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FOR DU FONT USE ONLY Skin IrritaKw AR226-2946 Du Font HLR 112*90 In Rabbits Study Completed On March 5, 1990 PerformingLaboratory Haskell LEa. bIo.radtouryPofm|si r dTe oNxeicmooluorgsy anandd CIofmldpuansyt,riaInl cM. edicine Elkt w Road, P. Q. Box 50 Newark, Delaware 19714 Laboratory Project ID Haskell Laboratory Report No. 112-90 Page 1 of 8 company Sanded. Does not contain TSCA CBf GENERAL INFORMATION Du Pont HLR 112-90 Material Tested: Medical Research No.: Haskell No.: Hasken Test Code Ho.'. Physical Form; Purity: Composition: 18,267 Amber dispersion Synonym: Stability: Sponsor: The test material was assumed to be stable under the conditions of administration. Chemicals and Pigments Department E. I. du Pont de Nemours and Company, Milmlngton, Delaware Inc. Material Submitted By; Study Initiated - Completed: In-Life Phase Initiated - Completed: Teals and Pigments Department E* I. du Pont de Nemours and Company, Jackson Laboratory Deepwater, New Jersey Inc. 2/2/90 - 3/5/90 2/6/90 - 2/8/90 Notebook: There are 8 pages in this report. Distribution: 2 company Sanitized. Does not contain TSCA CBI Sk1r> Irr1tatl|onTest with DU Font HLR 112-90 hn Rabbits SUNWRY was evaluated for acute skin Irritation potential In 5 male'rabblts. _ie__te__st Material produced no dermal Irritation In any of th^reated rabolts during the study. Under the conditions of this study, HUI^hras not a skin Irritant. Work by: /.tt^Utft. Ufc/^A Carol Finl^ Technician- Study Director; L^^\Jj.oohnnrin^BxyQ.s^AaAr.ve^r \ Technologist Approved by: ^.B.A^k res E. Maiek, Ph.D. Research Toxicologlst Acute and Developmental Toxicology Division Reviewed and Approved for Issue: ^.^fiA^^ John lit. Sarver Study Director ^/r/^o Acknowledgment: Cralg Lightcap also participated In the conduct of this study. JWS:a1r;HLR39.12 - 3- Company Sanitized. Does not contain TSCA CBI '.. ";.'. ''^'v-'^^^'^s ' y ^ ^ ^Du Font BUt m'99 ',;?; ^ . STUDY DIRECTOR: 2/28/90 4 - - Company Sanitized. Does not contain TSCA CB1 DuPont HLB 112^0 The purpose of Wl of f when oppi 1 rabbits. This study w Laboratory Practice (Dp; the study records. No validity of the study. skin Irritation potential In of New Zealand NMte ke applicable EPA Good I lance are documented in niftcantly affected the l|tttilBll^^^^ A. Animal Husbandry NWl Young adult male New Zealand White r^l Marl and, Hewitt, New Jeriify. ^he rabMl^ suspended, stainless stci t, lifye^eslca|l unique Identification mil iber which was rec were received from Hare housed singly In Each rabbit was assigned a >d on a card affixed to the cage. Purl na Certified I Kflh NNr ft 9Q325 and water were available ad llbltua exc pt as noted wrt^r, itocol. Rabbits were quaranttne'ar weighe'd and observed for oert^ ;neaitn for approximately 2 weeks. Animal rooiiswepi?(i1i1<nedeNit^ ^controlled, 12-hour Hght/12-hour dark cycle, EnylrenBiental'^i Itlons of the rooms were targeted for a telBperatu < of 20*C * ? IH'iI relative humidify of SOS + 10%. Any excursions out >1de these Ganges wi |Ne of small magnitude and/or brief duration and did n<t adversely affect the validity of the study. B. Protocol On the day prior to IstudyInitiation, Nlj? hair of 6 male New Zealand White rabbits was closel, ' clipped to expiose l^ie skin from the scapular to the lumbar region of the back. The rabNtS^^body weights ranged from 2477 to 2733 grams on th day of treatment, Each rabbit was placed Into a stock ih^%had been fitted with a piece.of rubber sheet1n< ,, approximately ^ ^18". The rabbits remained In the stocks throughoul fne exposureyey^^nd during that time did not have access to food or water. Approxi lately 0.5 mL of 1------frwas applied directly on the test site beftea'tsh:C^-tnch gauze square that was held In place with non-Irritating t<lpe ^ rubber sheeting was then wrapped around the animal and securedwflsh ^Ips to retard evaporation and to keep the test material In contact witn the skin without undue pressure. Company Sanitized. Does not contain TSCA CB1 WM^ One rabbit died during exposure period, ^ross pathological examination revealed no abnoi attributed to stress associa' iI lwltf^^hs.^ the ideaftD.of this rabbit was, le^N ^ restraint. ------ produced no dermal Irritation In any o* the rtiallBing rabbits during the study. Individual skin Irrit ttion scp'res ape presented In Table II. A sumnary of responses Is prese ited In the table. Summary of Skin Responses Response No Response Erythena zrnr aihr 5/5 . 5/5 Edema 24 hr 48"nr" 5/5 5/5 Under the conditions of wts study. 'was not a skin Irritant. 6 Company Sanitized. Does nol fconlam TSCA CBl ^.a'iW'sH" Du Pont HLR 112.90 ! TWLC I PRAIZg1SCALE FORSCORIN6 PRIMARY SKIM IRRITATION Evaluation of Skin Reactions Erythema and eschar formation: No erythena ; Very slight erythema (barely perceptible) Well-defined erythena Moderate to severe erythema Severe erythema (beet redhess) to slight eschar formation (Injuries In! depth) Value 1 (Slight) 2 (Mild) 3 (Moderate) 4 (Severe) Edema formation: No edema Very slight edena (barely perceptible) Slight edema (edgeiss o< f area well defined by definite raising) Moderate edema (raised approximately 1.0 nm) Severe edema (raised more'than 1.0 mm extending beyond the area of exposure) 1 (Slight) 2 (Mild) 3 (Moderate) 4 (Severe) Abbreviations of other Abraded Intact Thickening Eschar No Effect Blanching dermal effects are: F = (assuring N = Necrosis G s Fissuring with (Heeding S = Epidermal Scaling L Sloughing R Raw Areas X Compound Adhered to Skin SN Superficial Necrosis 1 Draize, J. H., "Dermal Toxiclty." Appraisal of the Safety of Chemicals In Foods, Drugs and Cosmetics, The Editorial Committee of the Association of Food and Drug Officials Of the United States, Austin, Texas, 1959, pp. 46-59. Company Sanitized. Does not contain TSCA CBI - . ,i, RabMt ^^TirT ^ Number 24565 24566 24567 24568 24569 24570 ' 5 5 ^ MUJ& '^y'^*""'5f F W Ed jill hr 48 ftP 9 0 0 0 0 0 0 0 0 0 0 0 ^ : 0 0 l 1 j 0 0 - - 0 0 0 0 Rabbit dieflduring the exposure period. Company Sanitized. Does not contain TSCA CBI