A Division of Vista Charmed Company Highway 25 Post Offica Box 91 Adacdann, Miwiwippi 39730-0091 Phono (401) 369-8111 *^ LETTER OB' CERT IFI OAT I ON Date: 'iPO -*? { Customer: W00DGRAIN MOULDINGS, INC. P. 0. Box 7380 Waco, TX 76710 Attention: Richard Burge Date of Shipment: / Product: 5265 Trailer No. : Order No.: * o o&o Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Testjjs^hqd ABR-1A 8.410 8.300 Analysis 7 0.0 69 8.955 8.600 Not more than 8.5 PPM This material was produced to yield an inherent viscosity in the range of 0.62 to to 0.68. Laboratory Supervisor/Lead VAB.0001198399 PVC BULK TRAILER ANALYSIS WnmhMr '7^'26>3 <4 Particle Size Distribution: Scrson Analysis af Min On ftotap ahaitsr. 49 gam. Rosin plus 1.0 gms. Garb Mosfi Size Wt Taro p Not Wt H on Mosh Seroon Analysis 40 4? JO 100 120 140 7-*7 tf. go /S./> / ^ & 4^ On Rotap shakar 49 gma. Rosin plus 1.0 gma. Carto MoshSba Gross Wt. Tara Not Wt. % on Mosii Remarks. 40 100 120 140 Pan Star 207A Rovisod 1/12/97 Vista Polymers A Division of Vista Chemical Company Highway 25 Pool Office Box 91 Aderdeen, Mississippi 39730-0091 Phono (601) 369-8111 A Date: Customer: WOODGRAIN MOULDINGS, INC. P. 0. Box 7380 Waco, TX 76710 Attention: Richard Burge Date of Shipment: yAA VIS1A Product: 5265 Trailer No. : 8^/ Order No. : 0QO'0 tT/C - G OC PggBSgty Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A 8.410 6.300 8.955 8.600 Not more than 8.5 PPM This material was produced to yield an inherent viscosity in the range of 0.62 to to 0.66. Laboratory Supervisor/Lead VAB.0001198401 if 'jr. * : 'j 'Vj', 1^ ' *: ^ * ** i ^ FVC BULK TRAILER' ANALYSIS' :v\ 4 Particle Size Distribution: Scraan Analysts On Roup ahafcar. 49 1.0 Mash Sin Grow Wt Tam Nat Wl. H on Masft ScfNfi Analyst* O.CO O SL gjl J7.> On Roup shafcar 49 Rasta plus 141 Hull sira Tan Nat Wl H on Mooh Remarks 94 Star 207A Aaytsa* t/i9ir VAB.0001198402 Vista Potyman A Division of Vista Chamical Company Highway 25 Post Omco Box 91 Adsrdssft, Mississippi 39730-0091 Phon* <401) 369-8111 LETTER OB' CERT IFI CAT ION A Customer: WOODGRAIN MOULDINGS, INC. P. 0. Box 7380 Waco, TX 76710 Attention: Richard Burge Date of Shipment: 4 -- ~ t Product: 5265 Trailer No. : J " H 7^ Order No. : OODooSy^oov Property Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A 8.410 8.300 8.955 8.600 Not more than 8.5 PPM This material was produced to yield an inherent viscosity in the range of 0.62 to to 0.68. Laboratory Supervisor/Lead VAB.0001198403 Date PVC BULK TRAILER ANALYSIS Prod r 1 . ""gyr-- .57^7 Trailer Number. Order No. 4 Particle Size Distribution: Scrtan Analysis Mash Slsa 40 Qroas Wt. Tara Nat Wt. H on Mash >.0O Scrasn Analysis Msah Slsa Qroaa Wt. Tara Nat Wt. H on Maah 40 Min On Rotap shafcar. 40 gma. Rasln plus 1.0 oma. Carb 100 120 140 200 Plasty Pan Part. 0.9- J3 3! Min. On Rotap ahakar 40 gma. RaaJn plus 1.0 gma. Carb Pan 100 120 140 200 Qlaaay Part. Remarks 207A 1/12/07 98404 * Vista Potymws A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A CERTIFICATXON Date.^_l'?-CM Customer: WOODGRAIN MOULDINGS, P. 0. Box 7380 Waco, TX 76710 H Attention: Richard Burge Date of Shipment: * INC. Product: 5265 Trailer No.:~T~M^^ 4 Order No. : IS S^. //<f Moisture, % Bulk Density, gm/cc Particle Size, X on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity t Test Method ABR-1A 8.410 8.300 Analysis 8.955 8.600 Not more than 8.5 PPM This material was produced to yield an inherent viscosity in the range of 0.62 to to 0.68. 4 Laboratory Supervisor/Lead VAB.0001198405 i Customer ^ PVC BULK TRAILER ANALYSIS A Particle Size Distribution Screen Analysis Mesh Size 40 Gross Wt Tars Nat Wt o.QC % on Mash CVO Scraan Analysis Mash Size Gross Wt. Tara Nat Wt % on Mash 40 Min On Rotsp shaker. 49 gins. Rssin plus 1.0 gms. Garb 60 100 120 140 200 Glassy Pan Part. ,IZ 9.3</ VIO K!(/ (3.10 Afs: .2. 1A} LU_ 31.3 2W 13.3 L_2_ Min. On Rotsp shaker 49 gms. Rosin plus 1.0 gms. Carb Pan 90 90 100 120 140 200 Glassy Part. Remarks Star 207A Revised 1/12*7 VAB.0001198406 \ Date Piifitnmer Technician ^ G- pvc bulk Trailer analysis Product Silo 9 . Trailer Number 1 Time 130 Order No. e/3e?<?-//3 A Particle Size Distribution: Screen Analyeie Mesh Size 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carto 60 80 too 120 140 200 Glassy Pan Part. Gross Wt. Tare Net Wt. H on Mesh ------------------------------------------------------------------- ------------------------------- -------- * -- -i -*---------------------- - ,! -- --------------------------- ------ -- >. o --_ >./8 o.<f ,_ . _ ____ &9I //.g _ ^ _ ____ _____ /oAl /.g 31,1 /A 3 7 .. --r-r _ _ _________________________ t-so g.y 3.e Screen Analysis -------------------- ,,-- - _-- ____Min. -- ----------------------------- On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Mesh Size Gross Wt. Glassy Pan Part. 40 60 80 100 120 140 200 Tir* Net Wt. H on Mesh ----- Remarks __________________________ Star 207A Revised 1/12/87 ' " *-n ' -k I .. . . . . . . . . . .. *' VAB.0001198407 -- --------------------------------- Villa Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (dOl) 369-8111 LETTER OB' CERTIFICATION Date: 5*-/ sl / Customer: WOODGRAIN MOULDINGS, INC. P. 0. Box 7380 Waco, TX 76710 Attention: Richard Burge Date of Shipment: / Product: 5265 Trailer No. : Order No. : 8/38<f<?-//3 \ Pgg.egx$y Moisture, % Bulk Density, gm/cc Particle Size, X on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity ABR-1A 8.410 8.300 <2? ) 8.955 8.600 Not more than 8.5 PPM This material was produced to yield an inherent viscosity in the range of 0.62 to to 0.68. VAB.0001198408 Vida Polymen A Division of Vista ChemicaJ Company Highway 25 Post Office Box 91 Aderdeeiy Mississippi 39730-0091 Phone (601) 369-6111 A LETTER OB' CERT IFI CAT I ON Date: Customer: WOODGRAIN MOULDINGS, INC P. 0. Box 7380 Waco, TX 76710 Attention: Richard Burge Date of Shipment: VISIA Product: 5265 Trailer No.: Order No.: S73 r? 9-//<3 Pronerty Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity lestJfethod ABR-1A 8.410 8.300 Analysis -54(5 Jj- V 8.955 8.600 Not more than 8.5 PPM This material was produced to yield an inherent viscosity in the range of 0.62 to to 0.68. Laboratory/ S // // V VAB.0001198409 Dale Customer Technician FRONT PVC BULK TRAILER ANALYSIS Product J2(rS~ Trailer Number. Time Order MOIST Bnmmi I CONT Hottnm GEL BULK DENSITY I DRY TIME I COLOR vise L - *fCj 0(^1 a - ,50 -f.70 ii L- A RVCM MIDDLE A= END ji r 1i 1 1a 1 11 | 1 11 >* 11 (T 1 i M 1 11 1 > 1 i * ms Particle Size Distribution: Scrasn AnalysisMin On Rotap shaker. 49 gms. Rasln plus 1.0 gms. Carte Maah Size 40 90 120 140 Glassy Pan Part. Gross Wt. Tara Nat Wt. H on Mash <9.00 . 11 W3 fS.u 11.93 S.W 1.30 O.t) ml iM 1*1 111 JM Scraan Analysis Mash Size Gross Wt. 40 Min. On Rotap shaker 49 gms. Rasin plus 1.0 gms. Carb Pan 00 120 140 Glassy Part. Tara Nat Wt. H on Mash Visto Polymer* A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730*0091 Phone (601) 369*8111 LETTER OE CERTIFICATION 4 * >1 JJilf A Date: 79 y^/\ ?/ Customer: W00DGRAIN MOULDINGS, INC. P. 0. Box 7380 Waco, TX 76710 ' Attention: Richard Burge Date of Shipment: X 9 9/ Product: 5265 Trailer No. : 7JLJL Order No. : Moisture, % Bulk Density, gm/cc Particle Size, X on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test -Method ABR-1A 8.410 8.300 8.955 8.600 Not more than 8.5 PPM This material was produced to yield an inherent viscosity in the range of 0.62 to to 0.68. isor/Lead VAB.0001198411 Dale Cintomer Technician -4- PVC BULK TRAILER ANALYSIS Product Silo-(38^ Trailer Number Time--QjJS~ Order No.--------------- % * Particle Size Distribution Screen Analysis Mesh She Gross Wt Tare Net Wt H on Mean Screen Analysis 40 ? & <> O Mesh She Oross wt Tare Net Wt H on Meeh 40 Remarks On flotap shaker. 40 9ms. Resin plue 1.0 9m. Cart) 100 120 140 200 Qmy Pert. 6?.o L>- v ^ 12 o Z- l lu? L*?Z3o.6> jtj. o 3.3 On Rotap shatter 49 gets. Ream plus 1.0 pm. Cart) 100 120 140 Gtaasy Pert. Star 207A Rowsee 1/12/07 -M -l*J h*. wmmm m -< i|iiwe ||rT * -- 1--- 98412 ttu. Villa Polyman A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 397304)091 Phone |501) 369-8111 A LETTER OB' CERTIFICATION Date: ' 1 *7 i Customer: WOODGRAIN MOULDINGS, INC. P. 0. Box 7380 Waco, TX 76710 Attention: Richard Burge Date of Shipment: ?/ Product: 5265 Trailer No.: Order No. : -//o Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity ABR-1A 8.410 8.300 0.00 8.955 8.600 Not more than 8.5 PPM This material was produced to yield an inherent viscosity in the range of 0.62 to to 0.68. ervisor/Lead VAB.0001198413 `i i- P Customer PVC BULK TRAILER ANALYSIS Af Particle Size Distribution: Screen Analysis On Rotap shaker. 49 pa. Resin phis 1.0 gins. Csrto Mask Size Pan 40 M SO 100 120 140 200 Gross Wt.________ ___________ ________ ________ ________ ________ ________ _ Tare Net Wt. N on Mesh s.m /*i7 w // <n H.m M t*.i 32.9 23.1 ?.? 2A Screen Analysis On Rotap shaker 40 get. Resin phis 1.0 gats. Carto Glaaay Part. Mash Size areas Wt. Tare Net Wt. Hon Mesh 40 100 120 140 200 Remarks Star 207A 1/12/07 m cm t i' Tl Date Customer \JJ Technician. PVC BULK TRAILER ANALYSIS Product S3US~ Silo___ (d & Trailer Number. _ Time VO PP A Particle Size Distribution: Screen Analysis Mssh Sizs Gross Wt. Tars Nst Wt. % on Mssh Screen Analysis 40 <0.0 c?,Q Mssh Sizs Gross wt. Tars Net Wt. % on Mssh 40 Min On Rotap silaker. 49 gms. Rssin plus 1.0 gins. Carb 60 80 100 120 140 200 Glassy Pan Part. ' O (=> *?.7/ .717 /.?- 7? JS-&8 Z67 jL3<7T >. / /V-3 37-9 30. 2_ /?.</ 2 7 Min. On Rotap shaksr 49 gms. Rssin plus 1.0 gms. Carto Glassy Pan Part. 60 80 100 120 140 200 Remarks Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 LETTER OE CERTIEXCATXON Date: /-/-*?( Customer: WOODGRAIN MOULDINGS, INC. P. 0. Box 7380 Waco, TX 76710 Attention: Richard Burge Date of Shipment: / VISIA Product: 5265 Trailer No. : ~7<X80C} Order No.: 8/38^*?-/*? Property Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR- 1A Analysis - >V 8.410 .S3ST 8.300 fO'O___ -J3- / <}-7 8.955 8.600 Not more than 8.5 PPM This material was produced to yield an inherent viscosity in the range of 0.62 to to 0.68. odjlbuL^ Laboratory Supervisor/Lead VAB.0001198416 Vida Polymen A Division of * Visla Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A LETTER OF CERTIFICATION Date : 3 " ^ /#" Customer: W00DGRAIN MOULDINGS, INC. P. 0. Box 7380 Waco, TX 76710 Attention: Richard Burge Date of Shipment: J3 -^*0" f VISTA Product: 5265 Trailer No. : Order No. : e Outfit f Property Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity * Test Method ABR-1A Analysis __, /*? 8.410 __ / 8.300 fi- 0 /<?- $ /. 8.955 Not more than 8.5 PPM 8.600 This material was produced to yield an inherent viscosity in the range of 0.62 to to 0.68. VAB.0001198417 ft I i* *tf < - r i 8 I1 1 l 8 51 i U. -b-n. -T ' < *3 co o 5 o 03 o t l ( AB Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A LETTER OF CERTIFICATION Date: S>-/ Customer: W00DGRAIN MOULDINGS, INC. P. 0. Box 7380 Waco, TX 76710 Attention: Richard Burge Date of Shipment: 3-- Product: 5265 . sn / Trailer No. : Order No.: P- Property Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A 8.410 8.300 Analysis * (p. (PC- 8.955 8.600 / Cr Not more than 8.5 PPM This material was produced to yield an inherent viscosity in the range of 0.62 to to 0.68. VAB.0001198419 I - I LfJP r- U 1 . ri 1 PVC BULK TRAILER ANALYSIS jl II F Hato -3 - // ' ^7 f______ Product _________ Trailer Number *? *~f_ Particle Size Distribution: Screen AnalysisMin On Rotap shaker. 40 gins. Baaln phis 1.0 0ms. Carta Mesh Size 40 00 80 100 120 140 200 Gross Wt. Tare Net Wt. a-?o____4-.6Sr` 9.7? % on Mash H Screen Analysis Min. On Rotep shaker 40 gma. Resin plua 1.0 gms. Carta Mesh Size 40 60 Gross Wt. Tare Net Wt. H on Mesh 100 120 140 200 e -a Qlaaay Pan Part. ZJL Olesey Pan : -i !-* FI VAB.0001198420 Vista Polyman A Division of Vista ChomicaJ Company Highway 25 Post Office Box 91 Adordoen, Mississippi 39730-0091 Phono (601) 369-8111 A LETTER OF CERTIFXCATION Date*- 2*3-^) Customer: WOODGRAIN MOULDINGS, INC P. 0. Box 7380 Waco, TX 76710 Attention: Richard Burge Date of Shipment: VK1A Product: 5265 Trailer No.: l Order No. : &I3X?S- 10*7 Moisture. % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A 8.410 8.300 ao OoD 8.955 8.600 Not more bhan 8.5 PPM This material was produced to yield an inherent viscosity in the range of 0.62 to to 0.68. Laboratory Supervisor/Lead VAB.0001198421 9 Customer PVC BULK TRAILER ANALYSIS A Particle Size Distribution: Screen Analysis Mash Size Gross Wt. Tara Nat Wt. H on Mash Scraan Analysis 40 9.0* 0 Mash Size Gross Wt. Tara Nat Wt. H on Mash 40 _____ ______ _____ ______ Min On Rotap shaker. 49 gms. Raain plus 1.0 gma. Carte 120 140 200 Glassy Pan Part. Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carte Pan 100 120 140 200 Glassy Part. Remarks Star 207A Revised 1/12/97 WJ' -- i mi *rt**MW VAB.0001198422 4 m tta Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone {601) 369-8111 t LETTER OF CERTIFXOATION Date: 9 9/ Customer: W00DGRAIN MOULDINGS, INC. P. 0. Box 7380 Waco, TX 76710 Attention: Richard Burge Date of Shipment:/ 7/ Product: 5265 Trailer No.: 7^233*/ Order No . . Z/3&79-/0& Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test Method ABR-1A 8.410 8.300 Analysis 8.955 8.600 Not more than 8.5 PPM This material was produced to yield an inherent viscosity in the range of 0.62 to to 0.68. Lab isor/Lead VAB.0001198423 Customer Techn PVC BULK TRAILER ANALYSIS Particle Size Distribution: Screen Analysts Mesh Size Gross Wt. rTare Net Wt H on Mesh Screen Analysis 40 Mesh Size Gross Wt. Tare Net Wt. H on Mesh 40 Remarks. Min On Rotap shaker gms. Resin oms 60 100 120 140 200 Glassy Pan Part. / 2 Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 J3_ Glassy Pan Part. Star 207A r- - * j-- 1/12/67 am VAB.0001198424 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 LETTER OF CERTIFICATION Date: <f 9/ Customer: WOODGRAIN MOULDINGS, INC. P. 0. Box 7380 Waco, TX 76710 Attention: Richard Burge Date of Shipment: 9 9/ Product: 5265 Trailer No. : Order No. Moisture, % Bulk Density, gm/cc Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, ppm Inherent Viscosity Test_Method Analysis ABR -1A ____ 8.410 __ 8.300 ____ID 8.055 8.600 --3JL- ___ L3- Not more than 8.5 PPM This material was produced to yield an inherent viscosity in the range of 0.62 to to 0.68. in it Laboratory Sup<*rvisor/Lead VAB.0001198425 Date A?-?/ Customer Technic PVC BULK TRAILER ANALYSIS Product Trailer Number /' A Particle Size Distribution: Screen Analysis Mesh Size Gross Wt Ta Net Wt H on Mesh Screen Analysis 40 Mesh Size Gross Wt. Tare Net Wt H on Moeh 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 gins. Carb 60 80 100 120 140 200 GUassy Pan Part. O-fK *> 1% o Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Pan 60 60 100 120 140 200 Glassy Part. Remarks % Star 207A Revised 1/12/87 VAB.0001198426 PIJhHIttlhlttfllll "iM Hi|||llln|'l|kli1Mi|iim^d-.MMI'HIP"- i^'MHirPMi- H'Uiifi'ii:jMi*f"iiM'",->nir|n|iijfitigm4ti|i'rtPttttlL"'MTVli>li' l> MP*fT^IIIPiH|nilinTnff!Tr|inMV|fi|linVVP!Vtt'l|^l|l||IV|l|pi||VIVVfnifffTTflVVtV|VVV||VVV|nT1^1l^(Tf|IVV1lfnMinVVIVTEIIVnffl1lf 1 a iiiim pim ruv' - :<imoimp -inr- '^n ^i11 r'lc.^i'' ! --Mi`lP`j3i|nmMi,'PFJrvpMim:|iiijii,He'-p-ipnt?ii, J i i I. I I i I I I I I I I I I I I i i i i i i 4 i VAB.0001198427 p Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 Date: 5/17/91 Customer: X-Rail Systems 116 Pointer Street Newark, NJ 07114 Attention: Ray Stone Date of Shipment: 5/13/91 VISIA Product: 5385-3S Resin Order No.: 855544-175 Car No.: UTCX 48054 Property Compartment A CA CB Test Method Volatiles (Wt.X) .12 Contamination, (Blk/Brn) 2/6 Bulk Density, gm/cc. .569 Particle Size X on 40 Mesh X on 200 Mesh X on Pan 0.0 7.0 1.7 .11 3/5 .582 .03 3/7 .583 .03 2/5 . 569 Composite Result ABR-1A ABR-5A ABR-2A ABR-3 "b" Color RVCM, ppm 1.60 0.136 ABR-9 ABGC-26 This material was produced to yield an inherent viscosity of 0.90 -0.95 J. Richard Williams Quality Control Supervisor VAB.0001198428 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369*8111 Date: 5/14/91 Customer: X-Rail Systems 116 Pointer Street Newark. NJ 07114 Attention: Ray Stone Date of Shipment: 5/13/91 VISTA Product: 5385-3S Resin Order No.: 894576-066 Car No.: UTCX 48054 Compartment _CA_ CB Test Method Volatiles (Wt.X) .12 .11 .03 .03 ABR-1A Contamination, (Blk/Brn) 2/6 3/5 3/7 2/5 ABR-5A Bulk Density, gm/cc. .569 .582 .583 .569 ABR-2A Particle Size X on 40 Mesh X on 200 Mesh X on Pan 0.0 7.0 1.7 ABR-3 Composite Result "b" Color 1.60 ABR-9 RVCM, PPm 0.136 ABGC-26 This material was produced to yield an inherent viscosity of 0.90 -0.95 J. Richard Williams Quality Control Supervisor VAB.0001198429 'I < iii ;i . i ' i ^ ti "y t I HI *4 `I, \* V i *t /I'M *i i | /'V f *>- -.f %`r, .* J A Load Date: Product: Car Mo : Tine Logged In: J^farOO Logged In Bjr: Ship Date: Silo(a): Customer: Screen Analysis Mesh 40 60 Weight X a-<^> p s LI 80 100 120 140 LL ton 17 oJo? ILL 200 Pan 7-0 -L2. Drytine: Static Plot#: Avg. Microns: & Color L: 1*1 0'08 b / z> Technician VAB.0001198430 IP uX \\\ a-vd dp flyjL&L 3 dCvcvs '/"0 SHIPMENT 13 X VERS TONS * A * DATE: RAILCAR/TRAILER: PRODUCT: ORIGINAL CUSTOMER LOCATION: 53 iS ORIGINAL ORDER NUMBER NEW CUSTOMER: LOCATION: NEW ORDER NUMBER: DIVERSION AUTHORIZED BY: CUSTOMER SERVICE REP./ SUPERVISOR Aberdeen La 17s- TO: B b lrv&->* ' 0,**..C oojLv "BO J flu C-C `HajLvi 3 t*x odouUdP '~+?t CJfCL^d CO I/I ltd? hX**- /iU-i pCL^*-*- ca3oV >l/)0fddl rP fr> 10*d 960ft WdiT T66I !-(- . M AUW -fehi t bisinsoi rM /I A1 5 /7 VAB NOisnoH yisin:woaj Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 Date: 5/17/91 Customer: X-Rail Systems 116 Poinier Street Newark, NJ 07114 Attention: Ray Stone Date of Shipment: 5/15/91 VISTA Product 5385-3S Resin Order No. 855544-176 Car No. VIPX 45727 Coapft.rtffl3nt A ca OR Test Method Volatiles (Wt.X) . 10 06 .11 .09 ABR-1A Contamination, (Blk/Brn) 4/3 Bulk Density, gm/cc. .587 9/4 8,593 7/5 . 580 6/4 .581 ABR-5A ABR-2A Particle Size X on 40 Mesh X on 200 Mesh X on Pan 0.0 7.3 1.6 ABR-3 Composite Result "b" Color 1.59 ABR-9 RVCM, ppm 0.260 ABGC-26 This material was produced to yield an inherent viscosity of 0.90 -0.95 J. Richard Williams Quality Control Supervisor VAB.0001198432  DATE: RAILCAR/TRAILER: w a PRODUCT: ORIGINAL CUSTOMER: + LOCATION: M ORIGINAL ORDER NUMBER: ft MEN CUSTOMER: * LOCATION: NEW ORDER NUMBER: DIVERSION AUTHORIZED BY fe Ship dj*J$ Aber^toftn Laboratory 1 * t 4pa** . M t t *, N 1 i A *f t % 4 VAB.0001198433 * i ir i v 4fr ' JJ ^ ^ ' * ' tfe *W ^ ., Ht jjW`1^ I" '"-llrf- 14 ............. ^ ' V T" '* v V hr" ^ 1 J ' hl-.rjv %*: / %v'g- *. J 4^ 4 PVC RAILCAR ANALYSIS Load Date: Product: | 538C | Car No.: Tine Logged In; Logged In By: Ship Date: Silo(s) Cuatoner Screen Analysis Mesh 40 Weight % cp. ^ 60 o. 31 80 IM1 37-8 too 13,33 -2<.fc 120 g.go i2JL 140 <f.C B.8 200 5.93 so Pan ay? / 'fe Drytime: 4,3 Static Plow: O iZA Avg. Microns: I V Color L: 1 a o. i o b l. Technician T -OP.S VAB.0001198434