Document yXwkKEe2BrGEpwxy6wLGMO3X
BOILING POINT
TEST SUBSTANCE
Identity:N-ethylperfluorooctasnuelfonamidoethanolm;ay alsobe referretdo as N-ETFOSE Alcohol,FC-10,or FM-3422. (I-OctanesulfonamideN,-. ethyl1-,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-heptadecafluoro-N-(2hydroxyethyl)C-A,S # 1691-99-2)
Remarks: Materialisan off-whitew,axy solid.
METHOD:
Method followed: The boilinpgointwas determinedas a partoftheOECD Guideline104,"Vapor PressureCurve,Dynamic Method" study.
GLP: No .Yearstudy was performed: 1998 Remarks: Materiailsstableatroom temperature.Sample was indicatetdobe 99% pure inthevapor pressurestudy.
RESULTS
The followintgablesummarizes boilinpgointsmeasured duringvapor pressure testingofthe N-ETFOSE Alcoholmaterialp,lustheextrapolatiovnalueat atmosphericpressure.
rp
42
174.6
55
179.0
67
187.2
81
190.2
96
197.0
760*
474*
i'=0.9902
Extrapolatedvalues
37
172.2
48
176.4
68
188.2
83
191.6
93
195.8
760*
482*
r'=0.9908
Remarks:, No notewas made ifany decompositionwas occurring. CONCLUSIONS
Testingshouldbe conductedto recordan empiricavlalueto replacethe extrapolateodnes.
DATA QUALITY
ReliabilityK:limischranking= 3. The boilinpgointwas notobtainedempirically. Boilingpointvalueswere extrapolatefdromdataobtainedduringvapor pressure testing.
REFERENCES
Deterininatioonf Vapor PressureCurve by Dynamic Method forU1463 (ET FOSE), AScl Report# 044-VP.R3M, AScl Study ID #5030-044-01,Noverhber6, 1998. Conducted attherequestof3M Company.
OTHER
Submitter: 3M Company, EnvironmentalLaboratoryP,.O. Box 33331,St.Paul, Minnesota,55133
Last changed: 5/15/00
M;MM ASc I Corp.
R-DE NO. 218 722 2592
Nov. 30 1998 e4:31PM P2' =nON-WON
CAM Novemba30,1998
AS,clCorporation
4444,,@irpgaorukilvardC,)UlutM@i)n,nesqt5a58,1
(2187)22-4040
Fax(2187)22-2592
Ms. SusanBeach 3M EnvironmentalTechnology & SafetyServices 935 Bu,ShAvenue
St.Paul,Minnescga 55133
Dw Us. Beach:
I am writinginre$Ponw to your requestof boilingpointinformationfortestitemsU1463 and U1464- Unfominatdy we didnot obtainempiricalvaluesfortheboilingpointof eitheritom.
Although experimentalvalueswere not obtained,we did extrapolawvaluesusingthe tempenture and preaure curves obtainedforboth items. The tablesbelow summarize the exrrapoladons.
Testitem UIAO
... . .........
42
5e915l6 67200
67
- *70 2 760
r2.o.9m
174.6 179.0 197.2
190.2 197.0
474
-reuun @MmHg)
3'1 4t 68 93 93 760
Boilin..gT"Dmp.
L722m.2P2'1*(" .6
176.-4
191.6 195.8
482
I= ItemIJ14fd
42
171.6
58
178.8
68
181.8
9863
186.4
iS94
68
760
r
4M
r2.O."61
47
174.4
75
1$5883..088
96
isslo
9s
191'-40
191.0
L(*
193.0
7W
1407
si-0.9960
FROM Asci Corp.
MaE NC). 218 722 25M
NOV.-30 igga 04:31PM P3
Novetnber30, 1998 UL Beach- 3M Co. Page - 2 -
I Wlogi2e Ow dw extrapolatevdalueswam allwe can provide-7U boilingpointforboth compounds shouldhave been detamined befortvaporpressuredetmiiiinationP.leam callifyou' need Awdw information.
Sincerei
0?o0c Amato Deputy Director,AScl-ETD